IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 121735-001
Client Name, Sample Details

Michael Biggs
Taylor, MI 48180
Sample: Wedding Mints
Type: Flower
Method: FE04U HPLC-UV
***Water Activity: 0.35
***Moisture: 12.11%
Test Conditions

Prepsheet ID#: MIP200217a
Scale: XS205-MI2
Temp: 20.6 °C
Baro Pressure: 995.3 hPa
Analyst: KEB
Technician: ANJ/KEB
Sample ID#: 121735

Harvest/Process Date: 02/13/2020
Serving Size (g): 1
Date Received: 02/13/2020
Test Date: 02/17/2020
Valid Through: 02/17/2021
Report Issued: 02/18/2020
Sample #121735
Sample #121735 Sample #121735
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 1.1 27.9 N/D 1.8 0.1 0.1 N/D N/D N/D 31.0 25.6 1.6 27.4
Amount (mg/g) 11.3 278.9 N/D 18.0 1.1 1.0 N/D N/D N/D 310.3 255.9 15.8 273.8
Amount per Serving (mg) 11.3 278.9 N\D 18.0 1.1 1.0 N\D N\D N\D 310.3 Serving Size~ (g): 1.0
LOQ (mg/g) 0.98 0.98 0.98 0.98 0.98 0.98 0.98 0.98 0.98   %Decarb. THC CBD
±%RPD 2.38 1.39 3.78 0.46 0.49 1.27 1.53 0.27 0.78 4 0%

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 121735-001
Client Name, Sample Details

Michael Biggs
Taylor, MI 48180
Sample: Wedding Mints
Type: Flower
Method: FE04U HPLC-UV
***Water Activity: 0.35
***Moisture: 12.11%
Test Conditions

Prepsheet ID#: MIP200217a
Scale: XS205-MI2
Temp: 20.6 °C
Baro Pressure: 995.3 hPa
Analyst: KEB
Technician: ANJ/KEB
Sample ID#: 121735

Harvest/Process Date: 02/13/2020
Serving Size (g): 1
Date Received: 02/13/2020
Test Date: 02/17/2020
Valid Through: 02/17/2021
Report Issued: 02/18/2020
Sample #121735
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 5.6328 6.02906 107.03 5.98241 106.21 0.78
Cannabidiolic Acid (CBDA) 0 5.34989 5.5344 103.45 5.56017 103.93 0.46
Cannabigerol (CBG) 0 5.59525 5.78054 103.31 5.85415 104.63 1.27
Cannabidiol (CBD) 0 5.59702 5.41749 96.79 5.62631 100.52 3.78
Δ9-Tetrahydrocannabivarin (THCV) 0 5.75851 5.81456 100.97 5.79879 100.70 0.27
Cannabinol (CBN) 0 5.53079 5.64938 102.14 5.67693 102.64 0.49
Δ9-Tetrahydrocannabinol (THC) 0 5.54669 5.99187 108.03 5.8508 105.48 2.38
Cannabichromene (CBC) 0 5.81463 5.96263 102.55 5.8723 100.99 1.53
Tetrahydrocannabinolic acid (THCA) 0 5.56744 5.5758 100.15 5.49856 98.76 1.39

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 77802 Test Certificate #: 121735-001
Client Name, Sample Details

Michael Biggs
Taylor, MI 48180
Sample: Wedding Mints
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Prepsheet ID#: MIPS200218a
Scale: XS205-MI2
Temp: 21.5 °C
Baro PE: 975.0 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 121735

