IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 117090-001
Client Name, Sample Details

Corey Dascal
Dearborn Heights, MI 48125
Sample: Canna
License: C216190-641459
Type: Tincture
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190524
Scale: XS205-MI2
Temp: 22.8 °C
Baro Pressure: 985.2 hPa
Analyst: KEB
Technician: JRT
Sample ID#: 117090

Harvest/Process Date: 05/28/2019
Serving Size (g): 1
Date Received: 05/28/2019
Test Date: 05/24/2019
Valid Through: 05/24/2020
Report Issued: 05/28/2019
Sample #117090
Sample #117090 Sample #117090
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 3.8 N/D 69.1 0.7 N/D 1.1 3.8 N/D 0.7 79.2 3.8 69.8 79.1
Amount (mg/g) 37.9 N/D 691.4 7.4 N/D 10.5 37.8 N/D 6.6 791.6 37.9 697.9 790.7
Amount per Serving (mg) 37.9 N\D 691.4 7.4 N\D 10.5 37.8 N\D 6.6 791.6 Serving Size~ (g): 1.0
LOQ (mg/g) 3.48 3.48 3.48 3.48 3.48 3.48 3.48 3.48 3.48   %Decarb. THC CBD
±%RPD 2.41 0.73 1.50 0.85 1.66 0.65 1.34 1.60 2.62 100% 99

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 3

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 117090-001
Client Name, Sample Details

Corey Dascal
Dearborn Heights, MI 48125
Sample: Canna
License: C216190-641459
Type: Tincture
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190524
Scale: XS205-MI2
Temp: 22.8 °C
Baro Pressure: 985.2 hPa
Analyst: KEB
Technician: JRT
Sample ID#: 117090

Harvest/Process Date: 05/28/2019
Serving Size (g): 1
Date Received: 05/28/2019
Test Date: 05/24/2019
Valid Through: 05/24/2020
Report Issued: 05/28/2019
Sample #117090
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 4.99729 4.82169 96.49 4.94953 99.04 2.62
Cannabidiolic Acid (CBDA) 0 5.19649 5.07264 97.62 5.11573 98.45 0.85
Cannabigerol (CBG) 0 5.42123 5.36334 98.93 5.3983 99.58 0.65
Cannabidiol (CBD) 0 5.75381 5.75243 99.98 5.83919 101.48 1.50
Δ9-Tetrahydrocannabivarin (THCV) 0 5.44316 5.35152 98.32 5.43774 99.90 1.60
Cannabinol (CBN) 0 5.62142 5.46029 97.13 5.55159 98.76 1.66
Δ9-Tetrahydrocannabinol (THC) 0 5.28695 5.17578 97.90 5.05256 95.57 2.41
Cannabichromene (CBC) 0 5.30067 5.39769 101.83 5.32563 100.47 1.34
Tetrahydrocannabinolic acid (THCA) 0 5.18145 5.09318 98.30 5.05609 97.58 0.73

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 3
IRON Laboratories

Residual Solvents Analysis by
Mass Spectrometer
Test Certificate #: 117090-001
Client Name, Sample Details

Corey Dascal
Dearborn Heights, MI 48125
Sample: Canna
License: C216190-641459
Type: Tincture
Method: SOP FE-44-OR3
Test Conditions

Prepsheet ID#: MIHS190529a
Scale: XS205-MI2
Temp: 23 °C
Baro PE: 969.2 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 117090

