IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 121739-001
Client Name, Sample Details

Mike Smith
Macomb, MI 48044
Sample: Concentrate Syrup
Type: Tincture
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP200217a
Scale: XS205-MI2
Temp: 20.6 °C
Baro Pressure: 995.3 hPa
Analyst: KEB
Technician: ANJ/KEB
Sample ID#: 121739

Harvest/Process Date: 02/18/2020
Serving Size (g): 1
Date Received: 02/18/2020
Test Date: 02/17/2020
Valid Through: 02/17/2021
Report Issued: 02/18/2020
Sample #121739
Sample #121739 Sample #121739
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.4 N/D 0.1 N/D 0.0 0.0 0.1 N/D N/D 0.6 0.4 0.1 0.6
Amount (mg/g) 4.2 N/D 0.6 N/D 0.1 0.2 0.5 N/D N/D 5.6 4.2 0.6 5.7
Amount per Serving (mg) 4.2 N\D 0.6 N\D 0.1 0.2 0.5 N\D N\D 5.6 Serving Size~ (g): 1.0
LOQ (mg/g) 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08   %Decarb. THC CBD
±%RPD 2.38 1.39 3.78 0.46 0.49 1.27 1.53 0.27 0.78 100% 100%

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 121739-001
Client Name, Sample Details

Mike Smith
Macomb, MI 48044
Sample: Concentrate Syrup
Type: Tincture
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP200217a
Scale: XS205-MI2
Temp: 20.6 °C
Baro Pressure: 995.3 hPa
Analyst: KEB
Technician: ANJ/KEB
Sample ID#: 121739

Harvest/Process Date: 02/18/2020
Serving Size (g): 1
Date Received: 02/18/2020
Test Date: 02/17/2020
Valid Through: 02/17/2021
Report Issued: 02/18/2020
Sample #121739
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 5.6328 6.02906 107.03 5.98241 106.21 0.78
Cannabidiolic Acid (CBDA) 0 5.34989 5.5344 103.45 5.56017 103.93 0.46
Cannabigerol (CBG) 0 5.59525 5.78054 103.31 5.85415 104.63 1.27
Cannabidiol (CBD) 0 5.59702 5.41749 96.79 5.62631 100.52 3.78
Δ9-Tetrahydrocannabivarin (THCV) 0 5.75851 5.81456 100.97 5.79879 100.70 0.27
Cannabinol (CBN) 0 5.53079 5.64938 102.14 5.67693 102.64 0.49
Δ9-Tetrahydrocannabinol (THC) 0 5.54669 5.99187 108.03 5.8508 105.48 2.38
Cannabichromene (CBC) 0 5.81463 5.96263 102.55 5.8723 100.99 1.53
Tetrahydrocannabinolic acid (THCA) 0 5.56744 5.5758 100.15 5.49856 98.76 1.39

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 77802 Test Certificate #: 121739-001
Client Name, Sample Details

Mike Smith
Macomb, MI 48044
Sample: Concentrate Syrup
Type: Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Prepsheet ID#: MIPS200219a
Scale: XS205-MI2
Temp: 20.8 °C
Baro PE: 994.7 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 121739

