PJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802

Test Certificate #: 121118-001

Client Name, Sample Details
Jacs Edisnacks Warren, MI 48091 Sample: Alien OG Type: Flower Method: FE04U HPLC-UV *Water Activity: 0.48 *Moisture: 9.5%

Test Conditions
Prepsheet ID#: MIP200121a Scale: XS205-MI2 Temp: 21.7 °C Baro Pressure: 996.2 hPa Analyst: KEB Technician: KEB

Sample ID#: 121118
Harvest/Process Date: 01/22/2020 Serving Size (g): 1 Date Received: 01/22/2020 Test Date: 01/21/2020 Valid Through: 01/21/2021 Report Issued: 01/22/2020

Test Compounds	THC	THCA	CBD	CBDA	CBN	CBG*	CBC*	THCV*	CBDV*	Total Cannabinoids*	Total THC	Total CBD	Calc Max Total Cannabinoids*
Amount (%)	0.9	26.4	N/D	2.2	0.2	N/D	N/D	N/D	N/D	29.6	24.0	1.9	26.1
Amount (mg/g)	8.5	263.8	N/D	21.8	1.8	N/D	N/D	N/D	N/D	295.9	239.9	19.1	260.8
Amount per Serving (mg)	8.5	263.8	N\D	21.8	1.8	N\D	N\D	N\D	N\D	295.9	Serving Size~ (g):		1.0
LOQ (mg/g)	0.99	0.99	0.99	0.99	0.99	0.99	0.99	0.99	0.99		%Decarb.	THC	CBD
±%RPD	1.91	1.63	0.43	2.75	0.65	1.86	5.52	1.51	0.60		%Decarb.	3	0%

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 1 of 6

PJLA

ISO/IEC 17025:2005 Accredited

QC Report

Testing Accreditation #: 77802

Test Certificate #: 121118-001

Client Name, Sample Details
Jacs Edisnacks Warren, MI 48091 Sample: Alien OG Type: Flower Method: FE04U HPLC-UV *Water Activity: 0.48 *Moisture: 9.5%

Test Conditions
Prepsheet ID#: MIP200121a Scale: XS205-MI2 Temp: 21.7 °C Baro Pressure: 996.2 hPa Analyst: KEB Technician: KEB

Sample ID#: 121118
Harvest/Process Date: 01/22/2020 Serving Size (g): 1 Date Received: 01/22/2020 Test Date: 01/21/2020 Valid Through: 01/21/2021 Report Issued: 01/22/2020

Target Compound Name	LCS Spike (μg/g)	LCS Amount (μg/g)	Percent Recovery (%) LCS	LCS Duplicate Amount (μg/g)	Percent Recovery (%) LCSD	Relative Percent Difference (%)
Cannabidivarin (CBDV)	6.26716	6.35719	101.44	6.31908	100.83	0.60
Cannabidiolic Acid (CBDA)	5.67822	5.73332	100.97	5.57778	98.23	2.75
Cannabigerol (CBG)	5.95051	6.04489	101.59	5.93376	99.72	1.86
Cannabidiol (CBD)	5.74291	5.80253	101.04	5.77745	100.60	0.43
Δ9-Tetrahydrocannabivarin (THCV)	5.90468	5.96854	101.08	5.87898	99.56	1.51
Cannabinol (CBN)	5.55871	5.71157	102.75	5.67446	102.08	0.65
Δ9-Tetrahydrocannabinol (THC)	5.53589	5.91941	106.93	5.80731	104.90	1.91
Cannabichromene (CBC)	6.84752	6.907	100.87	6.536	95.45	5.52
Tetrahydrocannabinolic acid (THCA)	5.48264	5.59732	102.09	5.68914	103.77	1.63

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 2 of 6

PJLA

ISO/IEC 17025:2005 Accredited

Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 77802

Test Certificate #: 121118-001

Client Name, Sample Details
Jacs Edisnacks Warren, MI 48091 Sample: Alien OG Type: Flower Method: FE-52 (EN 15662 & AOAC 2007.01)

Test Conditions
Prepsheet ID#: MIPS200121a Scale: XS205-MI2 Temp: 20.5 °C Baro PE: 997.4 hPa Analyst: JRT Technician: JRT

Sample ID#: 121118
Harvest/Process Date: 01/22/2020 Serving Size (g): 1 Date Received: 01/22/2020 Test Date: 01/21/2020 Valid Through: 01/21/2021 Report Issued: 01/23/2020

