IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 116936-001
Client Name, Sample Details

Ananda
Cynthiana, KY 41031
Sample: 19AB110
Type: Topical
Method: FE04U HPLC-UV

Test Conditions

Prepsheet ID#: MIP190514
Scale: XS205-MI2
Temp: 22.3 °C
Baro Pressure: 979.6 hPa
Analyst: KEB
Technician: KEB

Sample ID#: 116936

Harvest/Process Date: 05/14/2019
Serving Size (g): 0.92
Date Received: 05/14/2019
Test Date: 05/14/2019
Valid Through: 05/14/2020
Report Issued: 05/15/2019

Sample #116936
Sample #116936 Sample #116936
Test
Compounds
THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.0 N/D 0.1 N/D N/D N/D N/D N/D N/D 0.1 0.0 0.1 0.1
Amount (mg/g) 0.3 N/D 0.8 N/D N/D N/D N/D N/D N/D 1.1 0.3 0.8 1.2
Amount per Serving (mg) 0.3 N\D 0.7 N\D N\D N\D N\D N\D N\D 1.0 Serving Size~ (g): 0.9
LOQ (mg/g) 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1   %Decarb. THC CBD
±%RPD 3.17 1.49 1.62 1.37 0.99 1.59 1.28 1.58 0.97 100% 100%

Serving size = 1 mL (declared)

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 5

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 116936-001
Client Name, Sample Details

Ananda
Cynthiana, KY 41031
Sample: 19AB110
Type: Topical
Method: FE04U HPLC-UV

Test Conditions

Prepsheet ID#: MIP190514
Scale: XS205-MI2
Temp: 22.3 °C
Baro Pressure: 979.6 hPa
Analyst: KEB
Technician: KEB

Sample ID#: 116936

Harvest/Process Date: 05/14/2019
Serving Size (g): 0.92
Date Received: 05/14/2019
Test Date: 05/14/2019
Valid Through: 05/14/2020
Report Issued: 05/15/2019

Sample #116936
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 5.05384 5.07242 100.37 5.12208 101.35 0.97
Cannabidiolic Acid (CBDA) 0 5.18208 5.27089 101.71 5.19911 100.33 1.37
Cannabigerol (CBG) 0 5.1609 5.24395 101.61 5.16148 100.01 1.59
Cannabidiol (CBD) 0 5.2701 5.44606 103.34 5.35871 101.68 1.62
Δ9-Tetrahydrocannabivarin (THCV) 0 5.10241 5.15866 101.10 5.24086 102.71 1.58
Cannabinol (CBN) 0 4.8176 4.87505 101.19 4.92371 102.20 0.99
Δ9-Tetrahydrocannabinol (THC) 0 5.25439 5.24713 99.86 5.41607 103.08 3.17
Cannabichromene (CBC) 0 4.70656 4.81543 102.31 4.87767 103.64 1.28
Tetrahydrocannabinolic acid (THCA) 0 4.75329 4.83769 101.78 4.91044 103.31 1.49

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 5

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 *Test Certificate #: 116936-002
Client Name, Sample Details

Ananda
Cynthiana, KY 41031
Sample: 19AB110
Type: Topical
Method: FE04U HPLC-UV

Test Conditions

Prepsheet ID#: MIP190521b
Scale: XS205-MI1
Temp: 22.5 °C
Baro Pressure: 985.7 hPa
Analyst: KEB
Technician: KEB

Sample ID#: 116936

Harvest/Process Date: 05/14/2019
Serving Size (g): 0.92
Date Received: 05/14/2019
Test Date: 05/21/2019
Valid Through: 05/21/2020
Report Issued: 05/22/2019

Sample #116936
Sample #116936 Sample #116936
Test
Compounds
THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.0 N/D 0.1 N/D N/D 0.0 N/D N/D N/D 0.2 0.0 0.1 0.2
Amount (mg/g) 0.4 N/D 1.3 N/D N/D 0.1 N/D N/D N/D 1.8 0.4 1.3 1.8
Amount per Serving (mg) 0.4 N\D 1.2 N\D N\D 0.1 N\D N\D N\D 1.7 Serving Size~ (g): 0.9
LOQ (mg/g) 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1   %Decarb. THC CBD
±%RPD 6.16 5.11 5.37 0.37 1.02 1.79 3.85 1.38 0.41 100% 100%

