ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Hemp Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 115685-001
Client Name, Sample Details

Just Cause
Drain, OR 97435
Sample: Biomass Hemp
License: AGR-1052775IHG
Type: Industrial Hemp
Method: FE58 HPLC1100-OR1
***Moisture: 13.13%
Test Conditions

Scale: XS205-OR1
Temp: 20.8 °C
Baro Pressure: 1011 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 115685

Harvest/Process Date: 03/15/2019
Date Received: 03/15/2019
Test Date: 03/20/2019
Sample #115685
Sample #115685 Sample #115685
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV Total THC Total CBD
Amount 0.02% 7.38% 0.61% 0.10% 0.03% N/D 0.08% 0.25% N/D 0.30% 7.08%
LOQ 0.02% 0.02% 0.02% 0.02% 0.02% 0.02% 0.02% 0.02% 0.02%
Uncertainty ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 115685-001
Client Name, Sample Details

Just Cause
Drain, OR 97435
Sample: Biomass Hemp
License: AGR-1052775IHG
Type: Industrial Hemp
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Prepsheet ID#: ORPS190318a
Scale: Veritas-OR1
Temp: 21.9 °C
Baro PE: 999.8 hPa
Analyst: JDM
Technician: JDM
Sample ID#: 115685

Harvest/Process Date: 03/15/2019
Date Received: 03/15/2019
Test Date: 03/19/2019
Sample #115685
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.120 Pass/<LOD Abamectin**** 0.500 0.120 Pass/<LOD
Acephate 0.400 0.120 Pass/<LOD Acequinocyl 2.000 0.241 Pass/<LOD
Acetamiprid 0.200 0.120 Pass/<LOD Azoxystrobin 0.200 0.120 Pass/<LOD
Bifenazate 0.200 0.120 Pass/<LOD Bifenthrin 0.200 0.120 Pass/<LOD
Boscalid 0.400 0.120 Pass/<LOD Carbaryl 0.200 0.120 Pass/<LOD
Carbofuran 0.200 0.120 Pass/<LOD Chlorantraniliprole 0.200 0.120 Pass/<LOD
Chlorfenapyr 1.000 0.481 Pass/<LOD Chlorpyrifos 0.200 0.120 Pass/<LOD
Clofentezine 0.200 0.120 Pass/<LOD Cyfluthrin** 1.000 0.481 Pass/<LOD
Cypermethrin*** 1.000 0.481 Pass/<LOD Daminozide 1.000 0.120 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.241 Pass/<LOD Diazinon 0.200 0.120 Pass/<LOD
Dimethoate 0.200 0.120 Pass/<LOD Ethoprophos 0.200 0.120 Pass/<LOD
Etofenprox 0.400 0.120 Pass/<LOD Etoxazole 0.200 0.120 Pass/<LOD
Fenoxycarb 0.200 0.120 Pass/<LOD Fenpyroximate 0.400 0.120 Pass/<LOD
Fipronil 0.400 0.120 Pass/<LOD Flonicamid 1.000 0.120 Pass/<LOD
Fludioxonil 0.400 0.120 Pass/<LOD Hexythiazox 1.000 0.120 Pass/<LOD
Imazalil 0.200 0.120 Pass/<LOD Imidacloprid 0.400 0.120 Pass/<LOD
Kresoxim Methyl 0.400 0.120 Pass/<LOD Malathion 0.200 0.120 Pass/<LOD
Metalaxyl 0.200 0.120 Pass/<LOD Methiocarb 0.200 0.120 Pass/<LOD
Methomyl 0.400 0.120 Pass/<LOD Methyl Parathion 0.200 0.120 Pass/<LOD
MGK-264‡ 0.200 0.120 Pass/<LOD Myclobutanil 0.000 0.120 Pass/<LOD
Naled 0.500 0.120 Pass/<LOD Oxamyl 1.000 0.120 Pass/<LOD
Paclobutrazol 0.400 0.120 Pass/<LOD Permethrins† 0.200 0.120 Pass/<LOD
Phosmet 0.200 0.120 Pass/<LOD Piperonyl Butoxide 2.000 0.120 Pass/<LOD
Prallethrin 0.200 0.120 Pass/<LOD Propiconazole 0.400 0.120 Pass/<LOD
Propoxur 0.200 0.120 Pass/<LOD Pyrethrins* 1.000 0.120 Pass/<LOD
Pyridaben 0.200 0.120 Pass/<LOD Spinosad***** 0.200 0.120 Pass/<LOD
Spiromesifen 0.200 0.120 Pass/<LOD Spirotetramat 0.200 0.120 Pass/<LOD
Spiroxamine‡ 0.400 0.120 Pass/<LOD Tebuconazole 0.400 0.120 Pass/<LOD
Thiacloprid 0.200 0.120 Pass/<LOD Thiamethoxam 0.200 0.120 Pass/<LOD
Trifloxystrobin 0.200 0.120 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 115685-001
Client Name, Sample Details

Just Cause
Drain, OR 97435
Sample: Biomass Hemp
License: AGR-1052775IHG
Type: Industrial Hemp
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Prepsheet ID#: ORPS190318a
Scale: Veritas-OR1
Temp: 21.9 °C
Baro PE: 999.8 hPa
Analyst: JDM
Technician: JDM
Sample ID#: 115685

