IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 115741-001
Client Name, Sample Details

Cannoid, LLC
Denver, CO 80221
Sample: Soft Gels 10015
Type: Concentrate
Method: FE04U HPLC-UV

Test Conditions

Prepsheet ID#: MIP190319a
Scale: XS205-MI2
Temp: 23.6 °C
Baro Pressure: 992.6 hPa
Analyst: KEB
Technician: KEB

Sample ID#: 115741

Harvest/Process Date: 03/19/2019
Serving Size (g): 0.92
Date Received: 03/19/2019
Test Date: 03/19/2019
Valid Through: 03/19/2020
Report Issued: 03/20/2019

Sample #115741
Sample #115741 Sample #115741
Test
Compounds
THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.3 N/D 3.3 0.1 0.0 0.1 0.2 0.1 0.2 4.3 0.3 3.3 4.3
Amount (mg/g) 3.1 N/D 32.9 0.5 0.4 0.7 2.0 0.9 2.1 42.6 3.1 33.3 42.5
Amount per Serving (mg) 2.9 N\D 30.3 0.5 0.4 0.6 1.8 0.8 1.9 39.2 Serving Size~ (g): 0.9
LOQ (mg/g) 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17 0.17   %Decarb. THC CBD
±%RPD 6.03 2.84 1.36 1.74 5.44 2.35 0.23 1.28 1.13 100% 99

1 serving ~ 1 mL (declared)

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 7

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 115741-001
Client Name, Sample Details

Cannoid, LLC
Denver, CO 80221
Sample: Soft Gels 10015
Type: Concentrate
Method: FE04U HPLC-UV

Test Conditions

Prepsheet ID#: MIP190319a
Scale: XS205-MI2
Temp: 23.6 °C
Baro Pressure: 992.6 hPa
Analyst: KEB
Technician: KEB

Sample ID#: 115741

Harvest/Process Date: 03/19/2019
Serving Size (g): 0.92
Date Received: 03/19/2019
Test Date: 03/19/2019
Valid Through: 03/19/2020
Report Issued: 03/20/2019

Sample #115741
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 5.34544 5.10533 95.51 5.16327 96.59 1.13
Cannabidiolic Acid (CBDA) 0 6.21895 5.89572 94.80 5.99912 96.47 1.74
Cannabigerol (CBG) 0 7.45405 7.22602 96.94 7.39797 99.25 2.35
Cannabidiol (CBD) 0 5.95866 5.85319 98.23 5.93357 99.58 1.36
Δ9-Tetrahydrocannabivarin (THCV) 0 6.6174 6.35545 96.04 6.27483 94.82 1.28
Cannabinol (CBN) 0 5.69242 5.76087 101.20 5.45589 95.84 5.44
Δ9-Tetrahydrocannabinol (THC) 0 5.86514 5.81124 99.08 6.17264 105.24 6.03
Cannabichromene (CBC) 0 7.80428 8.17806 104.79 8.19653 105.03 0.23
Tetrahydrocannabinolic acid (THCA) 0 5.76715 5.72969 99.35 5.895 102.22 2.84

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 7

IRON Laboratories

Pesticide Analysis by
Mass Spectrometer

Test Certificate #: 115741-001
Client Name, Sample Details

Cannoid, LLC
Denver, CO 80221
Sample: Soft Gels 10015
Type: Concentrate
Method: FE-52 (EN 15662 & AOAC 2007.01)

Test Conditions

Prepsheet ID#: MIPS190319c
Scale: XS205-MI2
Temp: 22.8 °C
Baro PE: 979.5 hPa
Analyst: MEH
Technician: MEH

Sample ID#: 115741

Harvest/Process Date: 03/19/2019
Serving Size (g): 0.92
Date Received: 03/19/2019
Test Date: 03/19/2019
Valid Through: 03/18/2020
Report Issued: 03/22/2019

