ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 119458-001
Client Name, Sample Details

Salt Creek Hemp Co
Collbran, CO 81624
Sample: 2017 Crude Extract Batch 2nd Run
License: 73713 Colorado Dept of Agriculture
Type: AU Tincture
Method: FE04U HPLC-UV
Test Conditions

Scale: XS205-OR1
Temp: 20.8 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 119458

Lot #: Salt Creek 2017 Field Harvest 2nd Run
Batch #: 119458
Harvest/Process Date: 09/19/2019
Date Received: 09/19/2019
Test Date: 10/01/2019
Sample #119458
Sample #119458 Sample #119458
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 2.33 N/D 53.48 0.58 0.09 1.96 2.73 N/D 0.85 62.01 2.33 53.98 61.94
Amount (mg/g) 23.30 N/D 534.75 5.77 0.94 19.61 27.26 N/D 8.47 620.1 23.30 539.81 619.39
Amount per Serving (mg) N\D N\D N\D N\D N\D N\D N\D N\D N\D 0.00 Serving Size~ (g): 0.00
LOQ (mg/g) 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02   %Decarb. THC CBD
±%RPD +/-5% +/-5% +/-5% +/-5% +/-5% +/-5% +/-5% +/-5% +/-5% 100 99

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 5

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 119458-001
Client Name, Sample Details

Salt Creek Hemp Co
Collbran, CO 81624
Sample: 2017 Crude Extract Batch 2nd Run
License: 73713 Colorado Dept of Agriculture
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Scale: XS205-OR1
Temp: 21.5 °C
Baro Pressure: 994.9 hPa
Analyst: JER
Technician: JER
Sample ID#: 119458

Lot #: Salt Creek 2017 Field Harvest 2nd Run
Batch #: 119458
Harvest/Process Date: 09/19/2019
Date Received: 09/19/2019
Test Date: 09/29/2019
Sample #119458
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.135 Pass/<LOD Abamectin**** 0.500 0.135 Pass/<LOD
Acephate 0.400 0.135 Pass/<LOD Acequinocyl 2.000 0.270 Pass/<LOD
Acetamiprid 0.200 0.135 Pass/<LOD Azoxystrobin 0.200 0.135 Pass/<LOD
Bifenazate 0.200 0.135 Pass/<LOD Bifenthrin 0.200 0.135 Pass/<LOD
Boscalid 0.400 0.135 Pass/<LOD Carbaryl 0.200 0.135 Pass/<LOD
Carbofuran 0.200 0.135 Pass/<LOD Chlorantraniliprole 0.200 0.135 Pass/<LOD
Chlorfenapyr 1.000 0.539 Pass/<LOD Chlorpyrifos 0.200 0.135 Pass/<LOD
Clofentezine 0.200 0.135 Pass/<LOD Cyfluthrin** 1.000 0.539 Pass/<LOD
Cypermethrin*** 1.000 0.539 Pass/<LOD Daminozide 1.000 0.135 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.270 Pass/<LOD Diazinon 0.200 0.135 Pass/<LOD
Dimethoate 0.200 0.135 Pass/<LOD Ethoprophos 0.200 0.135 Pass/<LOD
Etofenprox 0.400 0.135 Pass/<LOD Etoxazole 0.200 0.135 Pass/<LOD
Fenoxycarb 0.200 0.135 Pass/<LOD Fenpyroximate 0.400 0.135 Pass/<LOD
Fipronil 0.400 0.135 Pass/<LOD Flonicamid 1.000 0.135 Pass/<LOD
Fludioxonil 0.400 0.135 Pass/<LOD Hexythiazox 1.000 0.135 Pass/<LOD
Imazalil 0.200 0.135 Pass/<LOD Imidacloprid 0.400 0.135 Pass/<LOD
Kresoxim Methyl 0.400 0.135 Pass/<LOD Malathion 0.200 0.135 Pass/<LOD
Metalaxyl 0.200 0.135 Pass/<LOD Methiocarb 0.200 0.135 Pass/<LOD
Methomyl 0.400 0.135 Pass/<LOD Methyl Parathion 0.200 0.135 Pass/<LOD
MGK-264‡ 0.200 0.135 Pass/<LOD Myclobutanil 0.000 0.135 Pass/<LOD
Naled 0.500 0.135 Pass/<LOD Oxamyl 1.000 0.135 Pass/<LOD
Paclobutrazol 0.400 0.135 Pass/<LOD Permethrins† 0.200 0.135 Pass/<LOD
Phosmet 0.200 0.135 Pass/<LOD Piperonyl Butoxide 2.000 0.135 Pass/<LOD
Prallethrin 0.200 0.135 Pass/<LOD Propiconazole 0.400 0.135 Pass/<LOD
Propoxur 0.200 0.135 Pass/<LOD Pyrethrins* 1.000 0.135 Pass/<LOD
Pyridaben 0.200 0.135 Pass/<LOD Spinosad***** 0.200 0.135 Pass/<LOD
Spiromesifen 0.200 0.135 Pass/<LOD Spirotetramat 0.200 0.135 Pass/<LOD
Spiroxamine‡ 0.400 0.135 Pass/<LOD Tebuconazole 0.400 0.135 Pass/<LOD
Thiacloprid 0.200 0.135 Pass/<LOD Thiamethoxam 0.200 0.135 Pass/<LOD
Trifloxystrobin 0.200 0.135 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 5