Compound	MRL (µg/g)	LOD (µg/g)	Status (µg/g)	Compound	MRL (µg/g)	LOD (µg/g)	Status (µg/g)
Aldicarb	0.400	0.125	Pass/<LOD	Abamectin****	0.500	0.125	Pass/<LOD
Acephate	0.400	0.125	Pass/<LOD	Acequinocyl	2.000	0.250	Pass/<LOD
Acetamiprid	0.200	0.125	Pass/<LOD	Azoxystrobin	0.200	0.125	Pass/<LOD
Bifenazate	0.200	0.125	Pass/<LOD	Bifenthrin	0.200	0.125	Pass/<LOD
Boscalid	0.400	0.125	Pass/<LOD	Carbaryl	0.200	0.125	Pass/<LOD
Carbofuran	0.200	0.125	Pass/<LOD	Chlorantraniliprole	0.200	0.125	Pass/<LOD
Chlorfenapyr	1.000	0.500	Pass/<LOD	Chlorpyrifos	0.200	0.125	Pass/<LOD
Clofentezine	0.200	0.125	Pass/<LOD	Cyfluthrin**	1.000	0.500	Pass/<LOD
Cypermethrin***	1.000	0.500	Pass/<LOD	Daminozide	1.000	0.500	Pass/<LOD
DDVP (Dichlorvos)	1.000	0.250	Pass/<LOD	Diazinon	0.200	0.125	Pass/<LOD
Dimethoate	0.200	0.125	Pass/<LOD	Ethoprophos	0.200	0.125	Pass/<LOD
Etofenprox	0.400	0.125	Pass/<LOD	Etoxazole	0.200	0.125	Pass/<LOD
Fenoxycarb	0.200	0.125	Pass/<LOD	Fenpyroximate	0.400	0.125	Pass/<LOD
Fipronil	0.400	0.125	Pass/<LOD	Flonicamid	1.000	0.125	Pass/<LOD
Fludioxonil	0.400	0.125	Pass/<LOD	Hexythiazox	1.000	0.125	Pass/<LOD
Imazalil	0.200	0.125	Pass/<LOD	Imidacloprid	0.400	0.125	Pass/<LOD
Kresoxim Methyl	0.400	0.125	Pass/<LOD	Malathion	0.200	0.125	Pass/<LOD
Metalaxyl	0.200	0.125	Pass/<LOD	Methiocarb	0.200	0.125	Pass/<LOD
Methomyl	0.400	0.125	Pass/<LOD	Methyl Parathion	0.200	0.125	Pass/<LOD
MGK-264‡	0.200	0.125	Pass/<LOD	Myclobutanil	0.200	0.125	Pass/<LOD
Naled	0.500	0.125	Pass/<LOD	Oxamyl	1.000	0.125	Pass/<LOD
Paclobutrazol	0.400	0.125	Pass/<LOD	Permethrins†	0.200	0.125	Pass/<LOD
Phosmet	0.200	0.125	Pass/<LOD	Piperonyl Butoxide	10.000	1.900	Pass/<LOD
Prallethrin	0.200	0.125	Pass/<LOD	Propiconazole	0.400	0.125	Pass/<LOD
Propoxur	0.200	0.125	Pass/<LOD	Pyrethrins*	1.000	0.125	Pass/<LOD
Pyridaben	0.200	0.125	Pass/<LOD	Spinosad*****	0.200	0.125	Pass/<LOD
Spiromesifen	0.200	0.125	Pass/<LOD	Spirotetramat	0.200	0.125	Pass/<LOD
Spiroxamine‡	0.400	0.125	Pass/<LOD	Tebuconazole	0.400	0.125	Pass/<LOD
Thiacloprid	0.200	0.125	Pass/<LOD	Thiamethoxam	0.200	0.125	Pass/<LOD
Trifloxystrobin	0.200	0.125	Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 2 of 6

PJLA

ISO/IEC 17025:2005 Accredited

Pesticide QC Report

Testing Accreditation #: 77802

Test Certificate #: 121118-001

Client Name, Sample Details
Jacs Edisnacks Warren, MI 48091 Sample: Alien OG Type: Flower Method: FE-52 (EN 15662 & AOAC 2007.01)

Test Conditions
Prepsheet ID#: MIPS200121a Scale: XS205-MI2 Temp: 20.5 °C Baro PE: 997.4 hPa Analyst: JRT Technician: JRT

