IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Michigan Compliant Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 118409-001
Client Name, Sample Details

Bigfoot Wellness
Burton, MI 48509
Sample: Rogue
Type: Flower
Method: FE04U
Metrc Test Pkg#: 1A4050100001D4E000000032
Metrc Source Pkg#: 1A4050100001D4E000000020
***Water Activity: 0.55
***Moisture: 12.36%

Test Conditions

Prepsheet ID#: MIP190724b
Scale: XS205-MI2
Temp: 22.7 °C
Baro PE: 984.2 hPa
Analyst: KEB
Technician: KEB

Sample ID#: 118409

Harvest/Process Date: 07/23/2019
Serving Size (g): 1
Date Received: 07/23/2019
Test Date: 07/24/2019
Valid Through: 07/24/2020

Sample #118409
Sample #118409 Sample #118409
Test
Compounds
THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.9 20.9 N/D 0.7 N/D 0.1 N/D N/D N/D 22.5 19.1 0.6 19.8
Amount (mg/g) 8.6 208.5 N/D 6.6 N/D 1.2 N/D N/D N/D 224.9 191.4 5.8 198.4
Amount per Serving (mg) 8.6 208.5 N\D 6.6 N\D 1.2 N\D N\D N\D 224.9 Serving Size~ (g): 1.0
LOQ (mg/g) 0.96 0.96 0.96 0.96 0.96 0.96 0.96 0.96 0.96   %Decarb. THC CBD
±%RPD 1.3 2.4 3.0 1.4 0.0 3.2 0.8 2.4 0.9 4 0%

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refers to the percentage of THC or CBD relative to THCA or CBDA, respectively.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 7

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Michigan Compliant QC Report

Testing Accreditation #: 77802 Test Certificate #: 118409-001
Client Name, Sample Details

Bigfoot Wellness
Burton, MI 48509
Sample: Rogue
Type: Flower
Method: FE04U
Metrc Test Pkg#: 1A4050100001D4E000000032
Metrc Source Pkg#: 1A4050100001D4E000000020
***Water Activity: 0.55
***Moisture: 12.36%

Test Conditions

Prepsheet ID#: MIP190724b
Scale: XS205-MI2
Temp: 22.7 °C
Baro PE: 984.2 hPa
Analyst: KEB
Technician: KEB

Sample ID#: 118409

Harvest/Process Date: 07/23/2019
Serving Size (g): 1
Date Received: 07/23/2019
Test Date: 07/24/2019
Valid Through: 07/24/2020

Sample #118409
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 5.741015809 5.563326626 96.90 5.514600645 96.06 0.88%
Cannabidiolic Acid (CBDA) 0 5.965856772 5.710228147 95.72 5.793232961 97.11 1.44%
Cannabigerol (CBG) 0 5.966349406 5.742755467 96.25 5.931527939 99.42 3.23%
Cannabidiol (CBD) 0 5.273500411 5.109891912 96.90 5.264938796 99.84 2.99%
Δ9-Tetrahydrocannabivarin (THCV) 0 5.645793973 5.378392858 95.26 5.510440315 97.60 2.43%
Cannabinol (CBN) 0 5.768896526 5.584924365 96.81 5.583041402 96.78 0.03%
Δ9-Tetrahydrocannabinol (THC) 0 6.525987563 5.962098347 91.36 5.883263874 90.15 1.33%
Cannabichromene (CBC) 0 7.53890173 6.95777377 92.29 6.900156329 91.53 0.83%
Tetrahydrocannabinolic acid (THCA) 0 6.344229869 5.226560181 82.38 5.353178831 84.38 2.39%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 7

IRON Laboratories

Michigan Compliant Pesticide Analysis by
Mass Spectrometer

Test Certificate #: 118409-001
Client Name, Sample Details

Bigfoot Wellness
Burton, MI 48509
Sample: Rogue
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4050100001D4E000000032
Metrc Source Pkg#: 1A4050100001D4E000000020

Test Conditions

Prepsheet ID#: MIPS190725b
Scale: XS205-MI1
Temp: 23.7 °C
Baro PE: 987.0 hPa
Analyst: MEH
Technician: JRT

Sample ID#: 118409

Harvest/Process Date: 07/23/2019
Serving Size (g): 1
Date Received: 07/23/2019
Test Date: 07/25/2019
Valid Through: 07/25/2020

