ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-002

Test Certificate #: 115512-001

Client Name, Sample Details
Octo Consulting LLC Eugene, OR 97403 Sample: B21519b Type: AU Tincture Method: FE04C-OR4 HPLC1100-OR1

Test Conditions
Scale: XS205-OR1 Temp: 22.3 °C Baro Pressure: 999 hPa Analyst: HRM Technician: EDT

Sample ID#: 115512
Batch #: 115512 Harvest/Process Date: 03/07/2019 Serving Size (g): 0.1 Package Weight (g):1 Date Received: 03/07/2019 Test Date: 03/08/2019

Test Compounds	CBDV	CBDA	CBD	CBC	CBG	CBN	THC	THCA	THCV		Calc. Avg
Avg. Amount	12.79 mg/g	7.30 mg/g	895.09 mg/g	48.08 mg/g	13.25 mg/g	3.31 mg/g	26.76 mg/g	N/D	N/D	CBD	901.49 mg/g
LOQ	0.02 mg/g	0.02 mg/g	0.02 mg/g	0.02 mg/g	0.02 mg/g	0.02 mg/g	0.02 mg/g	0.02 mg/g	0.02 mg/g	THC	26.76 mg/g
Amount per Serving~	1.28 mg/srv	0.73 mg/srv	89.51 mg/srv	4.81 mg/srv	1.33 mg/srv	0.33 mg/srv	2.68 mg/srv	N/D	N/D	Serving Size~ (g):	0.10 g
Uncertainty	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	Serving Size~ (g):	0.10 g

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 1 of 5

ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-002

*Test Certificate #: 115512-002

Client Name, Sample Details
Octo Consulting LLC Eugene, OR 97403 Sample: B21519b Type: AU Tincture Method: FE04C-OR4 HPLC1100-OR1

Test Conditions
Scale: XS205-OR1 Temp: 21.1 °C Baro Pressure: 993.8 hPa Analyst: HRM Technician: EDT

Sample ID#: 115512
Batch #: 115512 Harvest/Process Date: 03/07/2019 Serving Size (g): 0.1 Package Weight (g):1 Date Received: 03/07/2019 Test Date: 03/19/2019

Test Compounds	CBDV	CBDA	CBD	CBC	CBG	CBN	THC	THCA	THCV		Calc. Avg
Avg. Amount	13.77 mg/g	8.00 mg/g	931.83 mg/g	58.49 mg/g	15.02 mg/g	5.87 mg/g	32.07 mg/g	N/D	N/D	CBD	938.85 mg/g
LOQ	0.02 mg/g	0.02 mg/g	0.02 mg/g	0.02 mg/g	0.02 mg/g	0.02 mg/g	0.02 mg/g	0.02 mg/g	0.02 mg/g	THC	32.07 mg/g
Amount per Serving~	1.38 mg/srv	0.80 mg/srv	93.18 mg/srv	5.85 mg/srv	1.50 mg/srv	0.59 mg/srv	3.21 mg/srv	N/D	N/D	Serving Size~ (g):	0.10 g
Uncertainty	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	Serving Size~ (g):	0.10 g

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC. Test Certificate No. 115512-002 supersedes Test Certificate No. 115512-001

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 2 of 5

ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-002

Test Certificate #: 115512-001

Client Name, Sample Details
Octo Consulting LLC Eugene, OR 97403 Sample: B21519b Type: AU Tincture Method: FE04C-OR4 HPLC1100-OR1

Test Conditions
Prepsheet ID#: ORP190402a Scale: XS205-OR1 Temp: 21.6 °C Baro Pressure: 993 hPa Analyst: JER Technician: JER

Sample ID#: 115512
Batch #: 115512 Harvest/Process Date: 03/07/2019 Serving Size (g): 0.1 Package Weight (g):1 Date Received: 03/07/2019 Test Date: 04/02/2019