Harvest/Process Date: 03/15/2019
Date Received: 03/15/2019
Test Date: 03/19/2019
Sample #115685
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.14 1.15 114.00 115.00 0.87
Acequinocyl N.D. 1 0.618 0.623 61.80 62.30 0.81 LR
Acetamiprid N.D. 1 1.1 1.14 110.00 114.00 3.57
Aldicarb N.D. 1 1.11 1.12 111.00 112.00 0.90
Avermectin B1a N.D. 0.97 1.2 1.27 123.71 130.93 5.67 HR
Azoxystrobin N.D. 1 0.892 0.973 89.20 97.30 8.69
Bifenazate N.D. 1 1.06 1.13 106.00 113.00 6.39
Bifenthrin N.D. 1 1.22 1.32 122.00 132.00 7.87 HR
Boscalid N.D. 1 0.976 0.908 97.60 90.80 7.22
Carbaryl N.D. 1 1.15 1.27 115.00 127.00 9.92
Carbofuran N.D. 1 1.25 1.27 125.00 127.00 1.59
Chlorantraniliprole N.D. 1 0.981 1.07 98.10 107.00 8.68
Chlorfenapyr N.D. 1 0.907 0.874 90.70 87.40 3.71
Chlorpyriphos N.D. 1 1.1 1.12 110.00 112.00 1.80
Clofentezine N.D. 1 1.18 1.13 118.00 113.00 4.33
Cyfluthrin N.D. 1 1.09 1.13 109.00 113.00 3.60
Cypermethrin N.D. 1 1.19 1.2 119.00 120.00 0.84
Daminoside N.D. 1 0.564 0.615 56.40 61.50 8.65 LR
Diazanon N.D. 1 1.01 0.992 101.00 99.20 1.80
Dichlorvos N.D. 1 1.2 1.24 120.00 124.00 3.28
Dimethoate N.D. 1 1.1 1.17 110.00 117.00 6.17
Ethoprophos N.D. 1 0.954 0.959 95.40 95.90 0.52
Etofenprox N.D. 1 1.11 1.15 111.00 115.00 3.54
Etoxazole N.D. 1 1.19 1.19 119.00 119.00 0.00
Fenoxycarb N.D. 1 1.08 1.05 108.00 105.00 2.82
Fenpyroximate N.D. 1 1.13 1.17 113.00 117.00 3.48
Fipronil N.D. 1 1.02 0.976 102.00 97.60 4.41
Flonicamid N.D. 1 1.15 1.1 115.00 110.00 4.44
Fludioxonil N.D. 1 0.974 0.978 97.40 97.80 0.41
Hexythiazox N.D. 1 0.867 0.852 86.70 85.20 1.75
Imazalil N.D. 1 1.14 1.2 114.00 120.00 5.13
Imidacloprid N.D. 1 1.25 1.23 125.00 123.00 1.61
Kresoxim-methyl N.D. 1 1.07 0.985 107.00 98.50 8.27
Malathion N.D. 1 1.07 1.06 107.00 106.00 0.94
Metalaxyl N.D. 1 1.18 1.22 118.00 122.00 3.33
Methiocarb N.D. 1 1.04 1.06 104.00 106.00 1.90
Methomyl N.D. 1 1.16 1.24 116.00 124.00 6.67
MGK-264 N.D. 1 0.998 1.11 99.80 111.00 10.63
Myclobutanil N.D. 1 1.11 1.07 111.00 107.00 3.67
Naled (dibrom) N.D. 1 0.719 0.752 71.90 75.20 4.49
Oxamyl N.D. 1 1.21 1.18 121.00 118.00 2.51
Paclobutrazol N.D. 1 1.09 1.21 109.00 121.00 10.43
Parathion-methyl N.D. 1 1.02 1.04 102.00 104.00 1.94
Permethrins N.D. 1 1.2 1.31 120.00 131.00 8.76 HR
Phosmet N.D. 1 1.05 1.09 105.00 109.00 3.74
Piperonyl butoxide N.D. 1 1.12 1.18 112.00 118.00 5.22
Prallethrin N.D. 1 1.03 1.1 103.00 110.00 6.57
Propiconazole N.D. 1 1.06 1.1 106.00 110.00 3.70
Propoxur N.D. 1 1.1 1.05 110.00 105.00 4.65
Pyrethrin N.D. 0.65 0.688 0.68 105.85 104.62 1.17
Pyridaben N.D. 1 1.09 1.15 109.00 115.00 5.36
SpinosynA N.D. 0.84 0.996 0.939 118.57 111.79 5.89
SpinosynD N.D. 0.16 0.243 0.231 151.88 144.38 5.06 HR
Spiromesifen N.D. 1 0.243 0.243 24.30 24.30 0.00 LR
Spirotetramat N.D. 1 0.816 0.815 81.60 81.50 0.12
Spiroxamine N.D. 1 1.21 1.22 121.00 122.00 0.82
Tebuconazole N.D. 1 1.1 1.11 110.00 111.00 0.90
Thiacloprid N.D. 1 1.16 1.19 116.00 119.00 2.55
Thiamethoxam N.D. 1 1.1 1.25 110.00 125.00 12.77
Trifloxystrobin N.D. 1 1.12 1.14 112.00 114.00 1.77

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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