IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 118587-001
Client Name, Sample Details

Duraid Gatie
Troy, MI 48085
Sample: Candy Pie
Type: Concentrate
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190731b
Scale: XS205-MI2
Temp: 22.9 °C
Baro Pressure: 984.5 hPa
Analyst: KEB
Technician: KEB
Sample ID#: 118587

Harvest/Process Date: 08/05/2019
Serving Size (g): 1
Date Received: 08/05/2019
Test Date: 07/31/2019
Valid Through: 07/31/2020
Report Issued: 08/05/2019
Sample #118587
Sample #118587 Sample #118587
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 2.8 80.5 N/D 2.6 N/D 0.4 0.4 N/D N/D 86.7 73.4 2.3 76.5
Amount (mg/g) 27.9 805.0 N/D 25.9 N/D 4.3 3.9 N/D N/D 867 733.9 22.7 764.8
Amount per Serving (mg) 27.9 805.0 N\D 25.9 N\D 4.3 3.9 N\D N\D 867.0 Serving Size~ (g): 1.0
LOQ (mg/g) 3.24 3.24 3.24 3.24 3.24 3.24 3.24 3.24 3.24   %Decarb. THC CBD
±%RPD 0.46 0.45 0.41 0.48 0.40 0.28 0.93 0.96 0.06 3 0%

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 3

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 118587-001
Client Name, Sample Details

Duraid Gatie
Troy, MI 48085
Sample: Candy Pie
Type: Concentrate
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190731b
Scale: XS205-MI2
Temp: 22.9 °C
Baro Pressure: 984.5 hPa
Analyst: KEB
Technician: KEB
Sample ID#: 118587

Harvest/Process Date: 08/05/2019
Serving Size (g): 1
Date Received: 08/05/2019
Test Date: 07/31/2019
Valid Through: 07/31/2020
Report Issued: 08/05/2019
Sample #118587
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 5.48684 5.56651 101.45 5.5698 101.51 0.06
Cannabidiolic Acid (CBDA) 0 5.44856 5.52163 101.34 5.54796 101.82 0.48
Cannabigerol (CBG) 0 5.45635 5.57752 102.22 5.56182 101.93 0.28
Cannabidiol (CBD) 0 4.77421 4.87642 102.14 4.85643 101.72 0.41
Δ9-Tetrahydrocannabivarin (THCV) 0 5.61762 5.71498 101.73 5.77038 102.72 0.96
Cannabinol (CBN) 0 5.26013 5.34569 101.63 5.36721 102.04 0.40
Δ9-Tetrahydrocannabinol (THC) 0 5.71097 5.71793 100.12 5.74416 100.58 0.46
Cannabichromene (CBC) 0 5.55402 5.73128 103.19 5.67823 102.24 0.93
Tetrahydrocannabinolic acid (THCA) 0 5.33427 5.39652 101.17 5.42082 101.62 0.45

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 3
IRON Laboratories

Residual Solvents Analysis by
Mass Spectrometer
Test Certificate #: 118587-001
Client Name, Sample Details

Duraid Gatie
Troy, MI 48085
Sample: Candy Pie
Type: Concentrate
Method: SOP FE-44-OR3
Test Conditions

Prepsheet ID#: MIHS190801b
Scale: XS205-MI2
Temp: 23.8 °C
Baro PE: 977.4 hPa
Analyst: JRT
Technician: MEH
Sample ID#: 118587

Harvest/Process Date: 08/05/2019
Serving Size (g): 1
Date Received: 08/05/2019
Test Date: 08/01/2019
Valid Through: 07/31/2020
Report Issued: 08/05/2019
Sample #118587
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 5,000 200 Pass/<LOD
1,4-dioxane 5,000 200 Pass/<LOD 1-Butanol 5,000 200 Pass/<LOD
1-Pentanol 5,000 200 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 750 50 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 50 50 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 50 50 Pass/<LOD 2-Butanol 5,000 200 Pass/<LOD
2-Butanone (MEK) 5,000 200 Pass/<LOD 2-Ethoxyethanol 5,000 200 Pass/<LOD
2-Methylbutane (Isopentane) 750 50 Pass/<LOD 2-Methylpentane (Hexanes) 50 50 Pass/<LOD
2-Methylpropane (Isobutane) 800 50 Pass/<LOD 2-propanol (Isopropyl Alcohol) 500 50 Pass/<LOD
2-Propanone (Acetone) 750 50 Pass/149 3-Methylpentane (Hexanes) 50 50 Pass/<LOD
Acetonitrile 60 50 Pass/<LOD Benzene 1 1 Pass/<LOD
Butane 800 50 Failed/1,299 Chloroform 2 2 Pass/<LOD
Cumene 5,000 1,000 Pass/<LOD Cyclohexane 50 50 Pass/<LOD
Dichloromethane 125 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 1,000 500 Pass/<LOD Ethyl acetate 400 50 Pass/<LOD
Ethyl ether 500 100 Pass/<LOD Ethylene glycol 5,000 500 Pass/<LOD
Ethylene oxide 5 5 Pass/<LOD Heptane 500 50 Pass/<LOD
Hexane 50 50 Pass/<LOD Isopropyl acetate 5,000 200 Pass/<LOD
Methanol 250 200 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 5,000 500 Pass/<LOD N,N-Dimethylformamide (DMF) 5,000 500 Pass/<LOD
Pentane 750 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 2,100 50 Pass/<LOD Pyridine 5,000 200 Pass/<LOD
Sulfolane 5,000 200 Pass/<LOD Tetrahydrofuran (THF) 5,000 200 Pass/<LOD
Toluene 150 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 150 50 Pass/<LOD