Test Compounds	CBDV	CBDA	CBD	CBC	CBG	CBN	THC	THCA	THCV		Calc. Avg
Avg. Amount	13.38 mg/g	7.51 mg/g	958.05 mg/g	48.80 mg/g	13.83 mg/g	3.83 mg/g	26.84 mg/g	N/D	N/D	CBD	964.63 mg/g
LOQ	2.51 mg/g	2.51 mg/g	2.51 mg/g	2.51 mg/g	2.51 mg/g	2.51 mg/g	2.51 mg/g	2.51 mg/g	2.51 mg/g	THC	26.84 mg/g
Amount per Serving~	1.34 mg/srv	0.75 mg/srv	95.81 mg/srv	4.88 mg/srv	1.38 mg/srv	0.38 mg/srv	2.68 mg/srv	N/D	N/D	Serving Size~ (g):	0.10 g
Uncertainty	2.99% RPD	3.60% RPD	3.01% RPD	0.57% RPD	2.10% RPD	8.88% RPD	99.46% RPD	0.83% RPD	0.43% RPD	Serving Size~ (g):	0.10 g

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 3 of 5

ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report

Testing Accreditation #: 4092-002

Test Certificate #: 115512-001

Client Name, Sample Details
Octo Consulting LLC Eugene, OR 97403 Sample: B21519b Type: AU Tincture Method: FE04C-OR4 HPLC1100-OR1

Test Conditions
Prepsheet ID#: ORP190402a Scale: XS205-OR1 Temp: 21.6 °C Baro Pressure: 993 hPa Analyst: JER Technician: JER

Sample ID#: 115512
Batch #: 115512 Harvest/Process Date: 03/07/2019 Serving Size (g): 0.1 Package Weight (g):1 Date Received: 03/07/2019 Test Date: 04/02/2019

Target Compound Name	LCS Spike (μg/g)	LCS Amount (μg/g)	Percent Recovery (%) LCS	LCS Duplicate Amount (μg/g)	Percent Recovery (%) LCSD	Relative Percent Difference (%)
Cannabidivarin (CBDV)	6.50358	6.77663	104.20	6.80839	104.69	0.47%
Cannabidiolic Acid (CBDA)	6.05388	6.3198	104.39	6.29758	104.03	0.35%
Cannabigerol (CBG)	6.5128	6.74636	103.59	6.70863	103.01	0.56%
Cannabidiol (CBD)	6.63301	6.90871	104.16	6.93601	104.57	0.39%
Δ9-Tetrahydrocannabivarin (THCV)	6.49291	6.75362	104.02	6.78242	104.46	0.43%
Cannabinol (CBN)	6.35509	6.55479	103.14	6.60778	103.98	0.81%
Δ9-Tetrahydrocannabinol (THC)	7.89308	8.0678	102.21	8.13409	103.05	0.82%
Cannabichromene (CBC)	4.7329	4.72822	99.90	4.83271	102.11	2.19%
Tetrahydrocannabinolic acid (THCA)	6.32463	6.54092	103.42	6.59554	104.28	0.83%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 4 of 5

ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-002

Test Certificate #: 115512-001

Client Name, Sample Details
Octo Consulting LLC Eugene, OR 97403 Sample: B21519b Type: AU Tincture Method: FE04U HPLC-UV

Test Conditions
Prepsheet ID#: ORP190507a Scale: XS205-OR1 Temp: 21.9 °C Baro Pressure: 1003 hPa Analyst: HRM Technician: JER

Sample ID#: 115512
Batch #: 115512 Harvest/Process Date: 03/07/2019 Serving Size (g): 0.1 Package Weight (g):1 Date Received: 03/07/2019 Test Date: 05/07/2019

Test Compounds	THC	THCA	CBD	CBDA	CBN	CBG	CBC	THCV*	CBDV	Total Cannabinoids*	Total THC	Total CBD	Calc Max Total Cannabinoids*
Amount (%)	2.25	N/D	80.41	0.77	0.26	1.12	4.06	N/D	1.02	89.88	2.25	81.08	89.79
Amount (mg/g)	22.47	N/D	804.09	7.68	2.62	11.18	40.56	N/D	10.19	898.79	22.47	810.83	897.85
Amount per Serving (mg)	2.25	N\D	80.41	0.77	0.26	1.12	4.06	N\D	1.02	89.88	Serving Size~ (g):		0.10
LOQ (mg/g)	0.02	0.02	0.02	0.02	0.02	0.02	0.02	0.02	0.02		%Decarb.	THC	CBD
±%RPD	4.00	3.14	5.05	3.91	1.16	4.62	1.38	3.06	4.25		%Decarb.	100	0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 4 of 5

ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report

Testing Accreditation #: 4092-002

Test Certificate #: 115512-001

Client Name, Sample Details
Octo Consulting LLC Eugene, OR 97403 Sample: B21519b Type: AU Tincture Method: FE04U HPLC-UV

Test Conditions
Prepsheet ID#: ORP190507a Scale: XS205-OR1 Temp: 21.9 °C Baro Pressure: 1003 hPa Analyst: HRM Technician: JER

Sample ID#: 115512
Batch #: 115512 Harvest/Process Date: 03/07/2019 Serving Size (g): 0.1 Package Weight (g):1 Date Received: 03/07/2019 Test Date: 05/07/2019

Target Compound Name	Method Blank (μg/g)	LCS Spike (μg/g)	LCS Amount (μg/g)	Percent Recovery (%) LCS	LCS Duplicate Amount (μg/g)	Percent Recovery (%) LCSD	Relative Percent Difference (%)
Cannabidivarin (CBDV)	N.D.	5.2	5.29	101.73	5.07	97.50	4.25
Cannabidiolic Acid (CBDA)	N.D.	5.14	5.22	101.56	5.02	97.67	3.91
Cannabigerol (CBG)	N.D.	5.26	5.31	100.95	5.07	96.39	4.62
Cannabidiol (CBD)	N.D.	5.21	5.28	101.34	5.02	96.35	5.05
Δ9-Tetrahydrocannabivarin (THCV)	N.D.	5.3	5.31	100.19	5.15	97.17	3.06
Cannabinol (CBN)	N.D.	5.05	5.19	102.77	5.13	101.58	1.16
Δ9-Tetrahydrocannabinol (THC)	N.D.	5.42	5.61	103.51	5.39	99.45	4.00
Cannabichromene (CBC)	N.D.	5.05	5.1	100.99	5.03	99.60	1.38
Tetrahydrocannabinolic acid (THCA)	N.D.	5.17	5.17	100.00	5.01	96.91	3.14

N.D. = Not Detected

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 5 of 5

Heavy Metals Analysis

Test Certificate #: 115512-001

Client Name, Sample Details
Octo Consulting LLC Eugene, OR 97403 Sample: B21519b Type: AU Tincture Method: FE60 ICPMS-MI

Test Conditions
Analyst: JER Technician: TAC

Sample ID#: 115512
Batch #: 115512 Harvest/Process Date: 03/07/2019 Serving Size (g): 0.1 Package Weight (g):1 Date Received: 03/07/2019 Report Issued: 03/14/2019

Test Compound	MRL (PPM)	LOD (PPM)	Status (PPM)
Arsenic	0.2	0.05	Pass/<LOD
Copper			Not Tested
Cadmium	0.2	0.05	Pass/<LOD
Chromium	0.6	0.063	Pass/<LOD
Lead	0.5	0.05	Pass/<LOD
Mercury	0.1	0.05	Pass/<LOD
Nickel			Not Tested

MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 5 of 5

ORELAP Cert No. 4092-002OLCC No. 1002158CD2E

Marijuana Potency Analysis byHigh Performance Liquid Chromatography

Client Name, Sample Details

Test Conditions

Sample ID#: 115512

ORELAP Cert No. 4092-002OLCC No. 1002158CD2E

Marijuana Potency Analysis byHigh Performance Liquid Chromatography

Client Name, Sample Details

Test Conditions

Sample ID#: 115512

ORELAP Cert No. 4092-002OLCC No. 1002158CD2E

Marijuana Potency Analysis byHigh Performance Liquid Chromatography

Client Name, Sample Details

Test Conditions

Sample ID#: 115512

ORELAP Cert No. 4092-002OLCC No. 1002158CD2E

QC Report

Client Name, Sample Details

Test Conditions

Sample ID#: 115512

ORELAP Cert No. 4092-002OLCC No. 1002158CD2E

Marijuana Potency Analysis byHigh Performance Liquid Chromatography

Client Name, Sample Details

Test Conditions

Sample ID#: 115512

ORELAP Cert No. 4092-002OLCC No. 1002158CD2E

QC Report

Client Name, Sample Details

Test Conditions

Sample ID#: 115512

Heavy Metals Analysis

Client Name, Sample Details

Test Conditions

Sample ID#: 115512

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E