IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Michigan Compliant Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 117709-001
Client Name, Sample Details

Vendco
Warren, MI 48091
Sample: Sour Diesel
Type: Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4050100001D4E000000009
Metrc Source Pkg#: 1A4050100001D4E000000002
***Water Activity: 0.49
***Moisture: 12.07%
Test Conditions

Prepsheet ID#: MIP190702a
Scale: XS205-MI2
Temp: 23.9 °C
Baro Pressure: 976.6 hPa
Analyst: KEB
Technician: KEB
Sample ID#: 117709

Harvest/Process Date: 07/01/2019
Serving Size (g): 1
Date Received: 07/01/2019
Test Date: 07/02/2019
Valid Through: 07/02/2020
Report Issued: 07/03/2019
Sample #117709
Sample #117709 Sample #117709
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 1.0 18.7 N/D 0.6 N/D 0.1 N/D N/D N/D 20.4 17.4 0.5 18.0
Amount (mg/g) 10.3 186.9 N/D 5.8 N/D 1.0 N/D N/D N/D 204 174.2 5.1 180.3
Amount per Serving (mg) 10.3 186.9 N\D 5.8 N\D 1.0 N\D N\D N\D 204.0 Serving Size~ (g): 1.0
LOQ (mg/g) 0.97 0.97 0.97 0.97 0.97 0.97 0.97 0.97 0.97   %Decarb. THC CBD
±%RPD 4.10 1.46 4.06 0.83 3.12 1.67 2.01 2.04 0.33 5 0%

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Michigan Compliant QC Report
Testing Accreditation #: 77802 Test Certificate #: 117709-001
Client Name, Sample Details

Vendco
Warren, MI 48091
Sample: Sour Diesel
Type: Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4050100001D4E000000009
Metrc Source Pkg#: 1A4050100001D4E000000002
***Water Activity: 0.49
***Moisture: 12.07%
Test Conditions

Prepsheet ID#: MIP190702a
Scale: XS205-MI2
Temp: 23.9 °C
Baro Pressure: 976.6 hPa
Analyst: KEB
Technician: KEB
Sample ID#: 117709

Harvest/Process Date: 07/01/2019
Serving Size (g): 1
Date Received: 07/01/2019
Test Date: 07/02/2019
Valid Through: 07/02/2020
Report Issued: 07/03/2019
Sample #117709
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 5.06837 5.38786 106.30 5.40591 106.66 0.33
Cannabidiolic Acid (CBDA) 0 5.17879 5.65126 109.12 5.69834 110.03 0.83
Cannabigerol (CBG) 0 5.48129 5.69463 103.89 5.79063 105.64 1.67
Cannabidiol (CBD) 0 4.82992 5.01775 103.89 5.22574 108.20 4.06
Δ9-Tetrahydrocannabivarin (THCV) 0 4.91764 5.37495 109.30 5.48579 111.55 2.04
Cannabinol (CBN) 0 5.14403 5.38927 104.77 5.56034 108.09 3.12
Δ9-Tetrahydrocannabinol (THC) 0 5.52274 5.74507 104.03 5.51438 99.85 4.10
Cannabichromene (CBC) 0 5.27375 5.38275 102.07 5.27574 100.04 2.01
Tetrahydrocannabinolic acid (THCA) 0 4.91097 5.14386 104.74 5.21935 106.28 1.46

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 6
IRON Laboratories

Michigan Compliant Pesticide Analysis by
Mass Spectrometer
Test Certificate #: 117709-001
Client Name, Sample Details

Vendco
Warren, MI 48091
Sample: Sour Diesel
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4050100001D4E000000009
Metrc Source Pkg#: 1A4050100001D4E000000002
Test Conditions

Prepsheet ID#: MIPS190705b
Scale: XS205-MI1
Temp: 24.0 °C
Baro PE: 979.6 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 117709