Total Butanes = 1299 ug/g (FAIL); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

Total PPM: 1,448.00
* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 3
IRON Laboratories

Residual Solvents QC Report
Test Certificate #: 118587-001
Client Name, Sample Details

Duraid Gatie
Troy, MI 48085
Sample: Candy Pie
Type: Concentrate
Method: SOP FE-44-OR3
Test Conditions

Prepsheet ID#: MIHS190801b
Scale: XS205-MI2
Temp: 23.8 °C
Baro PE: 977.4 hPa
Analyst: JRT
Technician: MEH
Sample ID#: 118587

Harvest/Process Date: 08/05/2019
Serving Size (g): 1
Date Received: 08/05/2019
Test Date: 08/01/2019
Valid Through: 07/31/2020
Report Issued: 08/05/2019
Sample #118587
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 250 242 234 96.80 93.60 3.36
n-Propane N.D. 250 155 138 62.00 55.20 11.60 LR
Isobutane N.D. 250 177 161 70.80 64.40 9.47 LR
Methanol N.D. 250 202 196 80.80 78.40 3.02
n-Butane N.D. 250 188 169 75.20 67.60 10.64 LR
2,2-Dimethylpropane N.D. 250 203 188 81.20 75.20 7.67
Ethanol N.D. 250 212 211 84.80 84.40 0.47
Isopentane N.D. 250 214 198 85.60 79.20 7.77
Acetonitrile N.D. 250 222 220 88.80 88.00 0.90
Diethyl ether N.D. 250 233 219 93.20 87.60 6.19
2-propanone N.D. 250 239 230 95.60 92.00 3.84
2-propanol N.D. 250 227 222 90.80 88.80 2.23
n-Pentane N.D. 250 201 188 80.40 75.20 6.68
2,2-Dimethylbutane N.D. 250 228 210 91.20 84.00 8.22
2,3-Dimethylbutane N.D. 250 226 214 90.40 85.60 5.45
Methylene chloride N.D. 250 224 217 89.60 86.80 3.17
2-Methylpentane N.D. 250 234 214 93.60 85.60 8.93
3-Methylpentane N.D. 250 232 217 92.80 86.80 6.68
2-Butanol N.D. 0 0 0 0.00 0.00 0.00
n-Hexane N.D. 250 228 217 91.20 86.80 4.94
Ethyl acetate N.D. 250 225 217 90.00 86.80 3.62
Tetrahydrofuran N.D. 0 0 0 0.00 0.00 0.00
Trichloroethylene N.D. 25 26 23 104.00 92.00 12.24
Isopropyl acetate N.D. 0 0 0 0.00 0.00 0.00
Benzene N.D. 25 25 24 100.00 96.00 4.08
Chloroform N.D. 25 20 20 80.00 80.00 0.00
Cyclohexane N.D. 0 0 0 0.00 0.00 0.00
Ethylene glycol N.D. 0 0 0 0.00 0.00 0.00
Heptane N.D. 250 247 235 98.80 94.00 4.98
2-Ethoxyethanol N.D. 0 0 0 0.00 0.00 0.00
1,4-Dioxane N.D. 0 0 0 0.00 0.00 0.00
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 260 245 104.00 98.00 5.94
Chlorobenzene N.D. 250 242 234 96.80 93.60 3.36
Ethylbenzene N.D. 0 0 0 0.00 0.00 0.00
m-Xylene/p-Xylene N.D. 125 134 125 107.20 100.00 6.95
o-Xylene N.D. 125 134 129 107.20 103.20 3.80
Cumene N.D. 0 0 0 0.00 0.00 0.00
Ethylene oxide N.D. 0 0 0 0.00 0.00 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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