Sample #115741
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.127 Pass/<LOD Abamectin**** 0.500 0.127 Pass/<LOD
Acephate 0.400 0.127 Pass/<LOD Acequinocyl 2.000 0.254 Pass/<LOD
Acetamiprid 0.200 0.127 Pass/<LOD Azoxystrobin 0.200 0.127 Pass/<LOD
Bifenazate 0.200 0.127 Pass/<LOD Bifenthrin 0.200 0.127 Pass/<LOD
Boscalid 0.400 0.127 Pass/<LOD Carbaryl 0.200 0.127 Pass/<LOD
Carbofuran 0.200 0.127 Pass/<LOD Chlorantraniliprole 0.200 0.127 Pass/<LOD
Chlorfenapyr 1.000 0.508 Pass/<LOD Chlorpyrifos 0.200 0.127 Pass/<LOD
Clofentezine 0.200 0.127 Pass/<LOD Cyfluthrin** 1.000 0.508 Pass/<LOD
Cypermethrin*** 1.000 0.508 Pass/<LOD Daminozide 1.000 0.508 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.254 Pass/<LOD Diazinon 0.200 0.127 Pass/<LOD
Dimethoate 0.200 0.127 Pass/<LOD Ethoprophos 0.200 0.127 Pass/<LOD
Etofenprox 0.400 0.127 Pass/<LOD Etoxazole 0.200 0.127 Pass/<LOD
Fenoxycarb 0.200 0.127 Pass/<LOD Fenpyroximate 0.400 0.127 Pass/<LOD
Fipronil 0.400 0.127 Pass/<LOD Flonicamid 1.000 0.127 Pass/<LOD
Fludioxonil 0.400 0.127 Pass/<LOD Hexythiazox 1.000 0.127 Pass/<LOD
Imazalil 0.200 0.127 Pass/<LOD Imidacloprid 0.400 0.127 Pass/<LOD
Kresoxim Methyl 0.400 0.127 Pass/<LOD Malathion 0.200 0.127 Pass/<LOD
Metalaxyl 0.200 0.127 Pass/<LOD Methiocarb 0.200 0.127 Pass/<LOD
Methomyl 0.400 0.127 Pass/<LOD Methyl Parathion 0.200 0.127 Pass/<LOD
MGK-264‡ 0.200 0.127 Pass/<LOD Myclobutanil 0.200 0.127 Pass/<LOD
Naled 0.500 0.127 Pass/<LOD Oxamyl 1.000 0.127 Pass/<LOD
Paclobutrazol 0.400 0.127 Pass/<LOD Permethrins† 0.200 0.127 Pass/<LOD
Phosmet 0.200 0.127 Pass/<LOD Piperonyl Butoxide 2.000 1.929 Pass/<LOD
Prallethrin 0.200 0.127 Pass/<LOD Propiconazole 0.400 0.127 Pass/<LOD
Propoxur 0.200 0.127 Pass/<LOD Pyrethrins* 1.000 0.127 Pass/<LOD
Pyridaben 0.200 0.127 Pass/<LOD Spinosad***** 0.200 0.127 Pass/<LOD
Spiromesifen 0.200 0.127 Pass/<LOD Spirotetramat 0.200 0.127 Pass/<LOD
Spiroxamine‡ 0.400 0.127 Pass/<LOD Tebuconazole 0.400 0.127 Pass/<LOD
Thiacloprid 0.200 0.127 Pass/<LOD Thiamethoxam 0.200 0.127 Pass/<LOD
Trifloxystrobin 0.200 0.127 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 7

IRON Laboratories

Pesticide QC Report

Test Certificate #: 115741-001
Client Name, Sample Details

Cannoid, LLC
Denver, CO 80221
Sample: Soft Gels 10015
Type: Concentrate
Method: FE-52 (EN 15662 & AOAC 2007.01)

Test Conditions

Prepsheet ID#: MIPS190319c
Scale: XS205-MI2
Temp: 22.8 °C
Baro PE: 979.5 hPa
Analyst: MEH
Technician: MEH

Sample ID#: 115741

Harvest/Process Date: 03/19/2019
Serving Size (g): 0.92
Date Received: 03/19/2019
Test Date: 03/19/2019
Valid Through: 03/18/2020
Report Issued: 03/22/2019

