IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Michigan Compliant Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 115587-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Sherbert Smoothie 1
License: PR-000014
Type: Concentrate
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4050100000BBA000000047
Metrc Source Pkg#: 1A4050100000BBA000000040
Test Conditions

Prepsheet ID#: MIP190313a
Scale: XS205-MI2
Temp: 21.8 °C
Baro Pressure: 979.2 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 115587

Harvest/Process Date: 03/13/2019
Serving Size (g): 1
Date Received: 03/13/2019
Test Date: 03/13/2019
Valid Through: 03/13/2020
Report Issued: 03/14/2019
Sample #115587
Sample #115587 Sample #115587
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 2.6 77.2 N/D 2.9 N/D 1.0 N/D N/D N/D 83.7 70.3 2.6 73.9
Amount (mg/g) 26.0 771.7 N/D 29.1 N/D 10.4 N/D N/D N/D 837.2 702.8 25.5 738.7
Amount per Serving (mg) 26.0 771.7 N\D 29.1 N\D 10.4 N\D N\D N\D 837.2 Serving Size~ (g): 1.0
LOQ (mg/g) 3.26 3.26 3.26 3.26 3.26 3.26 3.26 3.26 3.26   %Decarb. THC CBD
±%RPD 3.26 5.89 6.05 4.51 1.42 0.46 0.98 4.84 2.98 3 0%

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Michigan Compliant QC Report
Testing Accreditation #: 77802 Test Certificate #: 115587-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Sherbert Smoothie 1
License: PR-000014
Type: Concentrate
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4050100000BBA000000047
Metrc Source Pkg#: 1A4050100000BBA000000040
Test Conditions

Prepsheet ID#: MIP190313a
Scale: XS205-MI2
Temp: 21.8 °C
Baro Pressure: 979.2 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 115587

Harvest/Process Date: 03/13/2019
Serving Size (g): 1
Date Received: 03/13/2019
Test Date: 03/13/2019
Valid Through: 03/13/2020
Report Issued: 03/14/2019
Sample #115587
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 4.96082 4.71021 94.95 4.85269 97.82 2.98
Cannabidiolic Acid (CBDA) 0 5.63577 5.60011 99.37 5.35286 94.98 4.51
Cannabigerol (CBG) 0 7.07509 6.86675 97.06 6.89835 97.50 0.46
Cannabidiol (CBD) 0 5.50944 5.32777 96.70 5.66015 102.74 6.05
Δ9-Tetrahydrocannabivarin (THCV) 0 6.04466 5.71585 94.56 5.99921 99.25 4.84
Cannabinol (CBN) 0 5.08973 5.19314 102.03 5.11993 100.59 1.42
Δ9-Tetrahydrocannabinol (THC) 0 5.00314 5.79256 115.78 5.60677 112.07 3.26
Cannabichromene (CBC) 0 8.15572 8.49697 104.18 8.58072 105.21 0.98
Tetrahydrocannabinolic acid (THCA) 0 5.33385 5.37677 100.80 5.06899 95.03 5.89

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 6
IRON Laboratories

Michigan Compliant Pesticide Analysis by
Mass Spectrometer
Test Certificate #: 115587-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Sherbert Smoothie 1
License: PR-000014
Type: Concentrate
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4050100000BBA000000047
Metrc Source Pkg#: 1A4050100000BBA000000040
Test Conditions

Prepsheet ID#: MIPS190319a
Scale: XS205-MI2
Temp: 22.8 °C
Baro PE: 979.5 hPa
Analyst: MEH
Technician: MEH
Sample ID#: 115587

