ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 119660-001
Client Name, Sample Details

Grateful Greenery
Lowell , OR 97452
Sample: 180726 J-1
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300017AE9000004925
Metrc Source Pkg#: 1A4010300017AE9000001106
***Water Activity: 0.5138
***Moisture: 11.2%
Test Conditions

Prepsheet ID#: ORP191023a
Scale: XS205-OR1
Temp: 23.6 °C
Baro Pressure: 1008 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 119660

Lot #: 180726 J-1
Batch #: 119660
Batch Weight (g): 721.212
Harvest/Process Date: 07/26/2018
Serving Size (g): 1
Date Received: 10/22/2019
Test Date: 10/23/2019
Sample #119660
Sample #119660 Sample #119660
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 3.54 23.00 N/D 1.27 0.16 0.36 0.06 N/D N/D 28.38 23.72 1.11 25.40
Amount (mg/g) 35.42 230.02 N/D 12.65 1.56 3.56 0.61 N/D N/D 283.82 237.15 11.09 253.97
Amount per Serving (mg) 35.42 230.02 N\D 12.65 1.56 3.56 0.61 N\D N\D 283.82 Serving Size~ (g): 1.00
LOQ (mg/g) 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05   %Decarb. THC CBD
±%RPD 0.58 0.27 +/-5% 2.09 15.38 10.53 +/-5% +/-5% +/-5% 13 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 119660-001
Client Name, Sample Details

Grateful Greenery
Lowell , OR 97452
Sample: 180726 J-1
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300017AE9000004925
Metrc Source Pkg#: 1A4010300017AE9000001106
***Water Activity: 0.5138
***Moisture: 11.2%
Test Conditions

Prepsheet ID#: ORP191023a
Scale: XS205-OR1
Temp: 23.6 °C
Baro Pressure: 1008 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 119660

Lot #: 180726 J-1
Batch #: 119660
Batch Weight (g): 721.212
Harvest/Process Date: 07/26/2018
Serving Size (g): 1
Date Received: 10/22/2019
Test Date: 10/23/2019
Sample #119660
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0
Cannabidiolic Acid (CBDA) N.D. 1.29 1.45 112.40 1.42 110.08 2.09
Cannabigerol (CBG) N.D. 0.16 0.2 125.00 0.18 112.50 10.53
Cannabidiol (CBD) N.D. 1 0 0.00 0 0.00 0
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0
Cannabinol (CBN) N.D. 0.1 0.07 70.00 0.06 60.00 15.38
Δ9-Tetrahydrocannabinol (THC) N.D. 3.31 3.43 103.63 3.41 103.02 0.58
Cannabichromene (CBC) N.D. 0.08 0.13 162.50 0.13 162.50 0.00
Tetrahydrocannabinolic acid (THCA) N.D. 18.31 18.75 102.40 18.7 102.13 0.27

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 119660-001
Client Name, Sample Details

Grateful Greenery
Lowell , OR 97452
Sample: 180726 J-1
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300017AE9000004925
Metrc Source Pkg#: 1A4010300017AE9000001106
Test Conditions

Prepsheet ID#: ORPS191024a
Scale: Veritas-OR1
Temp: 22.5 °C
Baro PE: 1007 hPa
Analyst: JER
Technician: JER/TMR
Sample ID#: 119660