Sample #115741
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.03 1.07 103.00 107.00 3.81
Acequinocyl N.D. 1 0.459 0.545 45.90 54.50 17.13 LR
Acetamiprid N.D. 1 1.11 1.07 111.00 107.00 3.67
Aldicarb N.D. 1 1.16 1.15 116.00 115.00 0.87
Avermectin B1a N.D. 0.97 1.17 0.946 120.62 97.53 21.17 Q
Azoxystrobin N.D. 1 1.06 1.1 106.00 110.00 3.70
Bifenazate N.D. 1 0.0166 0.0291 1.66 2.91 54.70 LRQ
Bifenthrin N.D. 1 0.861 0.953 86.10 95.30 10.14
Boscalid N.D. 1 0.815 0.978 81.50 97.80 18.18
Carbaryl N.D. 1 1.08 1.05 108.00 105.00 2.82
Carbofuran N.D. 1 1.22 1.29 122.00 129.00 5.58
Chlorantraniliprole N.D. 1 1.01 1.12 101.00 112.00 10.33
Chlorfenapyr N.D. 1 0.733 1.15 73.30 115.00 44.29 Q
Chlorpyriphos N.D. 1 1.09 1.11 109.00 111.00 1.82
Clofentezine N.D. 1 1.52 1.12 152.00 112.00 30.30 HRQ
Cyfluthrin N.D. 1 1.06 1.1 106.00 110.00 3.70
Cypermethrin N.D. 1 0.939 1.08 93.90 108.00 13.97
Daminoside N.D. 1 0.816 0.905 81.60 90.50 10.34
Diazanon N.D. 1 0.882 0.944 88.20 94.40 6.79
Dichlorvos N.D. 1 1.19 1.29 119.00 129.00 8.06
Dimethoate N.D. 1 1.16 1.09 116.00 109.00 6.22
Ethoprophos N.D. 1 1.05 1.13 105.00 113.00 7.34
Etofenprox N.D. 1 0.891 1.01 89.10 101.00 12.52
Etoxazole N.D. 1 1.12 1.06 112.00 106.00 5.50
Fenoxycarb N.D. 1 1.02 1.2 102.00 120.00 16.22
Fenpyroximate N.D. 1 0.938 1.07 93.80 107.00 13.15
Fipronil N.D. 1 1.07 1.16 107.00 116.00 8.07
Flonicamid N.D. 1 1.05 1.04 105.00 104.00 0.96
Fludioxonil N.D. 1 1.05 1.04 105.00 104.00 0.96
Hexythiazox N.D. 1 0.909 1.08 90.90 108.00 17.19
Imazalil N.D. 1 1.17 1.24 117.00 124.00 5.81
Imidacloprid N.D. 1 0.985 1.01 98.50 101.00 2.51
Kresoxim-methyl N.D. 1 1.08 1.13 108.00 113.00 4.52
Malathion N.D. 1 1.1 1.37 110.00 137.00 21.86 HRQ
Metalaxyl N.D. 1 1.16 1.19 116.00 119.00 2.55
Methiocarb N.D. 1 1.14 1.2 114.00 120.00 5.13
Methomyl N.D. 1 1.17 1.1 117.00 110.00 6.17
MGK-264 N.D. 1 0.834 0.828 83.40 82.80 0.72
Myclobutanil N.D. 1 0.926 1.07 92.60 107.00 14.43
Naled (dibrom) N.D. 1 0.906 0.959 90.60 95.90 5.68
Oxamyl N.D. 1 1.27 1.08 127.00 108.00 16.17
Paclobutrazol N.D. 1 0.993 1.13 99.30 113.00 12.91
Parathion-methyl N.D. 1 1.23 1.23 123.00 123.00 0.00
Permethrins N.D. 1 0.848 0.892 84.80 89.20 5.06
Phosmet N.D. 1 1.01 1.18 101.00 118.00 15.53
Piperonyl butoxide N.D. 1 1.35 1.25 135.00 125.00 7.69 HR
Prallethrin N.D. 1 1 1.14 100.00 114.00 13.08
Propiconazole N.D. 1 0.98 1.14 98.00 114.00 15.09
Propoxur N.D. 1 1.16 1.23 116.00 123.00 5.86
Pyrethrin N.D. 0.65 0.806 0.743 124.00 114.31 8.13
Pyridaben N.D. 1 0.955 1.08 95.50 108.00 12.29
SpinosynA N.D. 0.84 1.36 0.813 161.90 96.79 50.35 HRQ
SpinosynD N.D. 0.16 0.178 0.186 111.25 116.25 4.40
Spiromesifen N.D. 1 0.673 0.618 67.30 61.80 8.52 LR
Spirotetramat N.D. 1 1.23 1.24 123.00 124.00 0.81
Spiroxamine N.D. 1 1.29 1.25 129.00 125.00 3.15
Tebuconazole N.D. 1 0.859 1.04 85.90 104.00 19.06
Thiacloprid N.D. 1 1.08 1.02 108.00 102.00 5.71
Thiamethoxam N.D. 1 1.01 0.965 101.00 96.50 4.56
Trifloxystrobin N.D. 1 1.13 1.14 113.00 114.00 0.88