Sample #118409
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.125 Pass/<LOD Abamectin**** 0.500 0.125 Pass/<LOD
Acephate 0.400 0.125 Pass/<LOD Acequinocyl 2.000 0.250 Pass/<LOD
Acetamiprid 0.200 0.125 Pass/<LOD Azoxystrobin 0.200 0.125 Pass/<LOD
Bifenazate 0.200 0.125 Pass/<LOD Bifenthrin 0.200 0.125 Pass/<LOD
Boscalid 0.400 0.125 Pass/<LOD Carbaryl 0.200 0.125 Pass/<LOD
Carbofuran 0.200 0.125 Pass/<LOD Chlorantraniliprole 0.200 0.125 Pass/<LOD
Chlorfenapyr 1.000 0.499 Pass/<LOD Chlorpyrifos 0.200 0.125 Pass/<LOD
Clofentezine 0.200 0.125 Pass/<LOD Cyfluthrin** 1.000 0.499 Pass/<LOD
Cypermethrin*** 1.000 0.499 Pass/<LOD Daminozide 1.000 0.499 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.250 Pass/<LOD Diazinon 0.200 0.125 Pass/<LOD
Dimethoate 0.200 0.125 Pass/<LOD Ethoprophos 0.200 0.125 Pass/<LOD
Etofenprox 0.400 0.125 Pass/<LOD Etoxazole 0.200 0.125 Pass/<LOD
Fenoxycarb 0.200 0.125 Pass/<LOD Fenpyroximate 0.400 0.125 Pass/<LOD
Fipronil 0.400 0.125 Pass/<LOD Flonicamid 1.000 0.125 Pass/<LOD
Fludioxonil 0.400 0.125 Pass/<LOD Hexythiazox 1.000 0.125 Pass/<LOD
Imazalil 0.200 0.125 Pass/<LOD Imidacloprid 0.400 0.125 Pass/<LOD
Kresoxim Methyl 0.400 0.125 Pass/<LOD Malathion 0.200 0.125 Pass/<LOD
Metalaxyl 0.200 0.125 Pass/<LOD Methiocarb 0.200 0.125 Pass/<LOD
Methomyl 0.400 0.125 Pass/<LOD Methyl Parathion 0.200 0.125 Pass/<LOD
MGK-264‡ 0.200 0.125 Pass/<LOD Myclobutanil 0.200 0.125 Pass/<LOD
Naled 0.500 0.125 Pass/<LOD Oxamyl 1.000 0.125 Pass/<LOD
Paclobutrazol 0.400 0.125 Pass/<LOD Permethrins† 0.200 0.125 Pass/<LOD
Phosmet 0.200 0.125 Pass/<LOD Piperonyl Butoxide 2.000 1.897 Pass/<LOD
Prallethrin 0.200 0.125 Pass/<LOD Propiconazole 0.400 0.125 Pass/<LOD
Propoxur 0.200 0.125 Pass/<LOD Pyrethrins* 1.000 0.125 Pass/<LOD
Pyridaben 0.200 0.125 Pass/<LOD Spinosad***** 0.200 0.125 Pass/<LOD
Spiromesifen 0.200 0.125 Pass/<LOD Spirotetramat 0.200 0.125 Pass/<LOD
Spiroxamine‡ 0.400 0.125 Pass/<LOD Tebuconazole 0.400 0.125 Pass/<LOD
Thiacloprid 0.200 0.125 Pass/<LOD Thiamethoxam 0.200 0.125 Pass/<LOD
Trifloxystrobin 0.200 0.125 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 7

IRON Laboratories

Michigan Compliant Pesticide QC Report

Test Certificate #: 118409-001
Client Name, Sample Details

Bigfoot Wellness
Burton, MI 48509
Sample: Rogue
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4050100001D4E000000032
Metrc Source Pkg#: 1A4050100001D4E000000020

Test Conditions

Prepsheet ID#: MIPS190725b
Scale: XS205-MI1
Temp: 23.7 °C
Baro PE: 987.0 hPa
Analyst: MEH
Technician: JRT

Sample ID#: 118409

Harvest/Process Date: 07/23/2019
Serving Size (g): 1
Date Received: 07/23/2019
Test Date: 07/25/2019
Valid Through: 07/25/2020