Lot #: 180726 J-1
Batch #: 119660
Batch Weight (g): 721.212
Harvest/Process Date: 07/26/2018
Serving Size (g): 1
Date Received: 10/22/2019
Test Date: 10/26/2019
Sample #119660
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.135 Pass/<LOD Abamectin**** 0.500 0.135 Pass/<LOD
Acephate 0.400 0.135 Pass/<LOD Acequinocyl 2.000 0.270 Pass/<LOD
Acetamiprid 0.200 0.135 Pass/<LOD Azoxystrobin 0.200 0.135 Pass/<LOD
Bifenazate 0.200 0.135 Pass/<LOD Bifenthrin 0.200 0.135 Pass/<LOD
Boscalid 0.400 0.135 Pass/<LOD Carbaryl 0.200 0.135 Pass/<LOD
Carbofuran 0.200 0.135 Pass/<LOD Chlorantraniliprole 0.200 0.135 Pass/<LOD
Chlorfenapyr 1.000 0.541 Pass/<LOD Chlorpyrifos 0.200 0.135 Pass/<LOD
Clofentezine 0.200 0.135 Pass/<LOD Cyfluthrin** 1.000 0.541 Pass/<LOD
Cypermethrin*** 1.000 0.541 Pass/<LOD Daminozide 1.000 0.135 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.270 Pass/<LOD Diazinon 0.200 0.135 Pass/<LOD
Dimethoate 0.200 0.135 Pass/<LOD Ethoprophos 0.200 0.135 Pass/<LOD
Etofenprox 0.400 0.135 Pass/<LOD Etoxazole 0.200 0.135 Pass/<LOD
Fenoxycarb 0.200 0.135 Pass/<LOD Fenpyroximate 0.400 0.135 Pass/<LOD
Fipronil 0.400 0.135 Pass/<LOD Flonicamid 1.000 0.135 Pass/<LOD
Fludioxonil 0.400 0.135 Pass/<LOD Hexythiazox 1.000 0.135 Pass/<LOD
Imazalil 0.200 0.135 Pass/<LOD Imidacloprid 0.400 0.135 Pass/<LOD
Kresoxim Methyl 0.400 0.135 Pass/<LOD Malathion 0.200 0.135 Pass/<LOD
Metalaxyl 0.200 0.135 Pass/<LOD Methiocarb 0.200 0.135 Pass/<LOD
Methomyl 0.400 0.135 Pass/<LOD Methyl Parathion 0.200 0.135 Pass/<LOD
MGK-264‡ 0.200 0.135 Pass/<LOD Myclobutanil 0.000 0.135 Pass/<LOD
Naled 0.500 0.135 Pass/<LOD Oxamyl 1.000 0.135 Pass/<LOD
Paclobutrazol 0.400 0.135 Pass/<LOD Permethrins† 0.200 0.135 Pass/<LOD
Phosmet 0.200 0.135 Pass/<LOD Piperonyl Butoxide 2.000 0.135 Pass/<LOD
Prallethrin 0.200 0.135 Pass/<LOD Propiconazole 0.400 0.135 Pass/<LOD
Propoxur 0.200 0.135 Pass/<LOD Pyrethrins* 1.000 0.135 Pass/<LOD
Pyridaben 0.200 0.135 Pass/<LOD Spinosad***** 0.200 0.135 Pass/<LOD
Spiromesifen 0.200 0.135 Pass/<LOD Spirotetramat 0.200 0.135 Pass/<LOD
Spiroxamine‡ 0.400 0.135 Pass/<LOD Tebuconazole 0.400 0.135 Pass/<LOD
Thiacloprid 0.200 0.135 Pass/<LOD Thiamethoxam 0.200 0.135 Pass/<LOD
Trifloxystrobin 0.200 0.135 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 119660-001
Client Name, Sample Details

Grateful Greenery
Lowell , OR 97452
Sample: 180726 J-1
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300017AE9000004925
Metrc Source Pkg#: 1A4010300017AE9000001106
Test Conditions

Prepsheet ID#: ORPS191024a
Scale: Veritas-OR1
Temp: 22.5 °C
Baro PE: 1007 hPa
Analyst: JER
Technician: JER/TMR
Sample ID#: 119660

