IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 118524-001
Client Name, Sample Details

James Gavriles
Novi, MI 48377
Sample: GMO Cookies
Type: Flower
Method: FE04U

Test Conditions

Prepsheet ID#: MIP190729a
Scale: XS205-MI2
Temp: 23.2 °C
Baro PE: 976.6 hPa
Analyst: KEB
Technician: KEB

Sample ID#: 118524

Harvest/Process Date: 07/30/2019
Serving Size (g): 1
Date Received: 07/30/2019
Test Date: 07/29/2019
Valid Through: 07/29/2020

Sample #118524
Sample #118524 Sample #118524
Test
Compounds
THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 1.2 30.8 N/D 0.9 0.1 N/D N/D N/D N/D 33.0 28.2 0.8 29.1
Amount (mg/g) 11.8 308.3 N/D 9.2 1.0 N/D N/D N/D N/D 330.3 282.2 8.1 291.3
Amount per Serving (mg) 11.8 308.3 N\D 9.2 1.0 N\D N\D N\D N\D 330.3 Serving Size~ (g): 1.0
LOQ (mg/g) 0.97 0.97 0.97 0.97 0.97 0.97 0.97 0.97 0.97   %Decarb. THC CBD
±%RPD 0.3 1.8 1.3 0.5 0.3 0.7 1.2 0.8 0.3 4 0%

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refers to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 118524-001
Client Name, Sample Details

James Gavriles
Novi, MI 48377
Sample: GMO Cookies
Type: Flower
Method: FE04U

Test Conditions

Prepsheet ID#: MIP190729a
Scale: XS205-MI2
Temp: 23.2 °C
Baro PE: 976.6 hPa
Analyst: KEB
Technician: KEB

Sample ID#: 118524

Harvest/Process Date: 07/30/2019
Serving Size (g): 1
Date Received: 07/30/2019
Test Date: 07/29/2019
Valid Through: 07/29/2020

Sample #118524
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 5.314221883 5.505333588 103.60 5.5191093 103.86 0.25%
Cannabidiolic Acid (CBDA) 0 5.600574119 5.721929497 102.17 5.747770243 102.63 0.45%
Cannabigerol (CBG) 0 5.574494735 5.78087464 103.70 5.742965727 103.02 0.66%
Cannabidiol (CBD) 0 4.947837354 5.210064484 105.30 5.141199976 103.91 1.33%
Δ9-Tetrahydrocannabivarin (THCV) 0 5.456339212 5.736326201 105.13 5.693397089 104.34 0.75%
Cannabinol (CBN) 0 5.150866121 5.383526894 104.52 5.401585633 104.87 0.33%
Δ9-Tetrahydrocannabinol (THC) 0 5.445237574 5.683146025 104.37 5.66877153 104.11 0.25%
Cannabichromene (CBC) 0 6.357126617 6.623391557 104.19 6.546723673 102.98 1.16%
Tetrahydrocannabinolic acid (THCA) 0 5.076022616 5.268810163 103.80 5.365878462 105.71 1.83%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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