ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 119457-001
Client Name, Sample Details

Salt Creek Hemp Co
Collbran, CO 81624
Sample: 2018 Crude Extract Batch 4
License: 73713 Colorado Dept of Agriculture
Type: AU Tincture
Method: FE04U HPLC-UV
Test Conditions

Scale: XS205-OR1
Temp: 20.8 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 119457

Lot #: Salt Creek 2018 Field Harvest Batch 4
Batch #: 119457
Harvest/Process Date: 09/19/2019
Date Received: 09/19/2019
Test Date: 10/01/2019
Sample #119457
Sample #119457 Sample #119457
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 2.90 N/D 66.28 0.58 N/D 2.81 1.58 N/D 0.91 75.05 2.90 66.79 74.98
Amount (mg/g) 29.01 N/D 662.79 5.79 N/D 28.10 15.76 N/D 9.09 750.54 29.01 667.87 749.83
Amount per Serving (mg) N\D N\D N\D N\D N\D N\D N\D N\D N\D 0.00 Serving Size~ (g): 0.00
LOQ (mg/g) 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02   %Decarb. THC CBD
±%RPD +/-5% +/-5% +/-5% +/-5% +/-5% +/-5% +/-5% +/-5% +/-5% 100 99

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 5

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 119457-001
Client Name, Sample Details

Salt Creek Hemp Co
Collbran, CO 81624
Sample: 2018 Crude Extract Batch 4
License: 73713 Colorado Dept of Agriculture
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Scale: XS205-OR1
Temp: 21.5 °C
Baro Pressure: 994.9 hPa
Analyst: JER
Technician: JER
Sample ID#: 119457

Lot #: Salt Creek 2018 Field Harvest Batch 4
Batch #: 119457
Harvest/Process Date: 09/19/2019
Date Received: 09/19/2019
Test Date: 09/29/2019
Sample #119457
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.133 Pass/<LOD Abamectin**** 0.500 0.133 Pass/<LOD
Acephate 0.400 0.133 Pass/<LOD Acequinocyl 2.000 0.265 Pass/<LOD
Acetamiprid 0.200 0.133 Pass/<LOD Azoxystrobin 0.200 0.133 Pass/<LOD
Bifenazate 0.200 0.133 Pass/<LOD Bifenthrin 0.200 0.133 Pass/<LOD
Boscalid 0.400 0.133 Pass/<LOD Carbaryl 0.200 0.133 Pass/<LOD
Carbofuran 0.200 0.133 Pass/<LOD Chlorantraniliprole 0.200 0.133 Pass/<LOD
Chlorfenapyr 1.000 0.531 Pass/<LOD Chlorpyrifos 0.200 0.133 Pass/<LOD
Clofentezine 0.200 0.133 Pass/<LOD Cyfluthrin** 1.000 0.531 Pass/<LOD
Cypermethrin*** 1.000 0.531 Pass/<LOD Daminozide 1.000 0.133 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.265 Pass/<LOD Diazinon 0.200 0.133 Pass/<LOD
Dimethoate 0.200 0.133 Pass/<LOD Ethoprophos 0.200 0.133 Pass/<LOD
Etofenprox 0.400 0.133 Pass/<LOD Etoxazole 0.200 0.133 Pass/<LOD
Fenoxycarb 0.200 0.133 Pass/<LOD Fenpyroximate 0.400 0.133 Pass/<LOD
Fipronil 0.400 0.133 Pass/<LOD Flonicamid 1.000 0.133 Pass/<LOD
Fludioxonil 0.400 0.133 Pass/<LOD Hexythiazox 1.000 0.133 Pass/<LOD
Imazalil 0.200 0.133 Pass/<LOD Imidacloprid 0.400 0.133 Pass/<LOD
Kresoxim Methyl 0.400 0.133 Pass/<LOD Malathion 0.200 0.133 Pass/<LOD
Metalaxyl 0.200 0.133 Pass/<LOD Methiocarb 0.200 0.133 Pass/<LOD
Methomyl 0.400 0.133 Pass/<LOD Methyl Parathion 0.200 0.133 Pass/<LOD
MGK-264‡ 0.200 0.133 Pass/<LOD Myclobutanil 0.000 0.133 Pass/<LOD
Naled 0.500 0.133 Pass/<LOD Oxamyl 1.000 0.133 Pass/<LOD
Paclobutrazol 0.400 0.133 Pass/<LOD Permethrins† 0.200 0.133 Pass/<LOD
Phosmet 0.200 0.133 Pass/<LOD Piperonyl Butoxide 2.000 0.133 Pass/<LOD
Prallethrin 0.200 0.133 Pass/<LOD Propiconazole 0.400 0.133 Pass/<LOD
Propoxur 0.200 0.133 Pass/<LOD Pyrethrins* 1.000 0.133 Pass/<LOD
Pyridaben 0.200 0.133 Pass/<LOD Spinosad***** 0.200 0.133 Pass/<LOD
Spiromesifen 0.200 0.133 Pass/<LOD Spirotetramat 0.200 0.133 Pass/<LOD
Spiroxamine‡ 0.400 0.133 Pass/<LOD Tebuconazole 0.400 0.133 Pass/<LOD
Thiacloprid 0.200 0.133 Pass/<LOD Thiamethoxam 0.200 0.133 Pass/<LOD
Trifloxystrobin 0.200 0.133 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 5