Sample ID#: 121118
Harvest/Process Date: 01/22/2020 Serving Size (g): 1 Date Received: 01/22/2020 Test Date: 01/21/2020 Valid Through: 01/21/2021 Report Issued: 01/23/2020

Target Compound Name	Method Blank (μg/g)	QC Spike (μg/g)	Matrix Spike (μg/g)	Matrix Spike Duplicate (μg/g)	MS recovery%	MSD recovery%	Relative Percent Difference (%)	QC Flag
Acephate	N.D.	1	1.13	1.15	113.00	115.00	1.75
Acequinocyl	N.D.	1	0.783	0.826	78.30	82.60	5.34
Acetamiprid	N.D.	1	1.01	1.04	101.00	104.00	2.93
Aldicarb	N.D.	1	1.11	1.17	111.00	117.00	5.26
Avermectin B1a	N.D.	0.97	1.39	1.36	143.30	140.21	2.18	HR
Azoxystrobin	N.D.	1	0.947	0.988	94.70	98.80	4.24
Bifenazate	N.D.	1	0.932	0.917	93.20	91.70	1.62
Bifenthrin	N.D.	1	1.05	1.1	105.00	110.00	4.65
Boscalid	N.D.	1	0.921	1.04	92.10	104.00	12.14
Carbaryl	N.D.	1	1.1	1.15	110.00	115.00	4.44
Carbofuran	N.D.	1	1.1	1.19	110.00	119.00	7.86
Chlorantraniliprole	N.D.	1	1.08	0.911	108.00	91.10	16.98
Chlorfenapyr	N.D.	1	0.961	0.984	96.10	98.40	2.37
Chlorpyriphos	N.D.	1	1.14	1.19	114.00	119.00	4.29
Clofentezine	N.D.	1	0.935	0.953	93.50	95.30	1.91
Cyfluthrin	N.D.	1	1.11	1.13	111.00	113.00	1.79
Cypermethrin	N.D.	1	1.18	1.18	118.00	118.00	0.00
Daminoside	N.D.	1	0.908	0.894	90.80	89.40	1.55
Diazanon	N.D.	1	2.51	2.33	251.00	233.00	7.44	HR
Dichlorvos	N.D.	1	1.55	1.44	155.00	144.00	7.36	HR
Dimethoate	N.D.	1	1.05	1.14	105.00	114.00	8.22
Ethoprophos	N.D.	1	0.845	0.93	84.50	93.00	9.58
Etofenprox	N.D.	1	1.2	1.14	120.00	114.00	5.13
Etoxazole	N.D.	1	1.17	1.14	117.00	114.00	2.60
Fenoxycarb	N.D.	1	0.925	0.888	92.50	88.80	4.08
Fenpyroximate	N.D.	1	1.14	1.19	114.00	119.00	4.29
Fipronil	N.D.	1	1.09	1.11	109.00	111.00	1.82
Flonicamid	N.D.	1	1.13	1.15	113.00	115.00	1.75
Fludioxonil	N.D.	1	1.01	1.06	101.00	106.00	4.83
Hexythiazox	N.D.	1	0.929	1.04	92.90	104.00	11.27
Imazalil	N.D.	1	0.942	0.97	94.20	97.00	2.93
Imidacloprid	N.D.	1	1.1	1.09	110.00	109.00	0.91
Kresoxim-methyl	N.D.	1	0.851	0.926	85.10	92.60	8.44
Malathion	N.D.	1	0.931	0.984	93.10	98.40	5.54
Metalaxyl	N.D.	1	1.03	1.12	103.00	112.00	8.37
Methiocarb	N.D.	1	1.02	0.978	102.00	97.80	4.20
Methomyl	N.D.	1	1.09	1.11	109.00	111.00	1.82
MGK-264	N.D.	1	0.913	0.823	91.30	82.30	10.37
Myclobutanil	N.D.	1	1.06	1.13	106.00	113.00	6.39
Naled (dibrom)	N.D.	1	0.606	0.618	60.60	61.80	1.96
Oxamyl	N.D.	1	1.17	1.17	117.00	117.00	0.00
Paclobutrazol	N.D.	1	0.978	0.989	97.80	98.90	1.12
Parathion-methyl	N.D.	1	0.861	0.899	86.10	89.90	4.32
Permethrins	N.D.	1	1.17	1.16	117.00	116.00	0.86
Phosmet	N.D.	1	0.984	1.04	98.40	104.00	5.53
Piperonyl butoxide	N.D.	1	1.2	1.14	120.00	114.00	5.13
Prallethrin	N.D.	1	0.86	0.894	86.00	89.40	3.88
Propiconazole	N.D.	1	0.846	0.898	84.60	89.80	5.96
Propoxur	N.D.	1	1.12	1.19	112.00	119.00	6.06
Pyrethrin	N.D.	0.65	0.711	0.726	109.38	111.69	2.09
Pyridaben	N.D.	1	1.17	1.2	117.00	120.00	2.53
SpinosynA	N.D.	0.84	0.723	0.8	86.07	95.24	10.11
SpinosynD	N.D.	0.16	0.14	0.159	87.50	99.38	12.71
Spiromesifen	N.D.	1	0.683	0.648	68.30	64.80	5.26
Spirotetramat	N.D.	1	1.08	0.856	108.00	85.60	23.14
Spiroxamine	N.D.	1	1.2	1.14	120.00	114.00	5.13
Tebuconazole	N.D.	1	0.884	0.9	88.40	90.00	1.79
Thiacloprid	N.D.	1	1.17	1.11	117.00	111.00	5.26
Thiamethoxam	N.D.	1	1.09	1.05	109.00	105.00	3.74
Trifloxystrobin	N.D.	1	0.974	0.957	97.40	95.70	1.76