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Test Certificate No. 116936-002 supersedes Test Certificate No. 116936-001

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 5

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report

Testing Accreditation #: 77802 *Test Certificate #: 116936-002
Client Name, Sample Details

Ananda
Cynthiana, KY 41031
Sample: 19AB110
Type: Topical
Method: FE04U HPLC-UV

Test Conditions

Prepsheet ID#: MIP190521b
Scale: XS205-MI1
Temp: 22.5 °C
Baro Pressure: 985.7 hPa
Analyst: KEB
Technician: KEB

Sample ID#: 116936

Harvest/Process Date: 05/14/2019
Serving Size (g): 0.92
Date Received: 05/14/2019
Test Date: 05/21/2019
Valid Through: 05/21/2020
Report Issued: 05/22/2019

Sample #116936
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 4.87837 5.05096 103.54 5.07158 103.96 0.41
Cannabidiolic Acid (CBDA) 0 5.09332 5.21514 102.39 5.23472 102.78 0.37
Cannabigerol (CBG) 0 5.29664 5.55824 104.94 5.65867 106.84 1.79
Cannabidiol (CBD) 0 5.65729 5.82171 102.91 6.1431 108.59 5.37
Δ9-Tetrahydrocannabivarin (THCV) 0 5.36955 5.57881 103.90 5.50233 102.47 1.38
Cannabinol (CBN) 0 5.53825 5.82733 105.22 5.76842 104.16 1.02
Δ9-Tetrahydrocannabinol (THC) 0 5.1945 5.63703 108.52 5.30036 102.04 6.16
Cannabichromene (CBC) 0 4.76568 5.15571 108.18 4.96114 104.10 3.85
Tetrahydrocannabinolic acid (THCA) 0 5.05641 5.51754 109.12 5.24268 103.68 5.11

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Test Certificate No. 116936-002 supersedes Test Certificate No. 116936-001

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 5

IRON Laboratories

Residual Solvents Analysis by
Mass Spectrometer

Test Certificate #: 116936-001
Client Name, Sample Details

Ananda
Cynthiana, KY 41031
Sample: 19AB110
Type: Topical
Method: SOP FE-44-OR3

Test Conditions

Prepsheet ID#: MIHS190514a
Scale: XS205-MI2
Temp: 22.3 °C
Baro PE: 979.6 hPa
Analyst: JRT
Technician: JRT

Sample ID#: 116936

Harvest/Process Date: 05/14/2019
Serving Size (g): 0.92
Date Received: 05/14/2019
Test Date: 05/14/2019
Valid Through: 05/13/2020
Report Issued: 05/15/2019

Sample #116936
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 5,000 200 Pass/<LOD
1,4-dioxane 5,000 200 Pass/<LOD 1-Butanol 5,000 200 Pass/<LOD
1-Pentanol 5,000 200 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 50 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 50 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 50 Pass/<LOD 2-Butanol 5,000 200 Pass/<LOD
2-Butanone (MEK) 5,000 200 Pass/<LOD 2-Ethoxyethanol 5,000 200 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 50 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 50 Pass/<LOD Benzene 2 2 Pass/<LOD
Butane 5,000 50 Pass/<LOD Chloroform 60 50 Pass/<LOD
Cumene 5,000 1,000 Pass/<LOD Cyclohexane 290 50 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 100 Pass/<LOD Ethylene glycol 5,000 500 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 200 Pass/<LOD
Methanol 3,000 200 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 5,000 500 Pass/<LOD N,N-Dimethylformamide (DMF) 5,000 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 50 Pass/<LOD Pyridine 5,000 200 Pass/<LOD
Sulfolane 5,000 200 Pass/<LOD Tetrahydrofuran (THF) 5,000 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 6 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 5

IRON Laboratories

Residual Solvents QC Report

Test Certificate #: 116936-001
Client Name, Sample Details

Ananda
Cynthiana, KY 41031
Sample: 19AB110
Type: Topical
Method: SOP FE-44-OR3

Test Conditions

Prepsheet ID#: MIHS190514a
Scale: XS205-MI2
Temp: 22.3 °C
Baro PE: 979.6 hPa
Analyst: JRT
Technician: JRT