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 119457-001
Client Name, Sample Details

Salt Creek Hemp Co
Collbran, CO 81624
Sample: 2018 Crude Extract Batch 4
License: 73713 Colorado Dept of Agriculture
Type: AU Tincture
Method: SOP FE-44-OR3
Test Conditions

Scale: XS205-OR1
Temp: 21.5 °C
Baro Pressure: 994.9 hPa
Analyst: JER
Technician: JER
Sample ID#: 119457

Lot #: Salt Creek 2018 Field Harvest Batch 4
Batch #: 119457
Harvest/Process Date: 09/19/2019
Date Received: 09/19/2019
Test Date: 09/26/2019
Sample #119457
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 150 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 5
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 119457-001
Client Name, Sample Details

Salt Creek Hemp Co
Collbran, CO 81624
Sample: 2018 Crude Extract Batch 4
License: 73713 Colorado Dept of Agriculture
Type: AU Tincture
Method: SOP FE-44-OR3

Test Conditions

Scale: XS205-OR1
Temp: 21..5 °C
Baro Pressure: 994.9 hPa
Analyst: JER
Technician: JER

Sample ID#: 119457

Lot #: Salt Creek 2018 Field Harvest Batch 4
Batch #: 119457
Harvest/Process Date: 09/19/2019
Date Received: 09/19/2019

Sample #119457
Sample #119457
  • α-Pinene (0.00%)
  • β-Ocimene (0.00%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.01%)
  • α-Terpinolene (0.01%)
  • β-Pinene (0.00%)
  • Linalool (0.03%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.02%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.00%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.65%)
  • α-Humulene (0.29%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.00%)
  • Guaiol (0.11%)
  • Caryophyllene Oxide (0.16%)
  • α-Bisabolol (0.23%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.03%)
  • Valenence (0.17%)

Total: 1.710%

Predominant Terpenes

0.65%   β-Caryophyllene Sweet, woody, spicy, clove 0.29%   α-Humulene Woody, oceanic-watery, spicy clove
0.23%   α-Bisabolol Fruity, nutty, coconut 0.17%   Valenence Sweet, citrus, grapefruit, woody, orange
0.16%   Caryophyllene Oxide Sweet, fresh, woody, spicy 0.11%   Guaiol Mild, guaiacwood, tea, rose

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 5

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Microbiology Analysis
Testing Accreditation #: 4092-002 Test Certificate #: 119457-001
Client Name, Sample Details

Salt Creek Hemp Co
Collbran, CO 81624
Sample: 2018 Crude Extract Batch 4
License: 73713 Colorado Dept of Agriculture
Type: AU Tincture
Test Conditions

Scale: XS205-OR1
Temp: 21.8 °C
Baro Pressure: 1000 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 119457

Lot #: Salt Creek 2018 Field Harvest Batch 4
Batch #: 119457
Harvest/Process Date: 09/19/2019
Date Received: 09/19/2019
Test Date: 10/07/2019
Sample #119457
Test Method MCFU (CFU/g) LOD (CFU/g) Status (CFU/g)
Total Aerobic FE-37 100,000.0 100.0 Pass/<LOD
Yeast & Mold FE-37 10,000.0 100.0 Pass/<LOD
Bile-tolerant gram-negative bacteria Not Tested N/A 0.0 Not Tested
Total Coliforms FE-37 1,000.0 100.0 Pass/<LOD
E. Coli FE-37 1,000.0 100.0 Pass/<LOD
Salmonella FE-56 1.0 1.0 Pass/<LOD
Aspergillus spp. Not Tested N/A 0.0 Not Tested

TNTC = Too Numerous To Count. Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 5