N.D. = Not Detected

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 3 of 6

PJLA

ISO/IEC 17025:2005 Accredited

Microbiology Analysis

Testing Accreditation #: 77802

Test Certificate #: 121118-001

Client Name, Sample Details
Jacs Edisnacks Warren, MI 48091 Sample: Alien OG Type: Flower

Test Conditions
Scale: PB303-S Temp: 22.2 °C Baro Pressure: 979.2 hPa Analyst: BCN(Plating)/ACR(PCR) Technician: BCN

Sample ID#: 121118
Harvest/Process Date: 01/22/2020 Serving Size (g): 1 Date Received: 01/22/2020 Test Date: 01/17/2020 Valid Through: 01/16/2021 Report Issued: 01/20/2020

Test	Method	MCFU (CFU/g)	LOD (CFU/g)	Status (CFU/g)
Total Aerobic	Not Tested	N/A	0	Not Tested
Yeast & Mold	FE-37 (Plating enumeration)	10,001	1,000	Pass/<LOD
Bile-tolerant gram-negative bacteria	Not Tested	N/A	0	Not Tested
Total Coliforms	FE-37 (Plating enumeration)	1,001	100	Pass/<LOD
E. Coli	FE-62 (PCR)	1	10	Pass/Not Present
Salmonella	FE-62 (PCR)	1	10	Pass/Not Present
Aspergillus spp.	FE-62 (PCR)	1	10	Pass/Not Present

E. coli test screens exclusively for Shiga toxin-producing E. coli.

TNTC = Too Numerous To Count. Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 4 of 6

PJLA

ISO/IEC 17025:2005 Accredited

Bio Analysis by
Microscopic Visual Inspection

Testing Accreditation #: 77802

Test Certificate #: 121118-001

Client Name, Sample Details
Jacs Edisnacks Warren, MI 48091 Sample: Alien OG Type: Flower Method: FE02 Microscope Dissection

Test Conditions
Analyst: ARH Technician: ARH

Sample ID#: 121118
Harvest/Process Date: 01/22/2020 Serving Size (g): 1 Date Received: 01/22/2020 Test Date: 01/15/2020 Valid Through: 01/14/2021 Report Issued: 01/15/2020

Severity Rating
Mold and Mildew	0	Pass
Mites (not Russet)	0	Pass
Russet Mites	0	Pass
Thrips	0	Pass
Aphids	0	Pass
Other Pests	0	Pass
Other Organic Matter	0	Pass
Inorganic Matter	0	Pass

Total Organic Foreign Matter	<2%	Pass
Inorganic Foreign Matter	0%	Pass
Stem Material	<5%	Pass

Severity Rating Key
Correlating %FM	≤2% FM			>2% FM
Severity Rating	0 None	1 Mild	2 Moderate	3 Severe	Units
Mold and Mildew	<2	2	3	4+	Locations/g
Mites (not russet)	<1	1-5	6-10	11+	Amount/g
Russet Mites	<1	1-10	11-50	51+	Amount/g
Thrips	<1	1-3	4-5	6+	Amount/g
Aphids	<1	1	2-4	5+	Amount/g
Other Pests	<1	1-5	6-10	11+	Amount/g
Other Organic Matter	<1	1-5	6-10	11+	Amount/g
Inorganic Matter	0	—	—	>0	Amount/g