Harvest/Process Date: 07/01/2019
Serving Size (g): 1
Date Received: 07/01/2019
Test Date: 07/05/2019
Valid Through: 07/05/2020
Report Issued: 07/08/2019
Sample #117709
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.119 Pass/<LOD Abamectin**** 0.500 0.119 Pass/<LOD
Acephate 0.400 0.119 Pass/<LOD Acequinocyl 2.000 0.239 Pass/<LOD
Acetamiprid 0.200 0.119 Pass/<LOD Azoxystrobin 0.200 0.119 Pass/<LOD
Bifenazate 0.200 0.119 Pass/<LOD Bifenthrin 0.200 0.119 Pass/<LOD
Boscalid 0.400 0.119 Pass/<LOD Carbaryl 0.200 0.119 Pass/<LOD
Carbofuran 0.200 0.119 Pass/<LOD Chlorantraniliprole 0.200 0.119 Pass/<LOD
Chlorfenapyr 1.000 0.478 Pass/<LOD Chlorpyrifos 0.200 0.119 Pass/<LOD
Clofentezine 0.200 0.119 Pass/<LOD Cyfluthrin** 1.000 0.478 Pass/<LOD
Cypermethrin*** 1.000 0.478 Pass/<LOD Daminozide 1.000 0.478 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.239 Pass/<LOD Diazinon 0.200 0.119 Pass/<LOD
Dimethoate 0.200 0.119 Pass/<LOD Ethoprophos 0.200 0.119 Pass/<LOD
Etofenprox 0.400 0.119 Pass/<LOD Etoxazole 0.200 0.119 Pass/<LOD
Fenoxycarb 0.200 0.119 Pass/<LOD Fenpyroximate 0.400 0.119 Pass/<LOD
Fipronil 0.400 0.119 Pass/<LOD Flonicamid 1.000 0.119 Pass/<LOD
Fludioxonil 0.400 0.119 Pass/<LOD Hexythiazox 1.000 0.119 Pass/<LOD
Imazalil 0.200 0.119 Pass/<LOD Imidacloprid 0.400 0.119 Pass/<LOD
Kresoxim Methyl 0.400 0.119 Pass/<LOD Malathion 0.200 0.119 Pass/<LOD
Metalaxyl 0.200 0.119 Pass/<LOD Methiocarb 0.200 0.119 Pass/<LOD
Methomyl 0.400 0.119 Pass/<LOD Methyl Parathion 0.200 0.119 Pass/<LOD
MGK-264‡ 0.200 0.119 Pass/<LOD Myclobutanil 0.200 0.119 Pass/<LOD
Naled 0.500 0.119 Pass/<LOD Oxamyl 1.000 0.119 Pass/<LOD
Paclobutrazol 0.400 0.119 Pass/<LOD Permethrins† 0.200 0.119 Pass/<LOD
Phosmet 0.200 0.119 Pass/<LOD Piperonyl Butoxide 2.000 1.816 Pass/<LOD
Prallethrin 0.200 0.119 Pass/<LOD Propiconazole 0.400 0.119 Pass/<LOD
Propoxur 0.200 0.119 Pass/<LOD Pyrethrins* 1.000 0.119 Pass/<LOD
Pyridaben 0.200 0.119 Pass/<LOD Spinosad***** 0.200 0.119 Pass/<LOD
Spiromesifen 0.200 0.119 Pass/<LOD Spirotetramat 0.200 0.119 Pass/<LOD
Spiroxamine‡ 0.400 0.119 Pass/<LOD Tebuconazole 0.400 0.119 Pass/<LOD
Thiacloprid 0.200 0.119 Pass/<LOD Thiamethoxam 0.200 0.119 Pass/<LOD
Trifloxystrobin 0.200 0.119 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 6
IRON Laboratories

Michigan Compliant Pesticide QC Report
Test Certificate #: 117709-001
Client Name, Sample Details

Vendco
Warren, MI 48091
Sample: Sour Diesel
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4050100001D4E000000009
Metrc Source Pkg#: 1A4050100001D4E000000002
Test Conditions

Prepsheet ID#: MIPS190705b
Scale: XS205-MI1
Temp: 24.0 °C
Baro PE: 979.6 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 117709

