IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 115552-001
Client Name, Sample Details

Secrets of Hemp
Columbus , IN 47201
Sample: Shea Butter 100 mg
Type: AU Topical
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190312b
Scale: XS205-MI2
Temp: 21.7 °C
Baro Pressure: 989.1 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 115552

Harvest/Process Date: 03/12/2019
Serving Size (g): 56.7
Date Received: 03/12/2019
Test Date: 03/12/2019
Valid Through: 03/12/2020
Report Issued: 03/13/2019
Sample #115552
Sample #115552 Sample #115552
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) N/D N/D 0.2 N/D N/D N/D N/D N/D N/D 0.2 0.0 0.2 0.2
Amount (mg/g) N/D N/D 2.0 N/D N/D N/D N/D N/D N/D 2 0.0 2.0 2.0
Amount per Serving (mg) N\D N\D 113.4 N\D N\D N\D N\D N\D N\D 113.4 Serving Size~ (g): 56.7
LOQ (mg/g) 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1   %Decarb. THC CBD
±%RPD 9.00 6.51 2.75 1.82 4.69 2.58 1.90 3.09 5.84 N/A 100%

1 serving = 2 oz wt (declared) Shea Butter 100mg Batch SB-101 BOD: 3/2019 Batch Size 200 oz Batch Qty 100- 2oz containers Shea Butter Refined: JEDWard International #18033/79528 PRC.CBD Analytical 360 Lot#GHL UIDANL0009689 UIB603120434 https://analytical360.com/m/tests/anl0009689

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 1

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 115552-001
Client Name, Sample Details

Secrets of Hemp
Columbus , IN 47201
Sample: Shea Butter 100 mg
Type: AU Topical
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP190312b
Scale: XS205-MI2
Temp: 21.7 °C
Baro Pressure: 989.1 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 115552

Harvest/Process Date: 03/12/2019
Serving Size (g): 56.7
Date Received: 03/12/2019
Test Date: 03/12/2019
Valid Through: 03/12/2020
Report Issued: 03/13/2019
Sample #115552
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 4.94854 4.69672 94.91 4.97906 100.62 5.84
Cannabidiolic Acid (CBDA) 0 5.42993 5.36249 98.76 5.26565 96.97 1.82
Cannabigerol (CBG) 0 6.88483 6.73192 97.78 6.56057 95.29 2.58
Cannabidiol (CBD) 0 5.22851 5.12305 97.98 4.98389 95.32 2.75
Δ9-Tetrahydrocannabivarin (THCV) 0 5.80951 5.79351 99.72 5.61708 96.69 3.09
Cannabinol (CBN) 0 5.01407 5.01451 100.01 4.78465 95.42 4.69
Δ9-Tetrahydrocannabinol (THC) 0 5.52917 5.20957 94.22 4.76098 86.11 9.00
Cannabichromene (CBC) 0 7.38002 7.36598 99.81 7.22727 97.93 1.90
Tetrahydrocannabinolic acid (THCA) 0 5.19522 5.25433 101.14 4.92302 94.76 6.51

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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