IRON Laboratories

Pesticide Analysis by
Mass Spectrometer

Test Certificate #: 116857-001
Client Name, Sample Details

Ananda
Cynthiana, KY 41031
Sample: Gaia 5.8% 2x Refined
Type: Concentrate
Method: FE-52 (EN 15662 & AOAC 2007.01)

Test Conditions

Prepsheet ID#: MIPS190510a
Scale: XS205-MI2
Temp: 22.8 °C
Baro PE: 981.3 hPa
Analyst: JRT
Technician: JRT

Sample ID#: 116857

Harvest/Process Date: 05/08/2019
Test Date: 05/10/2019
Valid Through: 05/09/2020
Report Issued: 05/14/2019

Sample #116857
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.129 Pass/<LOD Abamectin**** 0.500 0.129 Pass/<LOD
Acephate 0.400 0.129 Pass/<LOD Acequinocyl 2.000 0.258 Pass/<LOD
Acetamiprid 0.200 0.129 Pass/<LOD Azoxystrobin 0.200 0.129 Pass/<LOD
Bifenazate 0.200 0.129 Pass/<LOD Bifenthrin 0.200 0.129 Pass/<LOD
Boscalid 0.400 0.129 Pass/<LOD Carbaryl 0.200 0.129 Pass/<LOD
Carbofuran 0.200 0.129 Pass/<LOD Chlorantraniliprole 0.200 0.129 Pass/<LOD
Chlorfenapyr 1.000 0.517 Pass/<LOD Chlorpyrifos 0.200 0.129 Pass/<LOD
Clofentezine 0.200 0.129 Pass/<LOD Cyfluthrin** 1.000 0.517 Pass/<LOD
Cypermethrin*** 1.000 0.517 Pass/<LOD Daminozide 1.000 0.517 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.258 Pass/<LOD Diazinon 0.200 0.129 Pass/<LOD
Dimethoate 0.200 0.129 Pass/<LOD Ethoprophos 0.200 0.129 Pass/<LOD
Etofenprox 0.400 0.129 Pass/<LOD Etoxazole 0.200 0.129 Pass/<LOD
Fenoxycarb 0.200 0.129 Pass/<LOD Fenpyroximate 0.400 0.129 Pass/<LOD
Fipronil 0.400 0.129 Pass/<LOD Flonicamid 1.000 0.129 Pass/<LOD
Fludioxonil 0.400 0.129 Pass/<LOD Hexythiazox 1.000 0.129 Pass/<LOD
Imazalil 0.200 0.129 Pass/<LOD Imidacloprid 0.400 0.129 Pass/<LOD
Kresoxim Methyl 0.400 0.129 Pass/<LOD Malathion 0.200 0.129 Pass/<LOD
Metalaxyl 0.200 0.129 Pass/<LOD Methiocarb 0.200 0.129 Pass/<LOD
Methomyl 0.400 0.129 Pass/<LOD Methyl Parathion 0.200 0.129 Pass/<LOD
MGK-264‡ 0.200 0.129 Pass/<LOD Myclobutanil 0.200 0.129 Pass/<LOD
Naled 0.500 0.129 Pass/<LOD Oxamyl 1.000 0.129 Pass/<LOD
Paclobutrazol 0.400 0.129 Pass/<LOD Permethrins† 0.200 0.129 Pass/<LOD
Phosmet 0.200 0.129 Pass/<LOD Piperonyl Butoxide 2.000 1.963 Pass/<LOD
Prallethrin 0.200 0.129 Pass/<LOD Propiconazole 0.400 0.129 Pass/<LOD
Propoxur 0.200 0.129 Pass/<LOD Pyrethrins* 1.000 0.129 Pass/<LOD
Pyridaben 0.200 0.129 Pass/<LOD Spinosad***** 0.200 0.129 Pass/<LOD
Spiromesifen 0.200 0.129 Pass/<LOD Spirotetramat 0.200 0.129 Pass/<LOD
Spiroxamine‡ 0.400 0.129 Pass/<LOD Tebuconazole 0.400 0.129 Pass/<LOD
Thiacloprid 0.200 0.129 Pass/<LOD Thiamethoxam 0.200 0.129 Pass/<LOD
Trifloxystrobin 0.200 0.129 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories

Pesticide QC Report

Test Certificate #: 116857-001
Client Name, Sample Details

Ananda
Cynthiana, KY 41031
Sample: Gaia 5.8% 2x Refined
Type: Concentrate
Method: FE-52 (EN 15662 & AOAC 2007.01)

Test Conditions

Prepsheet ID#: MIPS190510a
Scale: XS205-MI2
Temp: 22.8 °C
Baro PE: 981.3 hPa
Analyst: JRT
Technician: JRT

Sample ID#: 116857

Harvest/Process Date: 05/08/2019
Test Date: 05/10/2019
Valid Through: 05/09/2020
Report Issued: 05/14/2019