Sample ID#: 116936

Harvest/Process Date: 05/14/2019
Serving Size (g): 0.92
Date Received: 05/14/2019
Test Date: 05/14/2019
Valid Through: 05/13/2020
Report Issued: 05/15/2019

Sample #116936
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 58 50 23.20 20.00 14.81 LRLR
Isobutane N.D. 250 86 79 34.40 31.60 8.48 LRLR
Methanol N.D. 250 174 171 69.60 68.40 1.74 LRLR
n-Butane N.D. 250 97 88 38.80 35.20 9.73 LRLR
2,2-Dimethylpropane N.D. 250 109 102 43.60 40.80 6.64 LRLR
Ethanol N.D. 250 202 202 80.80 80.80 0.00
Isopentane N.D. 250 135 126 54.00 50.40 6.90 LRLR
Acetonitrile N.D. 250 192 191 76.80 76.40 0.52
Diethyl ether N.D. 250 184 169 73.60 67.60 8.50 LR
2-propanone N.D. 250 196 196 78.40 78.40 0.00
2-propanol N.D. 250 209 209 83.60 83.60 0.00
n-Pentane N.D. 250 141 128 56.40 51.20 9.67 LRLR
2,2-Dimethylbutane N.D. 250 156 152 62.40 60.80 2.60 LRLR
2,3-Dimethylbutane N.D. 250 164 157 65.60 62.80 4.36 LRLR
Methylene chloride N.D. 250 201 198 80.40 79.20 1.50
2-Methylpentane N.D. 250 164 153 65.60 61.20 6.94 LRLR
3-Methylpentane N.D. 250 172 161 68.80 64.40 6.61 LRLR
2-Butanol N.D. 250 213 215 85.20 86.00 0.93
n-Hexane N.D. 250 172 163 68.80 65.20 5.37 LRLR
Ethyl acetate N.D. 250 211 207 84.40 82.80 1.91
Tetrahydrofuran N.D. 250 198 198 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 213 214 0.00 0.00 0.00
Benzene N.D. 250 215 214 86.00 85.60 0.47
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 191 186 76.40 74.40 2.65
Ethylene glycol N.D. 250 180 424 72.00 169.60 80.79 HRQ
Heptane N.D. 250 206 198 82.40 79.20 3.96
2-Ethoxyethanol N.D. 250 262 246 104.80 98.40 6.30
1,4-Dioxane N.D. 250 232 235 92.80 94.00 1.28
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 227 223 90.80 89.20 1.78
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 236 230 94.40 92.00 2.58
m-Xylene/p-Xylene N.D. 500 456 439 91.20 87.80 3.80
o-Xylene N.D. 250 230 221 92.00 88.40 3.99
Cumene N.D. 250 234 226 93.60 90.40 3.48
Ethylene oxide N.D. 250 213 172 85.20 68.80 21.30 LRQ

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 5

IRON Laboratories

Microbiology Analysis

Test Certificate #: 116936-001
Client Name, Sample Details

Ananda
Cynthiana, KY 41031
Sample: 19AB110
Type: Topical

Test Conditions

Scale: PB303-S
Temp: 23.2 °C
Baro Pressure: 974.3 hPa
Analyst: ARH
Technician: ARH

Sample ID#: 116936

Harvest/Process Date: 05/14/2019
Serving Size (g): 0.92
Date Received: 05/14/2019
Test Date: 05/14/2019
Valid Through: 05/13/2020
Report Issued: 05/16/2019

Sample #116936
Test Method MCFU (CFU/g) LOD (CFU/g) Status (CFU/g)
Total Aerobic FE-62 100,000 100 Pass/<LOD
Yeast & Mold FE-62 10,000 100 Pass/<LOD
Bile-tolerant gram-negative bacteria FE-62 1,000 100 Pass/<LOD
Total Coliforms FE-62 1,000 100 Pass/<LOD
E. Coli FE-62 10 10 Pass/Not Present
Salmonella FE-62 10 10 Pass/Not Present
Aspergillus spp. FE-62 10 10 Pass/Not Present

TNTC = Too Numerous To Count. Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 5