Harvest/Process Date: 02/18/2020
Serving Size (g): 1
Date Received: 02/18/2020
Test Date: 02/19/2020
Valid Through: 02/19/2021
Report Issued: 02/21/2020
Sample #121739
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.125 Pass/<LOD Abamectin**** 0.500 0.125 Pass/<LOD
Acephate 0.400 0.125 Pass/<LOD Acequinocyl 2.000 0.250 Pass/<LOD
Acetamiprid 0.200 0.125 Pass/<LOD Azoxystrobin 0.200 0.125 Pass/<LOD
Bifenazate 0.200 0.125 Pass/<LOD Bifenthrin 0.200 0.125 Pass/<LOD
Boscalid 0.400 0.125 Pass/<LOD Carbaryl 0.200 0.125 Pass/<LOD
Carbofuran 0.200 0.125 Pass/<LOD Chlorantraniliprole 0.200 0.125 Pass/<LOD
Chlorfenapyr 1.000 0.500 Pass/<LOD Chlorpyrifos 0.200 0.125 Pass/<LOD
Clofentezine 0.200 0.125 Pass/<LOD Cyfluthrin** 1.000 0.500 Pass/<LOD
Cypermethrin*** 1.000 0.500 Pass/<LOD Daminozide 1.000 0.500 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.250 Pass/<LOD Diazinon 0.200 0.125 Pass/<LOD
Dimethoate 0.200 0.125 Pass/<LOD Ethoprophos 0.200 0.125 Pass/<LOD
Etofenprox 0.400 0.125 Pass/<LOD Etoxazole 0.200 0.125 Pass/<LOD
Fenoxycarb 0.200 0.125 Pass/<LOD Fenpyroximate 0.400 0.125 Pass/<LOD
Fipronil 0.400 0.125 Pass/<LOD Flonicamid 1.000 0.125 Pass/<LOD
Fludioxonil 0.400 0.125 Pass/<LOD Hexythiazox 1.000 0.125 Pass/<LOD
Imazalil 0.200 0.125 Pass/<LOD Imidacloprid 0.400 0.125 Pass/<LOD
Kresoxim Methyl 0.400 0.125 Pass/<LOD Malathion 0.200 0.125 Pass/<LOD
Metalaxyl 0.200 0.125 Pass/<LOD Methiocarb 0.200 0.125 Pass/<LOD
Methomyl 0.400 0.125 Pass/<LOD Methyl Parathion 0.200 0.125 Pass/<LOD
MGK-264‡ 0.200 0.125 Pass/<LOD Myclobutanil 0.200 0.125 Pass/<LOD
Naled 0.500 0.125 Pass/<LOD Oxamyl 1.000 0.125 Pass/<LOD
Paclobutrazol 0.400 0.125 Pass/<LOD Permethrins† 0.200 0.125 Pass/<LOD
Phosmet 0.200 0.125 Pass/<LOD Piperonyl Butoxide 10.000 1.900 Pass/<LOD
Prallethrin 0.200 0.125 Pass/<LOD Propiconazole 0.400 0.125 Pass/<LOD
Propoxur 0.200 0.125 Pass/<LOD Pyrethrins* 1.000 0.125 Pass/<LOD
Pyridaben 0.200 0.125 Pass/<LOD Spinosad***** 0.200 0.125 Pass/<LOD
Spiromesifen 0.200 0.125 Pass/<LOD Spirotetramat 0.200 0.125 Pass/<LOD
Spiroxamine‡ 0.400 0.125 Pass/<LOD Tebuconazole 0.400 0.125 Pass/<LOD
Thiacloprid 0.200 0.125 Pass/<LOD Thiamethoxam 0.200 0.125 Pass/<LOD
Trifloxystrobin 0.200 0.125 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Pesticide QC Report
Testing Accreditation #: 77802 Test Certificate #: 121739-001
Client Name, Sample Details

Mike Smith
Macomb, MI 48044
Sample: Concentrate Syrup
Type: Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Prepsheet ID#: MIPS200219a
Scale: XS205-MI2
Temp: 20.8 °C
Baro PE: 994.7 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 121739