Harvest/Process Date: 03/13/2019
Serving Size (g): 1
Date Received: 03/13/2019
Test Date: 03/19/2019
Valid Through: 03/18/2020
Report Issued: 03/21/2019
Sample #115587
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.127 Pass/<LOD Abamectin**** 0.500 0.127 Pass/<LOD
Acephate 0.400 0.127 Pass/<LOD Acequinocyl 2.000 0.255 Pass/<LOD
Acetamiprid 0.200 0.127 Pass/<LOD Azoxystrobin 0.200 0.127 Pass/<LOD
Bifenazate 0.200 0.127 Pass/<LOD Bifenthrin 0.200 0.127 Pass/<LOD
Boscalid 0.400 0.127 Pass/<LOD Carbaryl 0.200 0.127 Pass/<LOD
Carbofuran 0.200 0.127 Pass/<LOD Chlorantraniliprole 0.200 0.127 Pass/<LOD
Chlorfenapyr 1.000 0.509 Pass/<LOD Chlorpyrifos 0.200 0.127 Pass/<LOD
Clofentezine 0.200 0.127 Pass/<LOD Cyfluthrin** 1.000 0.509 Pass/<LOD
Cypermethrin*** 1.000 0.509 Pass/<LOD Daminozide 1.000 0.509 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.255 Pass/<LOD Diazinon 0.200 0.127 Pass/<LOD
Dimethoate 0.200 0.127 Pass/<LOD Ethoprophos 0.200 0.127 Pass/<LOD
Etofenprox 0.400 0.127 Pass/<LOD Etoxazole 0.200 0.127 Pass/<LOD
Fenoxycarb 0.200 0.127 Pass/<LOD Fenpyroximate 0.400 0.127 Pass/<LOD
Fipronil 0.400 0.127 Pass/<LOD Flonicamid 1.000 0.127 Pass/<LOD
Fludioxonil 0.400 0.127 Pass/<LOD Hexythiazox 1.000 0.127 Pass/<LOD
Imazalil 0.200 0.127 Pass/<LOD Imidacloprid 0.400 0.127 Pass/<LOD
Kresoxim Methyl 0.400 0.127 Pass/<LOD Malathion 0.200 0.127 Pass/<LOD
Metalaxyl 0.200 0.127 Pass/<LOD Methiocarb 0.200 0.127 Pass/<LOD
Methomyl 0.400 0.127 Pass/<LOD Methyl Parathion 0.200 0.127 Pass/<LOD
MGK-264‡ 0.200 0.127 Pass/<LOD Myclobutanil 0.200 0.127 Pass/<LOD
Naled 0.500 0.127 Pass/<LOD Oxamyl 1.000 0.127 Pass/<LOD
Paclobutrazol 0.400 0.127 Pass/<LOD Permethrins† 0.200 0.127 Pass/<LOD
Phosmet 0.200 0.127 Pass/<LOD Piperonyl Butoxide 2.000 1.935 Pass/<LOD
Prallethrin 0.200 0.127 Pass/<LOD Propiconazole 0.400 0.127 Pass/<LOD
Propoxur 0.200 0.127 Pass/<LOD Pyrethrins* 1.000 0.127 Pass/<LOD
Pyridaben 0.200 0.127 Pass/<LOD Spinosad***** 0.200 0.127 Pass/<LOD
Spiromesifen 0.200 0.127 Pass/<LOD Spirotetramat 0.200 0.127 Pass/<LOD
Spiroxamine‡ 0.400 0.127 Pass/<LOD Tebuconazole 0.400 0.127 Pass/<LOD
Thiacloprid 0.200 0.127 Pass/<LOD Thiamethoxam 0.200 0.127 Pass/<LOD
Trifloxystrobin 0.200 0.127 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 6
IRON Laboratories

Michigan Compliant Pesticide QC Report
Test Certificate #: 115587-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Sherbert Smoothie 1
License: PR-000014
Type: Concentrate
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4050100000BBA000000047
Metrc Source Pkg#: 1A4050100000BBA000000040
Test Conditions

Prepsheet ID#: MIPS190319a
Scale: XS205-MI2
Temp: 22.8 °C
Baro PE: 979.5 hPa
Analyst: MEH
Technician: MEH
Sample ID#: 115587