Harvest/Process Date: 07/01/2019
Serving Size (g): 1
Date Received: 07/01/2019
Test Date: 07/05/2019
Valid Through: 07/05/2020
Report Issued: 07/08/2019
Sample #117709
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.23 1.2 123.00 120.00 2.47
Acequinocyl N.D. 1 0.744 0.7 74.40 70.00 6.09
Acetamiprid N.D. 1 1.22 1.17 122.00 117.00 4.18
Aldicarb N.D. 1 1.2 1.21 120.00 121.00 0.83
Avermectin B1a N.D. 0.97 1.19 1.19 122.68 122.68 0.00
Azoxystrobin N.D. 1 1.18 1.11 118.00 111.00 6.11
Bifenazate N.D. 1 0.698 0.714 69.80 71.40 2.27 LR
Bifenthrin N.D. 1 1.16 1.23 116.00 123.00 5.86
Boscalid N.D. 1 1.22 1.25 122.00 125.00 2.43
Carbaryl N.D. 1 1.16 1.17 116.00 117.00 0.86
Carbofuran N.D. 1 1.23 1.25 123.00 125.00 1.61
Chlorantraniliprole N.D. 1 1.17 1.18 117.00 118.00 0.85
Chlorfenapyr N.D. 1 0.91 0.999 91.00 99.90 9.32
Chlorpyriphos N.D. 1 1.3 1.29 130.00 129.00 0.77
Clofentezine N.D. 1 0.987 1.25 98.70 125.00 23.51 Q
Cyfluthrin N.D. 1 1.1 1.27 110.00 127.00 14.35
Cypermethrin N.D. 1 1.29 1.24 129.00 124.00 3.95
Daminoside N.D. 1 1.18 1.09 118.00 109.00 7.93
Diazanon N.D. 1 1.2 1.2 120.00 120.00 0.00
Dichlorvos N.D. 1 0.986 0.992 98.60 99.20 0.61
Dimethoate N.D. 1 1.25 1.23 125.00 123.00 1.61
Ethoprophos N.D. 1 1.24 1.15 124.00 115.00 7.53
Etofenprox N.D. 1 1.22 1.24 122.00 124.00 1.63
Etoxazole N.D. 1 1.3 1.26 130.00 126.00 3.13
Fenoxycarb N.D. 1 0.82 1.16 82.00 116.00 34.34 Q
Fenpyroximate N.D. 1 1.26 1.21 126.00 121.00 4.05
Fipronil N.D. 1 1.23 1.15 123.00 115.00 6.72
Flonicamid N.D. 1 1.29 1.3 129.00 130.00 0.77
Fludioxonil N.D. 1 1.19 1.24 119.00 124.00 4.12
Hexythiazox N.D. 1 1.09 1.14 109.00 114.00 4.48
Imazalil N.D. 1 1.11 1.12 111.00 112.00 0.90
Imidacloprid N.D. 1 1.3 1.3 130.00 130.00 0.00
Kresoxim-methyl N.D. 1 1.18 1.24 118.00 124.00 4.96
Malathion N.D. 1 1.08 1.08 108.00 108.00 0.00
Metalaxyl N.D. 1 1.24 1.17 124.00 117.00 5.81
Methiocarb N.D. 1 1.14 1.2 114.00 120.00 5.13
Methomyl N.D. 1 1.25 1.24 125.00 124.00 0.80
MGK-264 N.D. 1 1.02 1.2 102.00 120.00 16.22
Myclobutanil N.D. 1 1.2 1.22 120.00 122.00 1.65
Naled (dibrom) N.D. 1 0.655 0.654 65.50 65.40 0.15 LR
Oxamyl N.D. 1 1.3 1.28 130.00 128.00 1.55
Paclobutrazol N.D. 1 1.17 1.16 117.00 116.00 0.86
Parathion-methyl N.D. 1 1.26 1.19 126.00 119.00 5.71
Permethrins N.D. 1 1.29 1.25 129.00 125.00 3.15
Phosmet N.D. 1 1.01 1.17 101.00 117.00 14.68
Piperonyl butoxide N.D. 1 1.16 1.19 116.00 119.00 2.55
Prallethrin N.D. 1 0.839 0.95 83.90 95.00 12.41
Propiconazole N.D. 1 0.943 0.969 94.30 96.90 2.72
Propoxur N.D. 1 1.16 1.18 116.00 118.00 1.71
Pyrethrin N.D. 0.65 0.596 0.531 91.69 81.69 11.54
Pyridaben N.D. 1 1.27 1.24 127.00 124.00 2.39
SpinosynA N.D. 0.84 0.9 0.725 107.14 86.31 21.54 Q
SpinosynD N.D. 0.16 0.159 0.162 99.38 101.25 1.87
Spiromesifen N.D. 1 0.238 0.249 23.80 24.90 4.52 LR
Spirotetramat N.D. 1 1.06 1 106.00 100.00 5.83
Spiroxamine N.D. 1 1.29 1.24 129.00 124.00 3.95
Tebuconazole N.D. 1 1.1 1.08 110.00 108.00 1.83
Thiacloprid N.D. 1 1.24 1.29 124.00 129.00 3.95
Thiamethoxam N.D. 1 1.14 1.12 114.00 112.00 1.77
Trifloxystrobin N.D. 1 1.22 1.22 122.00 122.00 0.00

