IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 116207-001
Client Name, Sample Details

Scott Gilmore
HOLT, MI 48842
Sample: Pen Sample 1
Type: Concentrate
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190404b
Scale: XS205-MI2
Temp: 23 °C
Baro Pressure: 995.8 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 116207

Harvest/Process Date: 04/04/2019
Serving Size (g): 1
Date Received: 04/04/2019
Test Date: 04/04/2019
Valid Through: 04/04/2020
Report Issued: 04/05/2019
Sample #116207
Sample #116207 Sample #116207
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 55.9 N/D N/D N/D 0.9 2.2 2.7 0.3 N/D 62.0 55.9 0.0 62.0
Amount (mg/g) 559.3 N/D N/D N/D 9.3 21.6 26.8 3.4 N/D 620.4 559.3 0.0 620.4
Amount per Serving (mg) 559.3 N\D N\D N\D 9.3 21.6 26.8 3.4 N\D 620.4 Serving Size~ (g): 1.0
LOQ (mg/g) 3.43 3.43 3.43 3.43 3.43 3.43 3.43 3.43 3.43   %Decarb. THC CBD
±%RPD 15.38 2.31 6.25 6.05 5.60 4.33 2.30 4.16 3.36 100% N/A

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 3

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 116207-001
Client Name, Sample Details

Scott Gilmore
HOLT, MI 48842
Sample: Pen Sample 1
Type: Concentrate
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190404b
Scale: XS205-MI2
Temp: 23 °C
Baro Pressure: 995.8 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 116207

Harvest/Process Date: 04/04/2019
Serving Size (g): 1
Date Received: 04/04/2019
Test Date: 04/04/2019
Valid Through: 04/04/2020
Report Issued: 04/05/2019
Sample #116207
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 4.93343 4.92756 99.88 5.09602 103.30 3.36
Cannabidiolic Acid (CBDA) 0 5.25406 5.30457 100.96 5.63545 107.26 6.05
Cannabigerol (CBG) 0 5.1864 5.08884 98.12 5.31418 102.46 4.33
Cannabidiol (CBD) 0 5.37362 5.27168 98.10 5.61176 104.43 6.25
Δ9-Tetrahydrocannabivarin (THCV) 0 5.17141 5.21011 100.75 5.43167 105.03 4.16
Cannabinol (CBN) 0 4.70667 4.7373 100.65 5.01006 106.45 5.60
Δ9-Tetrahydrocannabinol (THC) 0 5.06908 5.05197 99.66 5.89342 116.26 15.38
Cannabichromene (CBC) 0 6.23678 5.72119 91.73 5.591 89.65 2.30
Tetrahydrocannabinolic acid (THCA) 0 5.00387 4.87983 97.52 4.994 99.80 2.31

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 3
IRON Laboratories

Residual Solvents Analysis by
Mass Spectrometer
Test Certificate #: 116207-001
Client Name, Sample Details

Scott Gilmore
HOLT, MI 48842
Sample: Pen Sample 1
Type: Concentrate
Method: SOP FE-44-OR3
Test Conditions

Prepsheet ID#: MIHS190411a
Scale: XS205-MI2
Temp: 23 °C
Baro PE: 979.9 hPa
Analyst: MEH
Technician: JRT
Sample ID#: 116207

