ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-002 Test Certificate #: 119399-001
Client Name, Sample Details

brandon pettigrew
veneta, OR 97487
Sample: RSO #1
Type: Extract
Method: FE04U HPLC-UV

Test Conditions

Scale: XS205-OR1
Temp: 21.4 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: EDT

Sample ID#: 119399

Batch #: 119399
Harvest/Process Date: 09/12/2019
Date Received: 09/12/2019
Test Date: 09/23/2019

Sample #119399
Sample #119399 Sample #119399
Test
Compounds
THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 4.90 N/D 63.29 N/D 0.44 1.22 2.41 N/D 0.98 73.25 4.90 63.29 73.25
Amount (mg/g) 49.04 N/D 632.93 N/D 4.43 12.21 24.07 N/D 9.84 732.52 49.04 632.93 732.52
Amount per Serving (mg) N\D N\D N\D N\D N\D N\D N\D N\D N\D 0.00 Serving Size~ (g): 0.00
LOQ (mg/g) 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02   %Decarb. THC CBD
±%RPD +/-5% +/-5% +/-5% +/-5% +/-5% +/-5% +/-5% +/-5% +/-5% 100 100

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Residual Solvents Analysis by
Mass Spectrometer

Test Certificate #: 119399-001
Client Name, Sample Details

brandon pettigrew
veneta, OR 97487
Sample: RSO #1
Type: Extract
Method: SOP FE-44-OR3

Test Conditions

Scale: XS205-OR1
Temp: 21.7 °C
Baro Pressure: 995.3 hPa
Analyst: JER
Technician: JER

Sample ID#: 119399

Batch #: 119399
Harvest/Process Date: 09/12/2019
Date Received: 09/12/2019
Test Date: 09/17/2019

Sample #119399
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/102 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 150 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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