Sample #118409
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.02 1.04 102.00 104.00 1.94
Acequinocyl N.D. 1 0.908 0.863 90.80 86.30 5.08
Acetamiprid N.D. 1 0.97 0.977 97.00 97.70 0.72
Aldicarb N.D. 1 0.947 0.908 94.70 90.80 4.20
Avermectin B1a N.D. 0.97 0.955 0.964 98.45 99.38 0.94
Azoxystrobin N.D. 1 0.872 0.919 87.20 91.90 5.25
Bifenazate N.D. 1 1.01 0.985 101.00 98.50 2.51
Bifenthrin N.D. 1 1.01 1.02 101.00 102.00 0.99
Boscalid N.D. 1 0.847 0.943 84.70 94.30 10.73
Carbaryl N.D. 1 0.905 0.902 90.50 90.20 0.33
Carbofuran N.D. 1 0.987 0.993 98.70 99.30 0.61
Chlorantraniliprole N.D. 1 0.912 0.97 91.20 97.00 6.16
Chlorfenapyr N.D. 1 0.815 1.9 81.50 190.00 79.93 HRQ
Chlorpyriphos N.D. 1 1.05 0.981 105.00 98.10 6.79
Clofentezine N.D. 1 0.993 0.993 99.30 99.30 0.00
Cyfluthrin N.D. 1 1.12 1.04 112.00 104.00 7.41
Cypermethrin N.D. 1 1.02 1.04 102.00 104.00 1.94
Daminoside N.D. 1 1.21 1.13 121.00 113.00 6.84
Diazanon N.D. 1 0.999 1.04 99.90 104.00 4.02
Dichlorvos N.D. 1 0.947 0.9 94.70 90.00 5.09
Dimethoate N.D. 1 1.05 0.985 105.00 98.50 6.39
Ethoprophos N.D. 1 0.846 0.878 84.60 87.80 3.71
Etofenprox N.D. 1 0.985 1.03 98.50 103.00 4.47
Etoxazole N.D. 1 1.01 1.01 101.00 101.00 0.00
Fenoxycarb N.D. 1 0.986 1.01 98.60 101.00 2.40
Fenpyroximate N.D. 1 1.01 1.01 101.00 101.00 0.00
Fipronil N.D. 1 1.07 1.09 107.00 109.00 1.85
Flonicamid N.D. 1 1.11 1.12 111.00 112.00 0.90
Fludioxonil N.D. 1 1.1 1.01 110.00 101.00 8.53
Hexythiazox N.D. 1 0.853 0.855 85.30 85.50 0.23
Imazalil N.D. 1 0.961 0.967 96.10 96.70 0.62
Imidacloprid N.D. 1 0.998 0.962 99.80 96.20 3.67
Kresoxim-methyl N.D. 1 0.971 0.971 97.10 97.10 0.00
Malathion N.D. 1 0.954 0.911 95.40 91.10 4.61
Metalaxyl N.D. 1 0.945 0.952 94.50 95.20 0.74
Methiocarb N.D. 1 0.971 0.946 97.10 94.60 2.61
Methomyl N.D. 1 0.975 1.01 97.50 101.00 3.53
MGK-264 N.D. 1 0.916 0.853 91.60 85.30 7.12
Myclobutanil N.D. 1 0.963 0.928 96.30 92.80 3.70
Naled (dibrom) N.D. 1 0.763 0.74 76.30 74.00 3.06
Oxamyl N.D. 1 1.09 1.08 109.00 108.00 0.92
Paclobutrazol N.D. 1 0.934 0.922 93.40 92.20 1.29
Parathion-methyl N.D. 1 1.21 1.04 121.00 104.00 15.11
Permethrins N.D. 1 0.962 1.07 96.20 107.00 10.63
Phosmet N.D. 1 0.893 0.936 89.30 93.60 4.70
Piperonyl butoxide N.D. 1 1.04 1.05 104.00 105.00 0.96
Prallethrin N.D. 1 0.87 0.784 87.00 78.40 10.40
Propiconazole N.D. 1 0.846 0.848 84.60 84.80 0.24
Propoxur N.D. 1 1.01 0.974 101.00 97.40 3.63
Pyrethrin N.D. 0.65 0.605 0.588 93.08 90.46 2.85
Pyridaben N.D. 1 0.957 0.984 95.70 98.40 2.78
SpinosynA N.D. 0.84 0.558 0.737 66.43 87.74 27.64 LRQ
SpinosynD N.D. 0.16 0.13 0.153 81.25 95.63 16.25
Spiromesifen N.D. 1 0.715 0.74 71.50 74.00 3.44
Spirotetramat N.D. 1 0.816 0.909 81.60 90.90 10.78
Spiroxamine N.D. 1 0.961 1.01 96.10 101.00 4.97
Tebuconazole N.D. 1 0.988 0.933 98.80 93.30 5.73
Thiacloprid N.D. 1 0.974 0.965 97.40 96.50 0.93
Thiamethoxam N.D. 1 0.925 0.906 92.50 90.60 2.08
Trifloxystrobin N.D. 1 1.05 1.08 105.00 108.00 2.82

