IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 116919-001
Client Name, Sample Details

Andrew Burk
Waterford Township, MI 48328
Sample: Lemon Royale
License: P232193-200101
Type: Flower
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190513
Scale: XS205-MI2
Temp: 23 °C
Baro Pressure: 974.1 hPa
Analyst: KEB
Technician: KEB
Sample ID#: 116919

Harvest/Process Date: 05/13/2019
Serving Size (g): 1
Date Received: 05/13/2019
Test Date: 05/13/2019
Valid Through: 05/13/2020
Report Issued: 05/14/2019
Sample #116919
Sample #116919 Sample #116919
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.9 30.1 N/D 1.9 N/D N/D N/D N/D 0.8 33.7 27.2 1.7 29.8
Amount (mg/g) 8.6 300.7 N/D 19.3 N/D N/D N/D N/D 8.4 337 272.4 16.9 297.7
Amount per Serving (mg) 8.6 300.7 N\D 19.3 N\D N\D N\D N\D 8.4 337.0 Serving Size~ (g): 1.0
LOQ (mg/g) 2 2 2 2 2 2 2 2 2   %Decarb. THC CBD
±%RPD 2.47 1.88 0.84 0.34 0.59 0.22 1.93 0.01 1.18 3 0%

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 3

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 116919-001
Client Name, Sample Details

Andrew Burk
Waterford Township, MI 48328
Sample: Lemon Royale
License: P232193-200101
Type: Flower
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190513
Scale: XS205-MI2
Temp: 23 °C
Baro Pressure: 974.1 hPa
Analyst: KEB
Technician: KEB
Sample ID#: 116919

Harvest/Process Date: 05/13/2019
Serving Size (g): 1
Date Received: 05/13/2019
Test Date: 05/13/2019
Valid Through: 05/13/2020
Report Issued: 05/14/2019
Sample #116919
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 4.85143 4.984 102.73 4.92578 101.53 1.18
Cannabidiolic Acid (CBDA) 0 4.87793 5.0232 102.98 5.04043 103.33 0.34
Cannabigerol (CBG) 0 4.82261 5.00161 103.71 5.01265 103.94 0.22
Cannabidiol (CBD) 0 4.91169 5.11896 104.22 5.16189 105.09 0.84
Δ9-Tetrahydrocannabivarin (THCV) 0 4.95465 5.15435 104.03 5.15384 104.02 0.01
Cannabinol (CBN) 0 4.67219 4.85271 103.86 4.88153 104.48 0.59
Δ9-Tetrahydrocannabinol (THC) 0 5.30144 5.64045 106.39 5.78136 109.05 2.47
Cannabichromene (CBC) 0 4.58231 4.92277 107.43 5.01887 109.53 1.93
Tetrahydrocannabinolic acid (THCA) 0 4.78335 5.00314 104.59 5.09823 106.58 1.88

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 3
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 116919-001
Client Name, Sample Details

Andrew Burk
Waterford Township, MI 48328
Sample: Lemon Royale
License: P232193-200101
Type: Flower
Method: SOP FE-44-OR3
Test Conditions

Scale: XS205-MI2
Temp: 22.3 °C
Baro Pressure: 979.6 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 116919

Harvest/Process Date: 05/13/2019
Serving Size (g): 1
Date Received: 05/13/2019
Test Date: 05/14/2019
Valid Through: 05/13/2020
Report Issued: 05/15/2019
Sample #116919

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.050 %

β-Ocimene:

 N/D

Camphene:

0.010 %

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

0.260 %

α-Terpinolene:

0.010 %

β-Pinene:

 N/D

Linalool:

0.120 %

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

0.070 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.900 %

Geraniol:

0.010 %

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.590 %

α-Humulene:

0.250 %

Nerolidol 1:

 N/D

Nerolidol 2:

0.050 %

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

0.100 %

Other Terpenes

Total: 2.420%
a-Phellandrene = 0.00% a-Terpineol = 0.04% Valencene = 0.12% (Other terpenes are not included in the total)

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 3

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Bio Analysis by
Microscopic Visual Inspection
Testing Accreditation #: 77802 Test Certificate #: 116919-001
Client Name, Sample Details

Andrew Burk
Waterford Township, MI 48328
Sample: Lemon Royale
License: P232193-200101
Type: Flower
Method: FE02 Microscope Dissection
Test Conditions

Analyst: ARH
Technician: SEB
Sample ID#: 116919

Harvest/Process Date: 05/13/2019
Serving Size (g): 1
Date Received: 05/13/2019
Test Date: 05/13/2019
Valid Through: 05/13/2020
Report Issued: 05/13/2019
Sample #116919
Sample #116919 Sample #116919
Impurities: Detected
Aphids - Moderate, 3 per gram.
Molds: No Types: N/A
Pests: Yes Types: Aphids
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture -

The gland heads range from small to large in size and are abundant. Slightly more of them are clear than milky with a moderate amount turning amber in color. A few of the trichomes are damaged and degrading. A few of the trichomes are reduced due to stress. If you are interested in additional testing for quantitative microbial results, please call the lab within a 1-2 days to add on additional testing. Less than 2% foreign matter. Less than 5% stem material.

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 3