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 119458-001
Client Name, Sample Details

Salt Creek Hemp Co
Collbran, CO 81624
Sample: 2017 Crude Extract Batch 2nd Run
License: 73713 Colorado Dept of Agriculture
Type: AU Tincture
Method: SOP FE-44-OR3
Test Conditions

Scale: XS205-OR1
Temp: 21.5 °C
Baro Pressure: 994.9 hPa
Analyst: JER
Technician: JER
Sample ID#: 119458

Lot #: Salt Creek 2017 Field Harvest 2nd Run
Batch #: 119458
Harvest/Process Date: 09/19/2019
Date Received: 09/19/2019
Test Date: 09/26/2019
Sample #119458
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 150 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 5
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 119458-001
Client Name, Sample Details

Salt Creek Hemp Co
Collbran, CO 81624
Sample: 2017 Crude Extract Batch 2nd Run
License: 73713 Colorado Dept of Agriculture
Type: AU Tincture
Method: SOP FE-44-OR3

Test Conditions

Scale: XS205-OR1
Temp: 21..5 °C
Baro Pressure: 994.9 hPa
Analyst: JER
Technician: JER

Sample ID#: 119458

Lot #: Salt Creek 2017 Field Harvest 2nd Run
Batch #: 119458
Harvest/Process Date: 09/19/2019
Date Received: 09/19/2019

Sample #119458
Sample #119458
  • α-Pinene (0.00%)
  • β-Ocimene (0.00%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.01%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.01%)
  • Myrcene (0.03%)
  • α-Terpinolene (0.01%)
  • β-Pinene (0.00%)
  • Linalool (0.07%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.01%)
  • endo-Fenchol (0.07%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.03%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (1.06%)
  • α-Humulene (0.43%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.04%)
  • Guaiol (0.17%)
  • Caryophyllene Oxide (0.30%)
  • α-Bisabolol (0.18%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.09%)
  • Valenence (0.13%)

Total: 2.640%

Predominant Terpenes

1.06%   β-Caryophyllene Sweet, woody, spicy, clove 0.43%   α-Humulene Woody, oceanic-watery, spicy clove
0.30%   Caryophyllene Oxide Sweet, fresh, woody, spicy 0.18%   α-Bisabolol Fruity, nutty, coconut
0.17%   Guaiol Mild, guaiacwood, tea, rose 0.13%   Valenence Sweet, citrus, grapefruit, woody, orange

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 5

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Microbiology Analysis
Testing Accreditation #: 4092-002 Test Certificate #: 119458-001
Client Name, Sample Details

Salt Creek Hemp Co
Collbran, CO 81624
Sample: 2017 Crude Extract Batch 2nd Run
License: 73713 Colorado Dept of Agriculture
Type: AU Tincture
Test Conditions

Scale: XS205-OR1
Temp: 21.8 °C
Baro Pressure: 1000 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 119458

Lot #: Salt Creek 2017 Field Harvest 2nd Run
Batch #: 119458
Harvest/Process Date: 09/19/2019
Date Received: 09/19/2019
Test Date: 10/07/2019
Sample #119458
Test Method MCFU (CFU/g) LOD (CFU/g) Status (CFU/g)
Total Aerobic FE-37 100,000.0 100.0 Pass/<LOD
Yeast & Mold FE-37 10,000.0 100.0 Pass/<LOD
Bile-tolerant gram-negative bacteria Not Tested N/A 0.0 Not Tested
Total Coliforms FE-37 1,000.0 100.0 Pass/<LOD
E. Coli FE-37 1,000.0 100.0 Pass/<LOD
Salmonella FE-56 1.0 1.0 Pass/<LOD
Aspergillus spp. Not Tested N/A 0.0 Not Tested

TNTC = Too Numerous To Count. Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 5