Harvest/Process Date: 03/13/2019
Serving Size (g): 1
Date Received: 03/13/2019
Test Date: 03/19/2019
Valid Through: 03/18/2020
Report Issued: 03/21/2019
Sample #115587
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.24 1.08 124.00 108.00 13.79
Acequinocyl N.D. 1 0.569 0.604 56.90 60.40 5.97 LR
Acetamiprid N.D. 1 1.18 1.14 118.00 114.00 3.45
Aldicarb N.D. 1 1.19 1.14 119.00 114.00 4.29
Avermectin B1a N.D. 0.97 0.97 0.942 100.00 97.11 2.93
Azoxystrobin N.D. 1 1.14 1.13 114.00 113.00 0.88
Bifenazate N.D. 1 0.0915 0.0283 9.15 2.83 105.51 LRQ
Bifenthrin N.D. 1 0.922 1.06 92.20 106.00 13.93
Boscalid N.D. 1 1.05 0.985 105.00 98.50 6.39
Carbaryl N.D. 1 1.09 1.15 109.00 115.00 5.36
Carbofuran N.D. 1 1.28 1.19 128.00 119.00 7.29
Chlorantraniliprole N.D. 1 1.14 1.15 114.00 115.00 0.87
Chlorfenapyr N.D. 1 1.23 0.97 123.00 97.00 23.64 Q
Chlorpyriphos N.D. 1 1.2 1.15 120.00 115.00 4.26
Clofentezine N.D. 1 1.29 1.08 129.00 108.00 17.72
Cyfluthrin N.D. 1 1.27 1.23 127.00 123.00 3.20
Cypermethrin N.D. 1 1.19 1.13 119.00 113.00 5.17
Daminoside N.D. 1 0.938 0.993 93.80 99.30 5.70
Diazanon N.D. 1 1.03 1.1 103.00 110.00 6.57
Dichlorvos N.D. 1 1.17 1.15 117.00 115.00 1.72
Dimethoate N.D. 1 1.3 1.18 130.00 118.00 9.68
Ethoprophos N.D. 1 1.17 1.04 117.00 104.00 11.76
Etofenprox N.D. 1 1 1.05 100.00 105.00 4.88
Etoxazole N.D. 1 1.15 1.09 115.00 109.00 5.36
Fenoxycarb N.D. 1 1.23 1.23 123.00 123.00 0.00
Fenpyroximate N.D. 1 1.05 1.1 105.00 110.00 4.65
Fipronil N.D. 1 1.21 1.07 121.00 107.00 12.28
Flonicamid N.D. 1 1.29 1.13 129.00 113.00 13.22
Fludioxonil N.D. 1 1.1 0.975 110.00 97.50 12.05
Hexythiazox N.D. 1 0.985 0.996 98.50 99.60 1.11
Imazalil N.D. 1 1.29 1.21 129.00 121.00 6.40
Imidacloprid N.D. 1 1.07 1.02 107.00 102.00 4.78
Kresoxim-methyl N.D. 1 1.27 0.995 127.00 99.50 24.28 Q
Malathion N.D. 1 1.18 1.28 118.00 128.00 8.13
Metalaxyl N.D. 1 1.23 1.13 123.00 113.00 8.47
Methiocarb N.D. 1 1.24 1.15 124.00 115.00 7.53
Methomyl N.D. 1 1.19 1.11 119.00 111.00 6.96
MGK-264 N.D. 1 1.03 0.954 103.00 95.40 7.66
Myclobutanil N.D. 1 1.05 1.02 105.00 102.00 2.90
Naled (dibrom) N.D. 1 0.912 0.848 91.20 84.80 7.27
Oxamyl N.D. 1 1.24 1.16 124.00 116.00 6.67
Paclobutrazol N.D. 1 1.08 1.09 108.00 109.00 0.92
Parathion-methyl N.D. 1 1.09 1.19 109.00 119.00 8.77
Permethrins N.D. 1 0.878 1.03 87.80 103.00 15.93
Phosmet N.D. 1 1.25 1.15 125.00 115.00 8.33
Piperonyl butoxide N.D. 1 1.28 1.13 128.00 113.00 12.45
Prallethrin N.D. 1 1.15 1.06 115.00 106.00 8.14
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.24 1.13 124.00 113.00 9.28
Pyrethrin N.D. 0.65 0.876 0.876 134.77 134.77 0.00 HR
Pyridaben N.D. 1 0.994 1.11 99.40 111.00 11.03
SpinosynA N.D. 0.84 1.05 0.92 125.00 109.52 13.20
SpinosynD N.D. 0.16 0.19 0.171 118.75 106.88 10.53
Spiromesifen N.D. 1 0.655 0.8 65.50 80.00 19.93 LR
Spirotetramat N.D. 1 1.22 1.15 122.00 115.00 5.91
Spiroxamine N.D. 1 1.3 1.18 130.00 118.00 9.68
Tebuconazole N.D. 1 0.939 0.955 93.90 95.50 1.69
Thiacloprid N.D. 1 1.22 1.15 122.00 115.00 5.91
Thiamethoxam N.D. 1 1.11 1.06 111.00 106.00 4.61
Trifloxystrobin N.D. 1 1.22 1.13 122.00 113.00 7.66