Harvest/Process Date: 02/13/2020
Serving Size (g): 1
Date Received: 02/13/2020
Test Date: 02/18/2020
Valid Through: 02/18/2021
Report Issued: 02/20/2020
Sample #121735
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.125 Pass/<LOD Abamectin**** 0.500 0.125 Pass/<LOD
Acephate 0.400 0.125 Pass/<LOD Acequinocyl 2.000 0.250 Pass/<LOD
Acetamiprid 0.200 0.125 Pass/<LOD Azoxystrobin 0.200 0.125 Pass/<LOD
Bifenazate 0.200 0.125 Pass/<LOD Bifenthrin 0.200 0.125 Pass/<LOD
Boscalid 0.400 0.125 Pass/<LOD Carbaryl 0.200 0.125 Pass/<LOD
Carbofuran 0.200 0.125 Pass/<LOD Chlorantraniliprole 0.200 0.125 Pass/<LOD
Chlorfenapyr 1.000 0.500 Failed/1.653 Chlorpyrifos 0.200 0.125 Pass/<LOD
Clofentezine 0.200 0.125 Pass/<LOD Cyfluthrin** 1.000 0.500 Pass/<LOD
Cypermethrin*** 1.000 0.500 Pass/<LOD Daminozide 1.000 0.500 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.250 Pass/<LOD Diazinon 0.200 0.125 Pass/<LOD
Dimethoate 0.200 0.125 Pass/<LOD Ethoprophos 0.200 0.125 Pass/<LOD
Etofenprox 0.400 0.125 Pass/<LOD Etoxazole 0.200 0.125 Pass/<LOD
Fenoxycarb 0.200 0.125 Pass/<LOD Fenpyroximate 0.400 0.125 Pass/<LOD
Fipronil 0.400 0.125 Pass/<LOD Flonicamid 1.000 0.125 Pass/<LOD
Fludioxonil 0.400 0.125 Pass/<LOD Hexythiazox 1.000 0.125 Pass/<LOD
Imazalil 0.200 0.125 Pass/<LOD Imidacloprid 0.400 0.125 Pass/<LOD
Kresoxim Methyl 0.400 0.125 Pass/<LOD Malathion 0.200 0.125 Pass/<LOD
Metalaxyl 0.200 0.125 Pass/<LOD Methiocarb 0.200 0.125 Pass/<LOD
Methomyl 0.400 0.125 Pass/<LOD Methyl Parathion 0.200 0.125 Pass/<LOD
MGK-264‡ 0.200 0.125 Pass/<LOD Myclobutanil 0.200 0.125 Pass/<LOD
Naled 0.500 0.125 Pass/<LOD Oxamyl 1.000 0.125 Pass/<LOD
Paclobutrazol 0.400 0.125 Pass/<LOD Permethrins† 0.200 0.125 Pass/<LOD
Phosmet 0.200 0.125 Pass/<LOD Piperonyl Butoxide 10.000 1.900 Pass/<LOD
Prallethrin 0.200 0.125 Pass/<LOD Propiconazole 0.400 0.125 Pass/<LOD
Propoxur 0.200 0.125 Pass/<LOD Pyrethrins* 1.000 0.125 Pass/<LOD
Pyridaben 0.200 0.125 Pass/<LOD Spinosad***** 0.200 0.125 Pass/<LOD
Spiromesifen 0.200 0.125 Pass/<LOD Spirotetramat 0.200 0.125 Pass/<LOD
Spiroxamine‡ 0.400 0.125 Pass/<LOD Tebuconazole 0.400 0.125 Pass/<LOD
Thiacloprid 0.200 0.125 Pass/<LOD Thiamethoxam 0.200 0.125 Pass/<LOD
Trifloxystrobin 0.200 0.125 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Pesticide QC Report
Testing Accreditation #: 77802 Test Certificate #: 121735-001
Client Name, Sample Details

Michael Biggs
Taylor, MI 48180
Sample: Wedding Mints
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Prepsheet ID#: MIPS200218a
Scale: XS205-MI2
Temp: 21.5 °C
Baro PE: 975.0 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 121735