Harvest/Process Date: 02/18/2020
Serving Size (g): 1
Date Received: 02/18/2020
Test Date: 02/19/2020
Valid Through: 02/19/2021
Report Issued: 02/21/2020
Sample #121739
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.09 0.982 109.00 98.20 10.42
Acequinocyl N.D. 1 0.405 0.375 40.50 37.50 7.69 LR
Acetamiprid N.D. 1 0.966 1.08 96.60 108.00 11.14
Aldicarb N.D. 1 1.02 1.05 102.00 105.00 2.90
Avermectin B1a N.D. 0.97 1.04 0.873 107.22 90.00 17.46
Azoxystrobin N.D. 1 1.04 1 104.00 100.00 3.92
Bifenazate N.D. 1 0.29 0.239 29.00 23.90 19.28 LR
Bifenthrin N.D. 1 0.909 0.797 90.90 79.70 13.13
Boscalid N.D. 1 1.05 0.83 105.00 83.00 23.40
Carbaryl N.D. 1 1.11 1.11 111.00 111.00 0.00
Carbofuran N.D. 1 1.11 0.882 111.00 88.20 22.89
Chlorantraniliprole N.D. 1 0.984 1.14 98.40 114.00 14.69
Chlorfenapyr N.D. 1 1.1 1.02 110.00 102.00 7.55
Chlorpyriphos N.D. 1 1.01 0.94 101.00 94.00 7.18
Clofentezine N.D. 1 0.896 0.788 89.60 78.80 12.83
Cyfluthrin N.D. 1 1 0.912 100.00 91.20 9.21
Cypermethrin N.D. 1 1.05 0.973 105.00 97.30 7.61
Daminoside N.D. 1 0.37 0.372 37.00 37.20 0.54 LR
Diazanon N.D. 1 0.989 0.958 98.90 95.80 3.18
Dichlorvos N.D. 1 1.03 0.793 103.00 79.30 26.00
Dimethoate N.D. 1 1.16 1.01 116.00 101.00 13.82
Ethoprophos N.D. 1 1.07 0.901 107.00 90.10 17.15
Etofenprox N.D. 1 0.893 0.819 89.30 81.90 8.64
Etoxazole N.D. 1 1.08 1.02 108.00 102.00 5.71
Fenoxycarb N.D. 1 1.08 0.973 108.00 97.30 10.42
Fenpyroximate N.D. 1 0.944 0.843 94.40 84.30 11.30
Fipronil N.D. 1 1.28 1.31 128.00 131.00 2.32 HR
Flonicamid N.D. 1 1.17 1.07 117.00 107.00 8.93
Fludioxonil N.D. 1 1.07 1.06 107.00 106.00 0.94
Hexythiazox N.D. 1 0.879 0.854 87.90 85.40 2.89
Imazalil N.D. 1 1.17 1.03 117.00 103.00 12.73
Imidacloprid N.D. 1 1.14 1.06 114.00 106.00 7.27
Kresoxim-methyl N.D. 1 0.956 0.692 95.60 69.20 32.04 Q
Malathion N.D. 1 0.979 1.15 97.90 115.00 16.06
Metalaxyl N.D. 1 1.11 1.1 111.00 110.00 0.90
Methiocarb N.D. 1 1.16 1.07 116.00 107.00 8.07
Methomyl N.D. 1 1.04 1.1 104.00 110.00 5.61
MGK-264 N.D. 1 0.686 0.611 68.60 61.10 11.57
Myclobutanil N.D. 1 1.1 0.958 110.00 95.80 13.80
Naled (dibrom) N.D. 1 0.544 0.474 54.40 47.40 13.75 LR
Oxamyl N.D. 1 1.13 0.942 113.00 94.20 18.15
Paclobutrazol N.D. 1 1.1 0.87 110.00 87.00 23.35
Parathion-methyl N.D. 1 .723 .902 72.30 90.20 22.03
Permethrins N.D. 1 0.778 0.769 77.80 76.90 1.16
Phosmet N.D. 1 1.04 0.783 104.00 78.30 28.20
Piperonyl butoxide N.D. 1 1.13 0.952 113.00 95.20 17.10
Prallethrin N.D. 1 0.995 0.961 99.50 96.10 3.48
Propiconazole N.D. 1 0.941 0.867 94.10 86.70 8.19
Propoxur N.D. 1 1.1 0.999 110.00 99.90 9.62
Pyrethrin N.D. 0.65 0.651 0.564 100.15 86.77 14.32
Pyridaben N.D. 1 0.973 0.894 97.30 89.40 8.46
SpinosynA N.D. 0.84 0.858 0.718 102.14 85.48 17.77
SpinosynD N.D. 0.16 0.172 0.159 107.50 99.38 7.85
Spiromesifen N.D. 1 0.27 0.278 27.00 27.80 2.92 LR
Spirotetramat N.D. 1 1.04 0.891 104.00 89.10 15.43
Spiroxamine N.D. 1 1.13 1 113.00 100.00 12.21
Tebuconazole N.D. 1 0.984 0.919 98.40 91.90 6.83
Thiacloprid N.D. 1 1.12 1.05 112.00 105.00 6.45
Thiamethoxam N.D. 1 1.09 1.1 109.00 110.00 0.91
Trifloxystrobin N.D. 1 0.97 0.843 97.00 84.30 14.01

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 77802 Test Certificate #: 121739-001
Client Name, Sample Details