Harvest/Process Date: 05/28/2019
Serving Size (g): 1
Date Received: 05/28/2019
Test Date: 05/28/2019
Valid Through: 05/28/2020
Report Issued: 05/29/2019
Sample #117090
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 5,000 200 Pass/<LOD
1,4-dioxane 5,000 200 Pass/<LOD 1-Butanol 5,000 200 Pass/<LOD
1-Pentanol 5,000 200 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 50 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 50 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 50 Pass/<LOD 2-Butanol 5,000 200 Pass/<LOD
2-Butanone (MEK) 5,000 200 Pass/<LOD 2-Ethoxyethanol 5,000 200 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 50 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/61 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 50 Pass/<LOD Benzene 2 2 Pass/<LOD
Butane 5,000 50 Pass/<LOD Chloroform 60 50 Pass/<LOD
Cumene 5,000 1,000 Pass/<LOD Cyclohexane 290 50 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 100 Pass/<LOD Ethylene glycol 5,000 500 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 200 Pass/<LOD
Methanol 3,000 200 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 5,000 500 Pass/<LOD N,N-Dimethylformamide (DMF) 5,000 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 50 Pass/<LOD Pyridine 5,000 200 Pass/<LOD
Sulfolane 5,000 200 Pass/<LOD Tetrahydrofuran (THF) 5,000 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 6 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

Total PPM: 61.00
* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 3
IRON Laboratories

Residual Solvents QC Report
Test Certificate #: 117090-001
Client Name, Sample Details

Corey Dascal
Dearborn Heights, MI 48125
Sample: Canna
License: C216190-641459
Type: Tincture
Method: SOP FE-44-OR3
Test Conditions

Prepsheet ID#: MIHS190529a
Scale: XS205-MI2
Temp: 23 °C
Baro PE: 969.2 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 117090

Harvest/Process Date: 05/28/2019
Serving Size (g): 1
Date Received: 05/28/2019
Test Date: 05/28/2019
Valid Through: 05/28/2020
Report Issued: 05/29/2019
Sample #117090
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 124 124 49.60 49.60 0.00 LR
Isobutane N.D. 250 147 150 58.80 60.00 2.02 LR
Methanol N.D. 250 216 199 86.40 79.60 8.19
n-Butane N.D. 250 155 156 62.00 62.40 0.64 LR
2,2-Dimethylpropane N.D. 250 160 166 64.00 66.40 3.68 LR
Ethanol N.D. 250 216 217 86.40 86.80 0.46
Isopentane N.D. 250 178 184 71.20 73.60 3.31
Acetonitrile N.D. 250 194 197 77.60 78.80 1.53
Diethyl ether N.D. 250 214 209 85.60 83.60 2.36
2-propanone N.D. 250 213 210 85.20 84.00 1.42
2-propanol N.D. 250 215 215 86.00 86.00 0.00
n-Pentane N.D. 250 182 184 72.80 73.60 1.09
2,2-Dimethylbutane N.D. 250 194 198 77.60 79.20 2.04
2,3-Dimethylbutane N.D. 250 0 199 0.00 79.60 200.00 LRQ
Methylene chloride N.D. 250 212 216 84.80 86.40 1.87
2-Methylpentane N.D. 250 197 195 78.80 78.00 1.02
3-Methylpentane N.D. 250 203 202 81.20 80.80 0.49
2-Butanol N.D. 250 219 221 87.60 88.40 0.91
n-Hexane N.D. 250 207 206 82.80 82.40 0.48
Ethyl acetate N.D. 250 218 218 87.20 87.20 0.00
Tetrahydrofuran N.D. 250 210 211 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 219 220 0.00 0.00 0.00
Benzene N.D. 250 220 224 88.00 89.60 1.80
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 212 213 84.80 85.20 0.47
Ethylene glycol N.D. 250 231 486 92.40 194.40 71.13 HRQ
Heptane N.D. 250 227 227 90.80 90.80 0.00
2-Ethoxyethanol N.D. 250 272 264 108.80 105.60 2.99
1,4-Dioxane N.D. 250 233 232 93.20 92.80 0.43
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 231 233 92.40 93.20 0.86
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 236 233 94.40 93.20 1.28
m-Xylene/p-Xylene N.D. 500 454 454 90.80 90.80 0.00
o-Xylene N.D. 250 231 229 92.40 91.60 0.87
Cumene N.D. 250 232 231 92.80 92.40 0.43
Ethylene oxide N.D. 250 221 233 88.40 93.20 5.29

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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