Harvest/Process Date: 02/13/2020
Serving Size (g): 1
Date Received: 02/13/2020
Test Date: 02/18/2020
Valid Through: 02/18/2021
Report Issued: 02/20/2020
Sample #121735
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.904 0.994 90.40 99.40 9.48
Acequinocyl N.D. 1 0.707 0.672 70.70 67.20 5.08
Acetamiprid N.D. 1 0.901 1 90.10 100.00 10.42
Aldicarb N.D. 1 0.888 0.941 88.80 94.10 5.80
Avermectin B1a N.D. 0.97 0.86 0.945 88.66 97.42 9.42
Azoxystrobin N.D. 1 0.88 0.941 88.00 94.10 6.70
Bifenazate N.D. 1 0.48 0.484 48.00 48.40 0.83 LR
Bifenthrin N.D. 1 0.924 1.06 92.40 106.00 13.71
Boscalid N.D. 1 0.867 0.963 86.70 96.30 10.49
Carbaryl N.D. 1 0.928 0.951 92.80 95.10 2.45
Carbofuran N.D. 1 0.956 1.03 95.60 103.00 7.45
Chlorantraniliprole N.D. 1 0.878 0.87 87.80 87.00 0.92
Chlorfenapyr N.D. 1 0.916 1.01 91.60 101.00 9.76
Chlorpyriphos N.D. 1 0.93 0.944 93.00 94.40 1.49
Clofentezine N.D. 1 0.858 0.792 85.80 79.20 8.00
Cyfluthrin N.D. 1 0.899 0.973 89.90 97.30 7.91
Cypermethrin N.D. 1 0.972 1.03 97.20 103.00 5.79
Daminoside N.D. 1 0.419 0.409 41.90 40.90 2.42 LR
Diazanon N.D. 1 0.994 0.978 99.40 97.80 1.62
Dichlorvos N.D. 1 0.778 1.01 77.80 101.00 25.95
Dimethoate N.D. 1 0.892 0.982 89.20 98.20 9.61
Ethoprophos N.D. 1 0.819 0.881 81.90 88.10 7.29
Etofenprox N.D. 1 0.926 0.995 92.60 99.50 7.18
Etoxazole N.D. 1 0.965 1.05 96.50 105.00 8.44
Fenoxycarb N.D. 1 0.912 0.868 91.20 86.80 4.94
Fenpyroximate N.D. 1 0.886 0.93 88.60 93.00 4.85
Fipronil N.D. 1 1.2 1.14 120.00 114.00 5.13
Flonicamid N.D. 1 0.881 0.963 88.10 96.30 8.89
Fludioxonil N.D. 1 1.12 1.02 112.00 102.00 9.35
Hexythiazox N.D. 1 0.835 0.775 83.50 77.50 7.45
Imazalil N.D. 1 0.854 0.921 85.40 92.10 7.55
Imidacloprid N.D. 1 0.886 1.05 88.60 105.00 16.94
Kresoxim-methyl N.D. 1 0.673 0.842 67.30 84.20 22.31
Malathion N.D. 1 1.07 0.92 107.00 92.00 15.08
Metalaxyl N.D. 1 1.02 0.957 102.00 95.70 6.37
Methiocarb N.D. 1 0.962 0.88 96.20 88.00 8.90
Methomyl N.D. 1 0.987 0.994 98.70 99.40 0.71
MGK-264 N.D. 1 0.787 0.885 78.70 88.50 11.72
Myclobutanil N.D. 1 0.908 0.968 90.80 96.80 6.40
Naled (dibrom) N.D. 1 0.378 0.413 37.80 41.30 8.85 LR
Oxamyl N.D. 1 0.917 0.978 91.70 97.80 6.44
Paclobutrazol N.D. 1 0.86 0.88 86.00 88.00 2.30
Parathion-methyl N.D. 1 1.11 0.882 111.00 88.20 22.89
Permethrins N.D. 1 0.987 0.973 98.70 97.30 1.43
Phosmet N.D. 1 0.844 0.825 84.40 82.50 2.28
Piperonyl butoxide N.D. 1 1.06 1.13 106.00 113.00 6.39
Prallethrin N.D. 1 0.762 0.762 76.20 76.20 0.00
Propiconazole N.D. 1 0.82 0.86 82.00 86.00 4.76
Propoxur N.D. 1 0.917 0.996 91.70 99.60 8.26
Pyrethrin N.D. 0.65 0.455 0.564 70.00 86.77 21.39
Pyridaben N.D. 1 0.9 0.942 90.00 94.20 4.56
SpinosynA N.D. 0.84 0.51 0.661 60.71 78.69 25.79
SpinosynD N.D. 0.16 0.113 0.142 70.63 88.75 22.75
Spiromesifen N.D. 1 0.24 0.239 24.00 23.90 0.42 LR
Spirotetramat N.D. 1 0.742 0.826 74.20 82.60 10.71
Spiroxamine N.D. 1 0.899 0.979 89.90 97.90 8.52
Tebuconazole N.D. 1 0.881 0.881 88.10 88.10 0.00
Thiacloprid N.D. 1 0.963 0.975 96.30 97.50 1.24
Thiamethoxam N.D. 1 0.955 0.962 95.50 96.20 0.73
Trifloxystrobin N.D. 1 0.782 0.805 78.20 80.50 2.90

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Microbiology Analysis
Testing Accreditation #: 77802 Test Certificate #: 121735-001
Client Name, Sample Details

Michael Biggs
Taylor, MI 48180
Sample: Wedding Mints
Type: Flower
Test Conditions

Scale: PB303-S
Temp: 23.1 °C
Baro Pressure: 978 hPa
Analyst: BCN(Plating)/ACR(PCR)
Technician: BCN
Sample ID#: 121735

Harvest/Process Date: 02/13/2020
Serving Size (g): 1
Date Received: 02/13/2020
Test Date: 02/15/2020
Valid Through: 02/14/2021
Report Issued: 02/18/2020
Sample #121735
Test Method MCFU (CFU/g) LOD (CFU/g) Status (CFU/g)
Total Aerobic Not Tested N/A 0 Not Tested
Yeast & Mold FE-37 (Plating enumeration) 10,001 1,000 Pass/<LOD
Bile-tolerant gram-negative bacteria Not Tested N/A 0 Not Tested
Total Coliforms FE-37 (Plating enumeration) 1,001 100 Pass/<LOD
E. Coli FE-62 (PCR) 1 10 Pass/Not Present
Salmonella FE-62 (PCR) 1 10 Pass/Not Present
Aspergillus spp. FE-62 (PCR) 1 10 Pass/Not Present

E. coli test screens exclusively for Shiga toxin-producing E. coli. TNTC values for yeast and mold are >150,000 CFU/g. TNTC values for total coliforms are >15,000 CFU/g.