Sample #116857
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.18 1.18 118.00 118.00 0.00
Acequinocyl N.D. 1 0.388 0.443 38.80 44.30 13.24 LR
Acetamiprid N.D. 1 1.05 1.21 105.00 121.00 14.16
Aldicarb N.D. 1 1.2 1.28 120.00 128.00 6.45
Avermectin B1a N.D. 0.97 1.2 0.991 123.71 102.16 19.08
Azoxystrobin N.D. 1 1.3 1.21 130.00 121.00 7.17
Bifenazate N.D. 1 0.392 0.347 39.20 34.70 12.18 LR
Bifenthrin N.D. 1 0.961 0.937 96.10 93.70 2.53
Boscalid N.D. 1 1.05 1.23 105.00 123.00 15.79
Carbaryl N.D. 1 1.2 1.1 120.00 110.00 8.70
Carbofuran N.D. 1 1.24 1.26 124.00 126.00 1.60
Chlorantraniliprole N.D. 1 1 1.25 100.00 125.00 22.22 Q
Chlorfenapyr N.D. 1 1.11 0.763 111.00 76.30 37.05 Q
Chlorpyriphos N.D. 1 0.876 1.01 87.60 101.00 14.21
Clofentezine N.D. 1 0.779 0.914 77.90 91.40 15.95
Cyfluthrin N.D. 1 1.08 0.921 108.00 92.10 15.89
Cypermethrin N.D. 1 0.746 0.913 74.60 91.30 20.13 Q
Daminoside N.D. 1 0.464 0.347 46.40 34.70 28.85 LRQ
Diazanon N.D. 1 1.16 1.22 116.00 122.00 5.04
Dichlorvos N.D. 1 0.994 1.26 99.40 126.00 23.60 Q
Dimethoate N.D. 1 1.18 1.23 118.00 123.00 4.15
Ethoprophos N.D. 1 1.11 1.18 111.00 118.00 6.11
Etofenprox N.D. 1 0.862 0.901 86.20 90.10 4.42
Etoxazole N.D. 1 1.16 1.23 116.00 123.00 5.86
Fenoxycarb N.D. 1 1.12 1.03 112.00 103.00 8.37
Fenpyroximate N.D. 1 0.952 1 95.20 100.00 4.92
Fipronil N.D. 1 1.2 1.2 120.00 120.00 0.00
Flonicamid N.D. 1 0.96 0.994 96.00 99.40 3.48
Fludioxonil N.D. 1 1.13 1.11 113.00 111.00 1.79
Hexythiazox N.D. 1 0.774 0.784 77.40 78.40 1.28
Imazalil N.D. 1 1.25 1.29 125.00 129.00 3.15
Imidacloprid N.D. 1 0.976 1.06 97.60 106.00 8.25
Kresoxim-methyl N.D. 1 0.92 1.25 92.00 125.00 30.41 Q
Malathion N.D. 1 1.23 1.12 123.00 112.00 9.36
Metalaxyl N.D. 1 1.26 1.16 126.00 116.00 8.26
Methiocarb N.D. 1 1.03 1.12 103.00 112.00 8.37
Methomyl N.D. 1 0.946 0.941 94.60 94.10 0.53
MGK-264 N.D. 1 0.927 1.04 92.70 104.00 11.49
Myclobutanil N.D. 1 1.19 1.3 119.00 130.00 8.84
Naled (dibrom) N.D. 1 0.571 0.672 57.10 67.20 16.25 LR
Oxamyl N.D. 1 0.966 0.931 96.60 93.10 3.69
Paclobutrazol N.D. 1 1.18 1.18 118.00 118.00 0.00
Parathion-methyl N.D. 1 1.13 1.03 113.00 103.00 9.26
Permethrins N.D. 1 0.804 0.682 80.40 68.20 16.42 LR
Phosmet N.D. 1 1.09 1.08 109.00 108.00 0.92
Piperonyl butoxide N.D. 1 1.2 1.2 120.00 120.00 0.00
Prallethrin N.D. 1 1.06 1.07 106.00 107.00 0.94
Propiconazole N.D. 1 1.12 1.16 112.00 116.00 3.51
Propoxur N.D. 1 1.23 1.24 123.00 124.00 0.81
Pyrethrin N.D. 0.65 0.67 0.688 103.08 105.85 2.65
Pyridaben N.D. 1 0.995 0.965 99.50 96.50 3.06
SpinosynA N.D. 0.84 0.909 0.986 108.21 117.38 8.13
SpinosynD N.D. 0.16 0.188 0.188 117.50 117.50 0.00
Spiromesifen N.D. 1 0.425 0.453 42.50 45.30 6.38 LR
Spirotetramat N.D. 1 1.08 1.18 108.00 118.00 8.85
Spiroxamine N.D. 1 0.974 0.99 97.40 99.00 1.63
Tebuconazole N.D. 1 1.13 1.19 113.00 119.00 5.17
Thiacloprid N.D. 1 1.08 1.16 108.00 116.00 7.14
Thiamethoxam N.D. 1 0.943 1.07 94.30 107.00 12.62
Trifloxystrobin N.D. 1 1.23 1.3 123.00 130.00 5.53

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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