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 7

IRON Laboratories

Michigan Compliant Microbiology Analysis

Test Certificate #: 118409-001
Client Name, Sample Details

Bigfoot Wellness
Burton, MI 48509
Sample: Rogue
Type: Flower
Metrc Test Pkg#: 1A4050100001D4E000000032
Metrc Source Pkg#: 1A4050100001D4E000000020

Test Conditions

Scale: PB303-S
Analyst: ACR
Technician: ARH

Sample ID#: 118409

Harvest/Process Date: 07/23/2019
Serving Size (g): 1
Date Received: 07/23/2019
Test Date: 07/25/2019
Valid Through: 07/24/2020

Sample #118409
Test Method MCFU (CFU/g) LOD (CFU/g) Status (CFU/g)
Total Aerobic FE-62 (quantitative PCR) 100,000 193 Pass/9,000
Yeast & Mold FE-62 (quantitative PCR) 10,000 12 Pass/147
Bile-tolerant gram-negative bacteria FE-62 (quantitative PCR) 1,000 21 Pass/<LOD
Total Coliforms FE-62 (quantitative PCR) 1,000 19 Pass/<LOD
E. Coli FE-62 (PCR) 1 10 Pass/Not Present
Salmonella FE-62 (PCR) 1 10 Pass/Not Present
Aspergillus spp. FE-62 (PCR) 1 10 Pass/Not Present

TNTC = Too Numerous To Count.

Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 7

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Michigan Compliant Bio Analysis by
Microscopic Visual Inspection

Testing Accreditation #: 77802 Test Certificate #: 118409-001
Client Name, Sample Details

Bigfoot Wellness
Burton, MI 48509
Sample: Rogue
Type: Flower
Method: FE02
Metrc Test Pkg#: 1A4050100001D4E000000032
Metrc Source Pkg#: 1A4050100001D4E000000020

Test Conditions

Analyst: ACR
Technician: SEB

Sample ID#: 118409

Harvest/Process Date: 07/23/2019
Serving Size (g): 1
Date Received: 07/23/2019

Sample #118409
Sample #118409 Sample #118409
Impurities: Not Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture -

The gland heads range from small to large in size and are moderately abundant. Slightly more of them are clear than milky with a moderate amount turning amber in color. Some of the trichomes are damaged and degrading. A few of the trichomes are reduced due to stress. Less than 2% foreign matter. Less than 5% stem material.

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 6 of 7

IRON Laboratories

Michigan Compliant Heavy Metals Analysis

Test Certificate #: 118409-001
Client Name, Sample Details

Bigfoot Wellness
Burton, MI 48509
Sample: Rogue
Type: Flower
Method: FE60 ICPMS-MI1
Metrc Test Pkg#: 1A4050100001D4E000000032
Metrc Source Pkg#: 1A4050100001D4E000000020

Test Conditions

Analyst: JER
Technician: TAC

Sample ID#: 118409

Harvest/Process Date: 07/23/2019
Serving Size (g): 1
Date Received: 07/23/2019

Sample #118409
Sample #118409 Sample #118409
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Lead 0.5 0.05 Pass/<LOD
Arsenic 0.2 0.05 Pass/<LOD
Mercury 0.1 0.05 Pass/<LOD
Cadmium 0.2 0.05 Pass/<LOD
Chromium 0.6 0.063 Pass/<LOD

MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 7 of 7