TNTC = Too Numerous To Count. Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Bio Analysis by
Microscopic Visual Inspection
Testing Accreditation #: 77802 Test Certificate #: 121735-001
Client Name, Sample Details

Michael Biggs
Taylor, MI 48180
Sample: Wedding Mints
Type: Flower
Method: FE02 Microscope Dissection
Test Conditions

Analyst: ARH
Technician: ARH
Sample ID#: 121735

Harvest/Process Date: 02/13/2020
Serving Size (g): 1
Date Received: 02/13/2020
Test Date: 02/14/2020
Valid Through: 02/13/2021
Report Issued: 02/14/2020
Sample #121735
Sample #121735 Sample #121735
Severity Rating
Mold and Mildew 0 Pass
Mites (not Russet) 0 Pass
Russet Mites 0 Pass
Thrips 0 Pass
Aphids 0 Pass
Other Pests 0 Pass
Other Organic Matter 0 Pass
Inorganic Matter 0 Pass
Total Organic Foreign Matter <2% Pass
Inorganic Foreign Matter 0% Pass
Stem Material <5% Pass
Severity Rating Key
Correlating %FM ≤2% FM >2% FM
Severity Rating 0 None 1 Mild 2 Moderate 3 Severe Units
Mold and Mildew <2 2 3 4+ Locations/g
Mites (not russet) <1 1-5 6-10 11+ Amount/g
Russet Mites <1 1-10 11-50 51+ Amount/g
Thrips <1 1-3 4-5 6+ Amount/g
Aphids <1 1 2-4 5+ Amount/g
Other Pests <1 1-5 6-10 11+ Amount/g
Other Organic Matter <1 1-5 6-10 11+ Amount/g
Inorganic Matter 0 — — >0 Amount/g

In compliance with the MMFLA regulation, the action limits for foreign matter are as follows; no more that 2% organic matter, 5% stem material, and no presence of inorganic matter. Percent foreign contamination is based off of total surface area.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Heavy Metals Analysis
Testing Accreditation #: 77802 Test Certificate #: 121735-001
Client Name, Sample Details

Michael Biggs
Taylor, MI 48180
Sample: Wedding Mints
Type: Flower
Method: FE60 ICPMS-MI
Test Conditions

Prepsheet ID#: MIICP200213bMK
Temp: 20.4 °C
Baro PE: 979.9 hPa
Analyst: TAC
Technician: MK
Sample ID#: 121735

Harvest/Process Date: 02/13/2020
Serving Size (g): 1
Date Received: 02/13/2020
Report Issued: 02/17/2020
Sample #121735
Sample #121735 Sample #121735
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Arsenic 0.2 0.1 Pass/<LOD
Copper 0 1.5 Not Tested
Cadmium 0.2 0.1 Pass/<LOD
Chromium 0.6 0.3 Pass/<LOD
Lead 0.5 0.25 Pass/<LOD
Mercury 0.1 0.05 Pass/<LOD
Nickel 0.5 0.25 Pass/<LOD

The testing requirements set by the MRA for copper and nickel will not be effective until July 1, 2020.

MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 6 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 121735-001
Client Name, Sample Details

Michael Biggs
Taylor, MI 48180
Sample: Wedding Mints
Type: Flower
Method: FE60 ICPMS-MI
Test Conditions

Prepsheet ID#: MIICP200213bMK
Temp: 20.4 °C
Baro PE: 979.9 hPa
Analyst: TAC
Technician: MK
Sample ID#: 121735

Harvest/Process Date: 02/13/2020
Serving Size (g): 1
Date Received: 02/13/2020
Report Issued: 02/17/2020
Sample #121735
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD QC Flag
Arsenic N/D 0.160 0.162 101.25 0.158 98.75
Cadmium N/D 0.160 0.223 139.38 0.236 147.50
Chromium N/D 0.480 0.434 90.42 0.402 83.75
Copper N/D 2.400 2.443 101.79 2.772 115.50
Lead N/D 0.400 0.345 86.25 0.349 87.25
Mercury N/D 0.080 0.107 133.75 0.110 137.50
Nickel N/D 0.400 0.434 108.50 0.396 99.00

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 7 of 6