Harvest/Process Date: 04/04/2019
Serving Size (g): 1
Date Received: 04/04/2019
Test Date: 04/11/2019
Valid Through: 04/10/2020
Report Issued: 04/15/2019
Sample #116207
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 5,000 200 Pass/<LOD
1,4-dioxane 5,000 200 Pass/<LOD 1-Butanol 5,000 200 Pass/<LOD
1-Pentanol 5,000 200 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 750 50 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 50 50 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 50 50 Pass/<LOD 2-Butanol 5,000 200 Pass/<LOD
2-Butanone (MEK) 5,000 200 Pass/<LOD 2-Ethoxyethanol 5,000 200 Pass/<LOD
2-Methylbutane (Isopentane) 750 50 Pass/<LOD 2-Methylpentane (Hexanes) 50 50 Pass/<LOD
2-Methylpropane (Isobutane) 800 50 Pass/<LOD 2-propanol (Isopropyl Alcohol) 500 50 Pass/<LOD
2-Propanone (Acetone) 750 50 Pass/<LOD 3-Methylpentane (Hexanes) 50 50 Pass/<LOD
Acetonitrile 60 50 Pass/<LOD Benzene 1 1 Pass/<LOD
Butane 800 50 Pass/<LOD Chloroform 2 2 Pass/<LOD
Cumene 5,000 1,000 Pass/<LOD Cyclohexane 50 50 Pass/<LOD
Dichloromethane 125 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 1,000 500 Pass/<LOD Ethyl acetate 400 50 Pass/<LOD
Ethyl ether 500 100 Pass/<LOD Ethylene glycol 5,000 500 Pass/<LOD
Ethylene oxide 5 5 Pass/<LOD Heptane 500 50 Pass/<LOD
Hexane 50 50 Pass/<LOD Isopropyl acetate 5,000 200 Pass/<LOD
Methanol 250 200 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 5,000 500 Pass/<LOD N,N-Dimethylformamide (DMF) 5,000 500 Pass/<LOD
Pentane 750 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 2,100 50 Pass/<LOD Pyridine 5,000 200 Pass/<LOD
Sulfolane 5,000 200 Pass/<LOD Tetrahydrofuran (THF) 5,000 200 Pass/<LOD
Toluene 150 50 Pass/<LOD Trichloroethylene 25 6 Pass/<LOD
Xylenes* 150 50 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 3
IRON Laboratories

Residual Solvents QC Report
Test Certificate #: 116207-001
Client Name, Sample Details

Scott Gilmore
HOLT, MI 48842
Sample: Pen Sample 1
Type: Concentrate
Method: SOP FE-44-OR3
Test Conditions

Prepsheet ID#: MIHS190411a
Scale: XS205-MI2
Temp: 23 °C
Baro PE: 979.9 hPa
Analyst: MEH
Technician: JRT
Sample ID#: 116207

Harvest/Process Date: 04/04/2019
Serving Size (g): 1
Date Received: 04/04/2019
Test Date: 04/11/2019
Valid Through: 04/10/2020
Report Issued: 04/15/2019
Sample #116207
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 11 10 4.40 4.00 9.52 LR
Isobutane N.D. 250 18 18 7.20 7.20 0.00 LR
Methanol N.D. 250 182 186 72.80 74.40 2.17
n-Butane N.D. 250 27 29 10.80 11.60 7.14 LR
2,2-Dimethylpropane N.D. 250 33 34 13.20 13.60 2.99 LR
Ethanol N.D. 250 233 234 93.20 93.60 0.43
Isopentane N.D. 250 71 73 28.40 29.20 2.78 LR
Acetonitrile N.D. 250 229 226 91.60 90.40 1.32
Diethyl ether N.D. 250 169 163 67.60 65.20 3.61 LR
2-propanone N.D. 250 223 224 89.20 89.60 0.45
2-propanol N.D. 250 241 241 96.40 96.40 0.00
n-Pentane N.D. 250 90 90 36.00 36.00 0.00 LR
2,2-Dimethylbutane N.D. 250 116 113 46.40 45.20 2.62 LR
2,3-Dimethylbutane N.D. 250 132 135 52.80 54.00 2.25 LR
Methylene chloride N.D. 250 222 223 88.80 89.20 0.45
2-Methylpentane N.D. 250 128 129 51.20 51.60 0.78 LR
3-Methylpentane N.D. 250 140 142 56.00 56.80 1.42 LR
2-Butanol N.D. 250 253 249 101.20 99.60 1.59
n-Hexane N.D. 250 143 145 57.20 58.00 1.39 LR
Ethyl acetate N.D. 250 244 244 97.60 97.60 0.00
Tetrahydrofuran N.D. 250 225 228 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 249 247 0.00 0.00 0.00
Benzene N.D. 250 243 247 97.20 98.80 1.63
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 191 192 76.40 76.80 0.52
Ethylene glycol N.D. 250 260 266 104.00 106.40 2.28
Heptane N.D. 250 196 197 78.40 78.80 0.51
2-Ethoxyethanol N.D. 250 284 271 113.60 108.40 4.68
1,4-Dioxane N.D. 250 270 265 108.00 106.00 1.87
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 262 263 104.80 105.20 0.38
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 273 272 109.20 108.80 0.37
m-Xylene/p-Xylene N.D. 500 533 535 106.60 107.00 0.37
o-Xylene N.D. 250 272 273 108.80 109.20 0.37
Cumene N.D. 250 276 277 110.40 110.80 0.36
Ethylene oxide N.D. 250 171 162 68.40 64.80 5.41 LR

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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