ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 117010-001
Client Name, Sample Details

45th Parallel Farms #2
Dallas, OR 97338
Sample: Rusty Shackleford
License: 100861828BC
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A40103000023F4000001302
Metrc Source Pkg#: 1A40103000023F4000001224
***Water Activity: 0.521
***Moisture: 11.74%
Test Conditions

Prepsheet ID#: ORP190520a
Scale: XS205-OR1
Temp: 21.3 °C
Baro Pressure: 996 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 117010

Lot #: Rusty Shackleford Harvest 10/25/2018
Batch #: 117010
Batch Weight (g): 1537.67
Harvest/Process Date: 10/25/2018
Serving Size (g): 1
Date Received: 05/17/2019
Test Date: 05/20/2019
Sample #117010
Sample #117010 Sample #117010
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 2.34 18.83 N/D 0.79 0.12 0.10 0.06 N/D N/D 22.23 18.85 0.69 19.82
Amount (mg/g) 23.37 188.30 N/D 7.85 1.24 0.97 0.60 N/D N/D 222.33 188.51 6.88 198.20
Amount per Serving (mg) 23.37 188.30 N\D 7.85 1.24 0.97 0.60 N\D N\D 222.33 Serving Size~ (g): 1.00
LOQ (mg/g) 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05   %Decarb. THC CBD
±%RPD 8.06 0.19 +/-5% +/-5% 7.41 7.41 22.22 +/-5% +/-5% 11 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 117010-001
Client Name, Sample Details

45th Parallel Farms #2
Dallas, OR 97338
Sample: Rusty Shackleford
License: 100861828BC
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A40103000023F4000001302
Metrc Source Pkg#: 1A40103000023F4000001224
***Water Activity: 0.521
***Moisture: 11.74%
Test Conditions

Prepsheet ID#: ORP190520a
Scale: XS205-OR1
Temp: 21.3 °C
Baro Pressure: 996 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 117010

Lot #: Rusty Shackleford Harvest 10/25/2018
Batch #: 117010
Batch Weight (g): 1537.67
Harvest/Process Date: 10/25/2018
Serving Size (g): 1
Date Received: 05/17/2019
Test Date: 05/20/2019
Sample #117010
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0
Cannabidiolic Acid (CBDA) N.D. 1.29 1.1 85.27 1.1 85.27 0.00
Cannabigerol (CBG) N.D. 0.15 0.13 86.67 0.14 93.33 7.41
Cannabidiol (CBD) N.D. 1 0 0.00 0 0.00 0
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0
Cannabinol (CBN) N.D. 0.11 0.13 118.18 0.14 127.27 7.41
Δ9-Tetrahydrocannabinol (THC) N.D. 3.31 2.5 75.53 2.71 81.87 8.06
Cannabichromene (CBC) N.D. 0.08 0.04 50.00 0.05 62.50 22.22
Tetrahydrocannabinolic acid (THCA) N.D. 18.31 15.48 84.54 15.45 84.38 0.19

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 117010-001
Client Name, Sample Details

45th Parallel Farms #2
Dallas, OR 97338
Sample: Rusty Shackleford
License: 100861828BC
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A40103000023F4000001302
Metrc Source Pkg#: 1A40103000023F4000001224

Test Conditions

Scale: XS205-OR1
Temp: 19.4 °C
Baro Pressure: 1008 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 117010

Lot #: Rusty Shackleford Harvest 10/25/2018
Batch #: 117010
Batch Weight (g): 1537.67
Harvest/Process Date: 10/25/2018
Serving Size (g): 1
Date Received: 05/17/2019

Sample #117010
Sample #117010
  • α-Pinene (0.07%)
  • β-Ocimene (0.04%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.23%)
  • α-Terpinolene (0.00%)
  • β-Pinene (0.00%)
  • Linalool (0.06%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.04%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.09%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.93%)
  • α-Humulene (0.35%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.00%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.03%)
  • α-Bisabolol (0.00%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.03%)
  • Valenence (0.09%)

Total: 1.960%

Predominant Terpenes

0.93%   β-Caryophyllene Sweet, woody, spicy, clove 0.35%   α-Humulene Woody, oceanic-watery, spicy clove
0.23%   Myrcene Peppery, spicy balsam 0.09%   Valenence Sweet, citrus, grapefruit, woody, orange
0.09%   Limonene Citrus, orange, sweet 0.07%   α-Pinene Fresh camphor, sweet, pine, earthy, woody

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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