Lot #: 180726 J-1
Batch #: 119660
Batch Weight (g): 721.212
Harvest/Process Date: 07/26/2018
Serving Size (g): 1
Date Received: 10/22/2019
Test Date: 10/26/2019
Sample #119660
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.19 1.24 119.00 124.00 4.12
Acequinocyl N.D. 1 0.771 0.673 77.10 67.30 13.57 LR
Acetamiprid N.D. 1 1.23 1.26 123.00 126.00 2.41
Aldicarb N.D. 1 1.15 1.17 115.00 117.00 1.72
Avermectin B1a N.D. 0.97 1.2 1.4 123.71 144.33 15.38 HR
Azoxystrobin N.D. 1 1.1 1.17 110.00 117.00 6.17
Bifenazate N.D. 1 0.782 0.853 78.20 85.30 8.69
Bifenthrin N.D. 1 1.12 1.14 112.00 114.00 1.77
Boscalid N.D. 1 1.08 1.04 108.00 104.00 3.77
Carbaryl N.D. 1 1.21 1.22 121.00 122.00 0.82
Carbofuran N.D. 1 1.32 1.4 132.00 140.00 5.88 HR
Chlorantraniliprole N.D. 1 1.03 1.16 103.00 116.00 11.87
Chlorfenapyr N.D. 1 1.05 1.17 105.00 117.00 10.81
Chlorpyriphos N.D. 1 1.08 1.01 108.00 101.00 6.70
Clofentezine N.D. 1 0.947 1.03 94.70 103.00 8.40
Cyfluthrin N.D. 1 1.31 1.31 131.00 131.00 0.00 HR
Cypermethrin N.D. 1 1.29 1.38 129.00 138.00 6.74 HR
Daminoside N.D. 1 0.454 0.491 45.40 49.10 7.83 LR
Diazanon N.D. 1 3.66 3.99 366.00 399.00 8.63 HR
Dichlorvos N.D. 1 1.17 1.32 117.00 132.00 12.05 HR
Dimethoate N.D. 1 1.24 1.27 124.00 127.00 2.39
Ethoprophos N.D. 1 1.11 1.21 111.00 121.00 8.62
Etofenprox N.D. 1 1.15 1.21 115.00 121.00 5.08
Etoxazole N.D. 1 1.23 1.41 123.00 141.00 13.64 HR
Fenoxycarb N.D. 1 1.11 1.11 111.00 111.00 0.00
Fenpyroximate N.D. 1 1.38 1.35 138.00 135.00 2.20 HR
Fipronil N.D. 1 1.22 1.24 122.00 124.00 1.63
Flonicamid N.D. 1 1.28 1.32 128.00 132.00 3.08 HR
Fludioxonil N.D. 1 1.33 1.28 133.00 128.00 3.83 HR
Hexythiazox N.D. 1 1.05 0.844 105.00 84.40 21.75 Q
Imazalil N.D. 1 1.07 1.17 107.00 117.00 8.93
Imidacloprid N.D. 1 1.28 1.4 128.00 140.00 8.96 HR
Kresoxim-methyl N.D. 1 1.1 1.03 110.00 103.00 6.57
Malathion N.D. 1 0.992 1.19 99.20 119.00 18.15
Metalaxyl N.D. 1 1.22 1.25 122.00 125.00 2.43
Methiocarb N.D. 1 1.19 1.18 119.00 118.00 0.84
Methomyl N.D. 1 1.19 1.22 119.00 122.00 2.49
MGK-264 N.D. 1 0.991 0.916 99.10 91.60 7.87
Myclobutanil N.D. 1 1.2 1.26 120.00 126.00 4.88
Naled (dibrom) N.D. 1 0.379 0.384 37.90 38.40 1.31 LR
Oxamyl N.D. 1 1.35 1.43 135.00 143.00 5.76 HR
Paclobutrazol N.D. 1 1.16 1.26 116.00 126.00 8.26
Parathion-methyl N.D. 1 1.2 1.32 120.00 132.00 9.52 HR
Permethrins N.D. 1 1.17 1.19 117.00 119.00 1.69
Phosmet N.D. 1 1.09 1.1 109.00 110.00 0.91
Piperonyl butoxide N.D. 1 1.16 1.24 116.00 124.00 6.67
Prallethrin N.D. 1 1.12 1.13 112.00 113.00 0.89
Propiconazole N.D. 1 1.07 1.04 107.00 104.00 2.84
Propoxur N.D. 1 1.16 1.16 116.00 116.00 0.00
Pyrethrin N.D. 0.65 0.683 0.822 105.08 126.46 18.47
Pyridaben N.D. 1 1.19 1.15 119.00 115.00 3.42
SpinosynA N.D. 0.84 0.683 0.626 81.31 74.52 8.71
SpinosynD N.D. 0.16 0.144 0.124 90.00 77.50 14.93
Spiromesifen N.D. 1 0.195 0.198 19.50 19.80 1.53 LR
Spirotetramat N.D. 1 0.83 0.921 83.00 92.10 10.39
Spiroxamine N.D. 1 1.22 1.31 122.00 131.00 7.11 HR
Tebuconazole N.D. 1 1.12 1.13 112.00 113.00 0.89
Thiacloprid N.D. 1 1.28 1.39 128.00 139.00 8.24 HR
Thiamethoxam N.D. 1 1.21 1.3 121.00 130.00 7.17
Trifloxystrobin N.D. 1 1.11 1.22 111.00 122.00 9.44

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 119660-001
Client Name, Sample Details

Grateful Greenery
Lowell , OR 97452
Sample: 180726 J-1
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300017AE9000004925
Metrc Source Pkg#: 1A4010300017AE9000001106

Test Conditions

Scale: XS205-OR1
Temp: 21.7 °C
Baro Pressure: 1005 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 119660

Lot #: 180726 J-1
Batch #: 119660
Batch Weight (g): 721.212
Harvest/Process Date: 07/26/2018
Serving Size (g): 1
Date Received: 10/22/2019

Sample #119660
Sample #119660
  • α-Pinene (0.03%)
  • β-Ocimene (0.13%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.04%)
  • Myrcene (0.05%)
  • α-Terpinolene (0.34%)
  • β-Pinene (0.04%)
  • Linalool (0.00%)
  • ∆3-Carene (0.02%)
  • Fenchone (0.00%)
  • α-Terpinene (0.05%)
  • endo-Fenchol (0.00%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.03%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.24%)
  • α-Humulene (0.09%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.00%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.02%)
  • α-Bisabolol (0.00%)
  • α-Phellandrene (0.14%)
  • α-Terpineol (0.04%)
  • Valenence (0.15%)

Total: 1.410%

Predominant Terpenes

0.34%   α-Terpinolene Fresh wood, sweet, pine, citrus 0.24%   β-Caryophyllene Sweet, woody, spicy, clove
0.15%   Valenence Sweet, citrus, grapefruit, woody, orange 0.14%   α-Phellandrene Citrus, green, black pepper
0.13%   β-Ocimene Citrus, tropical, woody, green 0.09%   α-Humulene Woody, oceanic-watery, spicy clove

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4