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 6
IRON Laboratories

Michigan Compliant Residual Solvents Analysis by
Mass Spectrometer
Test Certificate #: 115587-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Sherbert Smoothie 1
License: PR-000014
Type: Concentrate
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4050100000BBA000000047
Metrc Source Pkg#: 1A4050100000BBA000000040
Test Conditions

Prepsheet ID#: MIHS190313a
Scale: XS205-MI2
Temp: 22.3 °C
Baro PE: 987.8 hPa
Analyst: MEH
Technician: JRT
Sample ID#: 115587

Harvest/Process Date: 03/13/2019
Serving Size (g): 1
Date Received: 03/13/2019
Test Date: 03/13/2019
Valid Through: 03/12/2020
Report Issued: 03/14/2019
Sample #115587
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 5,000 200 Pass/<LOD
1,4-dioxane 5,000 200 Pass/<LOD 1-Butanol 5,000 200 Pass/<LOD
1-Pentanol 5,000 200 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 750 50 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 50 50 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 50 50 Pass/<LOD 2-Butanol 5,000 200 Pass/<LOD
2-Butanone (MEK) 5,000 200 Pass/<LOD 2-Ethoxyethanol 5,000 200 Pass/<LOD
2-Methylbutane (Isopentane) 750 50 Pass/<LOD 2-Methylpentane (Hexanes) 50 50 Pass/<LOD
2-Methylpropane (Isobutane) 800 50 Pass/<LOD 2-propanol (Isopropyl Alcohol) 500 50 Pass/<LOD
2-Propanone (Acetone) 750 50 Pass/135 3-Methylpentane (Hexanes) 50 50 Pass/<LOD
Acetonitrile 60 50 Pass/<LOD Benzene 1 1 Pass/<LOD
Butane 800 50 Pass/588 Chloroform 2 2 Pass/<LOD
Cumene 5,000 1,000 Pass/<LOD Cyclohexane 50 50 Pass/<LOD
Dichloromethane 125 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 1,000 500 Pass/<LOD Ethyl acetate 400 50 Pass/<LOD
Ethyl ether 500 100 Pass/<LOD Ethylene glycol 5,000 500 Pass/<LOD
Ethylene oxide 5 5 Pass/<LOD Heptane 500 50 Pass/53
Hexane 50 50 Pass/<LOD Isopropyl acetate 5,000 200 Pass/<LOD
Methanol 250 200 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 5,000 500 Pass/<LOD N,N-Dimethylformamide (DMF) 5,000 500 Pass/<LOD
Pentane 750 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 2,100 50 Pass/<LOD Pyridine 5,000 200 Pass/<LOD
Sulfolane 5,000 200 Pass/<LOD Tetrahydrofuran (THF) 5,000 200 Pass/<LOD
Toluene 150 50 Pass/<LOD Trichloroethylene 25 6 Pass/<LOD
Xylenes* 150 50 Pass/<LOD

Total Butanes = 598 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

Total PPM: 776.00
* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 6
IRON Laboratories