In compliance with the MMFLA regulation, the action limits for foreign matter are as follows; no more that 2% organic matter, 5% stem material, and no presence of inorganic matter. Percent foreign contamination is based off of total surface area.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 5 of 6

PJLA

ISO/IEC 17025:2005 Accredited

Heavy Metals Analysis

Testing Accreditation #: 77802

Test Certificate #: 121118-001

Client Name, Sample Details
Jacs Edisnacks Warren, MI 48091 Sample: Alien OG Type: Flower Method: FE60 ICPMS-MI

Test Conditions
Prepsheet ID#: MIICP200116MK Temp: 17.1 °C Baro PE: 987.6 hPa Analyst: TAC Technician: MK

Sample ID#: 121118
Harvest/Process Date: 01/22/2020 Serving Size (g): 1 Date Received: 01/22/2020 Report Issued: 01/27/2020

Test Compound	MRL (PPM)	LOD (PPM)	Status (PPM)
Arsenic	0.2	0.1	Pass/<LOD
Copper	0	1.5	Not Tested
Cadmium	0.2	0.1	Pass/<LOD
Chromium	0.6	0.3	Pass/<LOD
Lead	0.5	0.25	Pass/<LOD
Mercury	0.1	0.05	Pass/<LOD
Nickel	0.5	0.25	Pass/<LOD

MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 6 of 6

PJLA

ISO/IEC 17025:2005 Accredited

QC Report

Testing Accreditation #: 77802

Test Certificate #: 121118-001

Client Name, Sample Details
Jacs Edisnacks Warren, MI 48091 Sample: Alien OG Type: Flower Method: FE60 ICPMS-MI

Test Conditions
Prepsheet ID#: MIICP200116MK Temp: 17.1 °C Baro PE: 987.6 hPa Analyst: TAC Technician: MK

Sample ID#: 121118
Harvest/Process Date: 01/22/2020 Serving Size (g): 1 Date Received: 01/22/2020 Report Issued: 01/27/2020

Target Compound Name	Method Blank (μg/g)	LCS Spike (μg/g)	LCS Amount (μg/g)	Percent Recovery (%) LCS	LCS Duplicate Amount (μg/g)	Percent Recovery (%) LCSD	QC Flag
Arsenic	-0.001	0.160	0.110	68.75	0.114	71.25	LR
Cadmium	0.000	0.160	0.139	86.88	0.150	93.75
Chromium	0.032	0.480	0.412	85.83	0.486	101.25
Copper	0.314	2.400	1.374	57.25	1.860	77.50	LRQ
Lead	-0.006	0.400	0.228	57.00	0.248	62.00	LR
Mercury	-0.001	0.080	0.064	80.00	0.067	83.75
Nickel	-.017	0.400	0.231	57.75	0.200	50.00	LR

N.D. = Not Detected

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 7 of 6

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis byHigh Performance Liquid Chromatography

Client Name, Sample Details

Test Conditions

Sample ID#: 121118

ISO/IEC 17025:2005 Accredited

QC Report

Client Name, Sample Details

Test Conditions

Sample ID#: 121118

ISO/IEC 17025:2005 Accredited

Pesticide Analysis byMass Spectrometer

Client Name, Sample Details

Test Conditions

Sample ID#: 121118

ISO/IEC 17025:2005 Accredited

Pesticide QC Report

Client Name, Sample Details

Test Conditions

Sample ID#: 121118

ISO/IEC 17025:2005 Accredited

Microbiology Analysis

Client Name, Sample Details

Test Conditions

Sample ID#: 121118

ISO/IEC 17025:2005 Accredited

Bio Analysis byMicroscopic Visual Inspection

Client Name, Sample Details

Test Conditions

Sample ID#: 121118

ISO/IEC 17025:2005 Accredited

Heavy Metals Analysis

Client Name, Sample Details

Test Conditions

Sample ID#: 121118

ISO/IEC 17025:2005 Accredited

QC Report

Client Name, Sample Details

Test Conditions

Sample ID#: 121118

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Pesticide Analysis by
Mass Spectrometer

Bio Analysis by
Microscopic Visual Inspection