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 6
IRON Laboratories

Michigan Compliant Microbiology Analysis
Test Certificate #: 117709-001
Client Name, Sample Details

Vendco
Warren, MI 48091
Sample: Sour Diesel
Type: Flower
Metrc Test Pkg#: 1A4050100001D4E000000009
Metrc Source Pkg#: 1A4050100001D4E000000002
Test Conditions

Scale: PB303-S
Temp: 24.6 °C
Baro Pressure: 980.2 hPa
Analyst: ACR
Technician: ARH
Sample ID#: 117709

Harvest/Process Date: 07/01/2019
Serving Size (g): 1
Date Received: 07/01/2019
Test Date: 07/05/2019
Valid Through: 07/04/2020
Report Issued: 07/08/2019
Sample #117709
Test Method MCFU (CFU/g) LOD (CFU/g) Status (CFU/g)
Total Aerobic FE-62 100,000 193 Pass/<LOD
Yeast & Mold FE-62 10,000 12 Pass/<LOD
Bile-tolerant gram-negative bacteria FE-62 1,000 21 Pass/<LOD
Total Coliforms FE-62 1,000 19 Pass/<LOD
E. Coli FE-62 1 10 Pass/Not Present
Salmonella FE-62 1 10 Pass/Not Present
Aspergillus spp. FE-62 1 10 Pass/Not Present

TNTC = Too Numerous To Count. Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Michigan Compliant Bio Analysis by
Microscopic Visual Inspection
Testing Accreditation #: 77802 Test Certificate #: 117709-001
Client Name, Sample Details

Vendco
Warren, MI 48091
Sample: Sour Diesel
Type: Flower
Method: FE02 Microscope Dissection
Metrc Test Pkg#: 1A4050100001D4E000000009
Metrc Source Pkg#: 1A4050100001D4E000000002
Test Conditions

Analyst: ACR
Technician: SEB
Sample ID#: 117709

Harvest/Process Date: 07/01/2019
Serving Size (g): 1
Date Received: 07/01/2019
Test Date: 07/03/2019
Valid Through: 07/03/2020
Report Issued: 07/03/2019
Sample #117709
Sample #117709 Sample #117709
Impurities: Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture -

The gland heads range from small to large in size and are moderately abundant. Slightly more of them are clear than milky with a moderate amount turning amber in color. Some of the trichomes are damaged and degrading. A few of the trichomes are reduced due to stress. Less than 2% foreign matter. Less than 5% stem material. See microbial analysis for a conclusive analysis.

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 6
IRON Laboratories

Michigan Compliant Heavy Metals Analysis
Test Certificate #: 117709-001
Client Name, Sample Details

Vendco
Warren, MI 48091
Sample: Sour Diesel
Type: Flower
Method: FE60 ICPMS-MI
Metrc Test Pkg#: 1A4050100001D4E000000009
Metrc Source Pkg#: 1A4050100001D4E000000002
Test Conditions

Analyst: JER
Technician: TAC
Sample ID#: 117709

Harvest/Process Date: 07/01/2019
Serving Size (g): 1
Date Received: 07/01/2019
Report Issued: 07/03/2019
Sample #117709
Sample #117709 Sample #117709
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Arsenic 0.2 0.05 Pass/<LOD
Copper Not Tested
Cadmium 0.2 0.05 Pass/0.077
Chromium 0.6 0.063 Pass/0.162
Lead 0.5 0.05 Pass/<LOD
Mercury 0.1 0.05 Pass/<LOD
Nickel Not Tested

MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 6 of 6