Michigan Compliant Residual Solvents QC Report
Test Certificate #: 115587-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Sherbert Smoothie 1
License: PR-000014
Type: Concentrate
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4050100000BBA000000047
Metrc Source Pkg#: 1A4050100000BBA000000040
Test Conditions

Prepsheet ID#: MIHS190313a
Scale: XS205-MI2
Temp: 22.3 °C
Baro PE: 987.8 hPa
Analyst: MEH
Technician: JRT
Sample ID#: 115587

Harvest/Process Date: 03/13/2019
Serving Size (g): 1
Date Received: 03/13/2019
Test Date: 03/13/2019
Valid Through: 03/12/2020
Report Issued: 03/14/2019
Sample #115587
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 48 45 19.20 18.00 6.45 LR
Isobutane N.D. 250 71 69 28.40 27.60 2.86 LR
Methanol N.D. 250 295 315 118.00 126.00 6.56
n-Butane N.D. 250 104 100 41.60 40.00 3.92 LR
2,2-Dimethylpropane N.D. 250 105 103 42.00 41.20 1.92 LR
Ethanol N.D. 250 255 253 102.00 101.20 0.79
Isopentane N.D. 250 157 152 62.80 60.80 3.24 LR
Acetonitrile N.D. 250 465 471 186.00 188.40 1.28 HR
Diethyl ether N.D. 250 258 253 103.20 101.20 1.96
2-propanone N.D. 250 324 309 129.60 123.60 4.74
2-propanol N.D. 250 313 295 125.20 118.00 5.92
n-Pentane N.D. 250 189 183 75.60 73.20 3.23
2,2-Dimethylbutane N.D. 250 197 198 78.80 79.20 0.51
2,3-Dimethylbutane N.D. 250 219 216 87.60 86.40 1.38
Methylene chloride N.D. 250 353 348 141.20 139.20 1.43 HR
2-Methylpentane N.D. 250 217 203 86.80 81.20 6.67
3-Methylpentane N.D. 250 222 217 88.80 86.80 2.28
2-Butanol N.D. 250 294 288 117.60 115.20 2.06
n-Hexane N.D. 250 231 225 92.40 90.00 2.63
Ethyl acetate N.D. 250 357 347 142.80 138.80 2.84 HR
Tetrahydrofuran N.D. 250 300 295 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 309 312 0.00 0.00 0.00
Benzene N.D. 250 301 297 120.40 118.80 1.34
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 257 249 102.80 99.60 3.16
Ethylene glycol N.D. 250 200 224 80.00 89.60 11.32
Heptane N.D. 250 261 251 104.40 100.40 3.91
2-Ethoxyethanol N.D. 250 263 262 105.20 104.80 0.38
1,4-Dioxane N.D. 250 285 282 114.00 112.80 1.06
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 297 297 118.80 118.80 0.00
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 291 289 116.40 115.60 0.69
m-Xylene/p-Xylene N.D. 500 587 586 117.40 117.20 0.17
o-Xylene N.D. 250 288 286 115.20 114.40 0.70
Cumene N.D. 250 277 279 110.80 111.60 0.72
Ethylene oxide N.D. 250 260 284 104.00 113.60 8.82

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 6
IRON Laboratories

Michigan Compliant Heavy Metals Analysis
Test Certificate #: 115587-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Sherbert Smoothie 1
License: PR-000014
Type: Concentrate
Method: FE60 ICPMS-MI
Metrc Test Pkg#: 1A4050100000BBA000000047
Metrc Source Pkg#: 1A4050100000BBA000000040
Test Conditions

Analyst: JER
Technician: TAC
Sample ID#: 115587

Harvest/Process Date: 03/13/2019
Serving Size (g): 1
Date Received: 03/13/2019
Report Issued: 03/19/2019
Sample #115587
Sample #115587 Sample #115587
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Arsenic 0.2 0.05 Pass/0.000
Copper Not Tested
Cadmium 0.2 0.05 Pass/0.000
Chromium 0.6 0.063 Pass/0.000
Lead 0.5 0.05 Pass/0.000
Mercury 0.1 0.05 Pass/0.000
Nickel Not Tested

MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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