Mike Smith
Macomb, MI 48044
Sample: Concentrate Syrup
Type: Tincture
Method: SOP FE-44-OR3
Test Conditions

Prepsheet ID#: 200217a
Scale: XS205-MI2
Temp: 20.3 °C
Baro PE: 988 hPa
Analyst: JRT
Technician: ANJ
Sample ID#: 121739

Harvest/Process Date: 02/18/2020
Serving Size (g): 1
Date Received: 02/18/2020
Test Date: 02/17/2020
Valid Through: 02/17/2021
Report Issued: 02/18/2020
Sample #121739
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 250 Pass/<LOD 1,2-Dimethoxyethane 5,000 250 Not Tested
1,4-dioxane 5,000 25 Not Tested 1-Butanol 5,000 250 Not Tested
1-Pentanol 5,000 250 Not Tested 1-Propanol 5,000 250 Not Tested
2,2-Dimethylpropane (Neopentane) 750 25 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 50 25 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 50 25 Pass/<LOD 2-Butanol 5,000 25 Not Tested
2-Butanone (MEK) 5,000 250 Not Tested 2-Ethoxyethanol 5,000 25 Not Tested
2-Methylbutane (Isopentane) 750 25 Pass/<LOD 2-Methylpentane (Hexanes) 50 25 Pass/<LOD
2-Methylpropane (Isobutane) 800 25 Pass/<LOD 2-propanol (Isopropyl Alcohol) 500 25 Pass/<LOD
2-Propanone (Acetone) 750 25 Pass/<LOD 3-Methylpentane (Hexanes) 50 25 Pass/<LOD
Acetonitrile 60 25 Pass/<LOD Benzene 1 1 Pass/<LOD
Butane 800 25 Pass/<LOD Chloroform 2 2 Pass/<LOD
Cumene 5,000 25 Not Tested Cyclohexane 50 25 Not Tested
Dichloromethane 125 25 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 250 Not Tested
Ethanol 1,000 25 Pass/<LOD Ethyl acetate 400 25 Pass/<LOD
Ethyl ether 500 25 Pass/<LOD Ethylene glycol 5,000 25 Not Tested
Ethylene oxide 5 3 Pass/<LOD Heptane 500 25 Pass/<LOD
Hexane 50 25 Pass/<LOD Isopropyl acetate 5,000 25 Not Tested
Methanol 250 25 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 5,000 250 Not Tested N,N-Dimethylformamide (DMF) 5,000 250 Not Tested
Pentane 750 25 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 2,100 25 Pass/<LOD Pyridine 5,000 250 Not Tested
Sulfolane 5,000 25 Not Tested Tetrahydrofuran (THF) 5,000 25 Not Tested
Toluene 150 25 Pass/<LOD Trichloroethylene 25 25 Pass/<LOD
Xylenes* 150 25 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Residual Solvents QC Report
Testing Accreditation #: 77802 Test Certificate #: 121739-001
Client Name, Sample Details

Mike Smith
Macomb, MI 48044
Sample: Concentrate Syrup
Type: Tincture
Method: SOP FE-44-OR3
Test Conditions

Prepsheet ID#: 200217a
Scale: XS205-MI2
Temp: 20.3 °C
Baro PE: 988 hPa
Analyst: JRT
Technician: ANJ
Sample ID#: 121739