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 7

IRON Laboratories

Residual Solvents Analysis by
Mass Spectrometer

Test Certificate #: 115741-001
Client Name, Sample Details

Cannoid, LLC
Denver, CO 80221
Sample: Soft Gels 10015
Type: Concentrate
Method: SOP FE-44-OR3

Test Conditions

Prepsheet ID#: MIHS190320a
Scale: XS205-MI2
Temp: 21.2 °C
Baro PE: 969.9 hPa
Analyst: MEH
Technician: JRT

Sample ID#: 115741

Harvest/Process Date: 03/19/2019
Serving Size (g): 0.92
Date Received: 03/19/2019
Test Date: 03/20/2019
Valid Through: 03/19/2020
Report Issued: 03/21/2019

Sample #115741
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 5,000 200 Pass/<LOD
1,4-dioxane 5,000 200 Pass/<LOD 1-Butanol 5,000 200 Pass/<LOD
1-Pentanol 5,000 200 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 50 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 50 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 50 Pass/<LOD 2-Butanol 5,000 200 Pass/<LOD
2-Butanone (MEK) 5,000 200 Pass/<LOD 2-Ethoxyethanol 5,000 200 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 50 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 50 Pass/<LOD Benzene 2 2 Pass/<LOD
Butane 5,000 50 Pass/<LOD Chloroform 60 50 Pass/<LOD
Cumene 5,000 1,000 Pass/<LOD Cyclohexane 290 50 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 100 Pass/<LOD Ethylene glycol 5,000 500 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 200 Pass/<LOD
Methanol 3,000 200 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 5,000 500 Pass/<LOD N,N-Dimethylformamide (DMF) 5,000 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 50 Pass/<LOD Pyridine 5,000 200 Pass/<LOD
Sulfolane 5,000 200 Pass/<LOD Tetrahydrofuran (THF) 5,000 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 6 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 7

IRON Laboratories

Residual Solvents QC Report

Test Certificate #: 115741-001
Client Name, Sample Details

Cannoid, LLC
Denver, CO 80221
Sample: Soft Gels 10015
Type: Concentrate
Method: SOP FE-44-OR3

Test Conditions

Prepsheet ID#: MIHS190320a
Scale: XS205-MI2
Temp: 21.2 °C
Baro PE: 969.9 hPa
Analyst: MEH
Technician: JRT

Sample ID#: 115741

Harvest/Process Date: 03/19/2019
Serving Size (g): 0.92
Date Received: 03/19/2019
Test Date: 03/20/2019
Valid Through: 03/19/2020
Report Issued: 03/21/2019