Harvest/Process Date: 02/18/2020
Serving Size (g): 1
Date Received: 02/18/2020
Test Date: 02/17/2020
Valid Through: 02/17/2021
Report Issued: 02/18/2020
Sample #121739
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 250 248 255 99.20 102.00 2.78
n-Propane N.D. 250 200 257 80.00 102.80 24.95 Q
Isobutane N.D. 250 228 248 91.20 99.20 8.40
Methanol N.D. 250 194 197 77.60 78.80 1.53
n-Butane N.D. 250 235 248 94.00 99.20 5.38
2,2-Dimethylpropane N.D. 250 239 255 95.60 102.00 6.48
Ethanol N.D. 250 211 219 84.40 87.60 3.72
Isopentane N.D. 250 254 259 101.60 103.60 1.95
Acetonitrile N.D. 250 227 231 90.80 92.40 1.75
Diethyl ether N.D. 250 240 253 96.00 101.20 5.27
2-propanone N.D. 250 240 241 96.00 96.40 0.42
2-propanol N.D. 250 230 235 92.00 94.00 2.15
n-Pentane 91.58 250 260 268 104.00 107.20 3.03 I
2,2-Dimethylbutane N.D. 250 251 261 100.40 104.40 3.91
2,3-Dimethylbutane N.D. 250 248 262 99.20 104.80 5.49
Methylene chloride N.D. 250 233 237 93.20 94.80 1.70
2-Methylpentane N.D. 250 254 259 101.60 103.60 1.95
3-Methylpentane N.D. 250 254 264 101.60 105.60 3.86
2-Butanol N.D. 0 0 0 0.00 0.00 0.00
n-Hexane N.D. 250 252 259 100.80 103.60 2.74
Ethyl acetate N.D. 250 230 238 92.00 95.20 3.42
Tetrahydrofuran N.D. 0 0 0 0.00 0.00 0.00
Trichloroethylene N.D. 25 26 27 104.00 108.00 3.77
Isopropyl acetate N.D. 0 0 0 0.00 0.00 0.00
Benzene N.D. 25 26 26 104.00 104.00 0.00
Chloroform N.D. 25 24 24 96.00 96.00 0.00
Cyclohexane N.D. 0 0 0 0.00 0.00 0.00
Ethylene glycol N.D. 0 0 0 0.00 0.00 0.00
Heptane N.D. 250 275 279 110.00 111.60 1.44
2-Ethoxyethanol N.D. 0 0 0 0.00 0.00 0.00
1,4-Dioxane N.D. 0 0 0 0.00 0.00 0.00
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 260 262 104.00 104.80 0.77
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 0 0 0 0.00 0.00 0.00
m-Xylene/p-Xylene N.D. 125 126 128 100.80 102.40 1.57
o-Xylene N.D. 125 123 127 98.40 101.60 3.20
Cumene N.D. 0 0 0 0.00 0.00 0.00
Ethylene oxide N.D. 25 24 27 96.00 108.00 11.76

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Heavy Metals Analysis
Testing Accreditation #: 77802 Test Certificate #: 121739-001
Client Name, Sample Details

Mike Smith
Macomb, MI 48044
Sample: Concentrate Syrup
Type: Tincture
Method: FE60 ICPMS-MI
Test Conditions

Prepsheet ID#: MIICP200213aMK
Temp: 19.5 °C
Baro PE: 973.6 hPa
Analyst: TAC
Technician: MK
Sample ID#: 121739

Harvest/Process Date: 02/18/2020
Serving Size (g): 1
Date Received: 02/18/2020
Report Issued: 02/17/2020
Sample #121739
Sample #121739 Sample #121739
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Arsenic 1.5 0.1 Pass/<LOD
Copper 0 1.5 Not Tested
Cadmium 0.5 0.1 Pass/<LOD
Chromium 2 0.3 Pass/<LOD
Lead 0.5 0.25 Pass/<LOD
Mercury 3 0.05 Pass/<LOD
Nickel 0 0.25 Not Tested

The testing requirements set by the MRA for copper and nickel will not be effective until July 1, 2020.

MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 121739-001
Client Name, Sample Details

Mike Smith
Macomb, MI 48044
Sample: Concentrate Syrup
Type: Tincture
Method: FE60 ICPMS-MI
Test Conditions

Prepsheet ID#: MIICP200213aMK
Temp: 19.5 °C
Baro PE: 973.6 hPa
Analyst: TAC
Technician: MK
Sample ID#: 121739

Harvest/Process Date: 02/18/2020
Serving Size (g): 1
Date Received: 02/18/2020
Report Issued: 02/17/2020
Sample #121739
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD QC Flag
Arsenic N/D 0.160 0.156 97.50 0.149 93.13
Cadmium N/D 0.160 0.163 101.88 0.146 91.25
Chromium N/D 0.480 0.724 150.83 0.622 129.58 HR
Copper N/D 2.400 2.813 117.21 2.523 105.13
Lead N/D 0.400 0.369 92.25 0.332 83.00
Mercury N/D 0.080 0.087 108.75 0.080 100.00
Nickel N/D 0.400 0.477 119.25 0.405 101.25

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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