Sample #115741
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 13 14 5.20 5.60 7.41 LR
Isobutane N.D. 250 43 44 17.20 17.60 2.30 LR
Methanol N.D. 250 335 321 134.00 128.40 4.27 HR
n-Butane N.D. 250 70 69 28.00 27.60 1.44 LR
2,2-Dimethylpropane N.D. 250 73 74 29.20 29.60 1.36 LR
Ethanol N.D. 250 226 227 90.40 90.80 0.44
Isopentane N.D. 250 128 125 51.20 50.00 2.37 LR
Acetonitrile N.D. 250 575 562 230.00 224.80 2.29 HR
Diethyl ether N.D. 250 241 235 96.40 94.00 2.52
2-propanone N.D. 250 327 310 130.80 124.00 5.34 HR
2-propanol N.D. 250 303 300 121.20 120.00 1.00
n-Pentane N.D. 250 157 154 62.80 61.60 1.93 LR
2,2-Dimethylbutane N.D. 250 179 167 71.60 66.80 6.94 LR
2,3-Dimethylbutane N.D. 250 184 193 73.60 77.20 4.77
Methylene chloride N.D. 250 350 347 140.00 138.80 0.86 HR
2-Methylpentane N.D. 250 193 187 77.20 74.80 3.16
3-Methylpentane N.D. 250 200 198 80.00 79.20 1.01
2-Butanol N.D. 250 297 291 118.80 116.40 2.04
n-Hexane N.D. 250 210 210 84.00 84.00 0.00
Ethyl acetate N.D. 250 354 347 141.60 138.80 2.00 HR
Tetrahydrofuran N.D. 250 307 302 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 319 315 0.00 0.00 0.00
Benzene N.D. 250 301 293 120.40 117.20 2.69
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 247 243 98.80 97.20 1.63
Ethylene glycol N.D. 250 219 211 87.60 84.40 3.72
Heptane N.D. 250 244 242 97.60 96.80 0.82
2-Ethoxyethanol N.D. 250 256 244 102.40 97.60 4.80
1,4-Dioxane N.D. 250 288 281 115.20 112.40 2.46
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 298 291 119.20 116.40 2.38
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 284 277 113.60 110.80 2.50
m-Xylene/p-Xylene N.D. 500 587 575 117.40 115.00 2.07
o-Xylene N.D. 250 284 278 113.60 111.20 2.14
Cumene N.D. 250 279 272 111.60 108.80 2.54
Ethylene oxide N.D. 250 249 249 99.60 99.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 7

IRON Laboratories

Microbiology Analysis

Test Certificate #: 115741-001
Client Name, Sample Details

Cannoid, LLC
Denver, CO 80221
Sample: Soft Gels 10015
Type: Concentrate

Test Conditions

Scale: XS205-MI
Temp: 19.7 °C
Baro Pressure: 987.1 hPa
Analyst: ACR
Technician: ARH

Sample ID#: 115741

Harvest/Process Date: 03/19/2019
Serving Size (g): 0.92
Date Received: 03/19/2019
Test Date: 03/25/2019
Valid Through: 03/24/2020
Report Issued: 03/27/2019

Sample #115741
Test Method MCFU (CFU/g) LOD (CFU/g) Status (CFU/g)
Total Aerobic FE-62 100,000 1 Pass/<LOD
Yeast & Mold FE-62 10,000 1 Pass/<LOD
Bile-tolerant gram-negative bacteria FE-62 1,000 1 Pass/<LOD
Total Coliforms FE-62 1,000 1 Pass/<LOD
E. Coli FE-62 1 1 Pass/Not Present
Salmonella FE-62 1 1 Pass/Not Present
Aspergillus spp. FE-62 1 1 Pass/Not Present

TNTC = Too Numerous To Count. Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories

Heavy Metals Analysis

Test Certificate #: 115741-001
Client Name, Sample Details

Cannoid, LLC
Denver, CO 80221
Sample: Soft Gels 10015
Type: Concentrate
Method: FE60 ICPMS-MI

Test Conditions

Analyst: JER
Technician: TAC

Sample ID#: 115741

Harvest/Process Date: 03/19/2019
Serving Size (g): 0.92
Date Received: 03/19/2019
Report Issued: 03/20/2019

Sample #115741
Sample #115741 Sample #115741
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Arsenic 0.2 0.05 Pass/0.000
Copper Not Tested
Cadmium 0.2 0.05 Pass/0.000
Chromium 0.6 0.063 Pass/0.000
Lead 0.5 0.05 Pass/0.232
Mercury 0.1 0.05 Pass/0.000
Nickel Not Tested

MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 7 of 7