ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 115511-001
Client Name, Sample Details

Octo Consulting LLC
Eugene, OR 97403
Sample: B21519a
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Test Conditions

Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 999 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 115511

Batch #: 115511
Harvest/Process Date: 03/07/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/07/2019
Test Date: 03/08/2019
Sample #115511
Sample #115511 Sample #115511
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Avg
Avg. Amount 13.10 mg/g 7.67 mg/g 913.82 mg/g 48.92 mg/g 13.37 mg/g 3.24 mg/g 27.35 mg/g N/D N/D CBD 920.55 mg/g
LOQ 0.02 mg/g 0.02 mg/g 0.02 mg/g 0.02 mg/g 0.02 mg/g 0.02 mg/g 0.02 mg/g 0.02 mg/g 0.02 mg/g THC 27.35 mg/g
Amount per Serving~ 1.31 mg/srv 0.77 mg/srv 91.38 mg/srv 4.89 mg/srv 1.34 mg/srv 0.32 mg/srv 2.74 mg/srv N/D N/D Serving Size~ (g): 0.10 g
Uncertainty ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 *Test Certificate #: 115511-002
Client Name, Sample Details

Octo Consulting LLC
Eugene, OR 97403
Sample: B21519a
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Test Conditions

Scale: XS205-OR1
Temp: 21.1 °C
Baro Pressure: 993.8 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 115511

Batch #: 115511
Harvest/Process Date: 03/07/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/07/2019
Test Date: 03/19/2019
Sample #115511
Sample #115511 Sample #115511
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Avg
Avg. Amount 12.63 mg/g 7.22 mg/g 916.87 mg/g 48.87 mg/g 13.60 mg/g 3.77 mg/g 26.81 mg/g 1.03 mg/g N/D CBD 923.20 mg/g
LOQ 0.02 mg/g 0.02 mg/g 0.02 mg/g 0.02 mg/g 0.02 mg/g 0.02 mg/g 0.02 mg/g 0.02 mg/g 0.02 mg/g THC 27.71 mg/g
Amount per Serving~ 1.26 mg/srv 0.72 mg/srv 91.69 mg/srv 4.89 mg/srv 1.36 mg/srv 0.38 mg/srv 2.68 mg/srv 0.10 mg/srv N/D Serving Size~ (g): 0.10 g
Uncertainty ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Test Certificate No. 115511-002 supersedes Test Certificate No. 115511-001
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 115511-001
Client Name, Sample Details

Octo Consulting LLC
Eugene, OR 97403
Sample: B21519a
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Test Conditions

Prepsheet ID#: ORP190402a
Scale: XS205-OR1
Temp: 21.6 °C
Baro Pressure: 993 hPa
Analyst: JER
Technician: JER
Sample ID#: 115511

Batch #: 115511
Harvest/Process Date: 03/07/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/07/2019
Test Date: 04/02/2019
Sample #115511
Sample #115511 Sample #115511
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Avg
Avg. Amount 13.11 mg/g 7.45 mg/g 946.97 mg/g 48.32 mg/g 13.73 mg/g 3.72 mg/g 26.66 mg/g N/D N/D CBD 953.49 mg/g
LOQ 2.34 mg/g 2.34 mg/g 2.34 mg/g 2.34 mg/g 2.34 mg/g 2.34 mg/g 2.34 mg/g 2.34 mg/g 2.34 mg/g THC 26.66 mg/g
Amount per Serving~ 1.31 mg/srv 0.75 mg/srv 94.70 mg/srv 4.83 mg/srv 1.37 mg/srv 0.37 mg/srv 2.67 mg/srv N/D N/D Serving Size~ (g): 0.10 g
Uncertainty 3.13% RPD 2.82% RPD 0.50% RPD 6.13% RPD 1.97% RPD 3.76% RPD 96.64% RPD 0.83% RPD 0.43% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 115511-001
Client Name, Sample Details

Octo Consulting LLC
Eugene, OR 97403
Sample: B21519a
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Test Conditions

Prepsheet ID#: ORP190402a
Scale: XS205-OR1
Temp: 21.6 °C
Baro Pressure: 993 hPa
Analyst: JER
Technician: JER
Sample ID#: 115511

Batch #: 115511
Harvest/Process Date: 03/07/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/07/2019
Test Date: 04/02/2019
Sample #115511
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 6.50358 6.77663 104.20 6.80839 104.69 0.47%
Cannabidiolic Acid (CBDA) 0 6.05388 6.3198 104.39 6.29758 104.03 0.35%
Cannabigerol (CBG) 0 6.5128 6.74636 103.59 6.70863 103.01 0.56%
Cannabidiol (CBD) 0 6.63301 6.90871 104.16 6.93601 104.57 0.39%
Δ9-Tetrahydrocannabivarin (THCV) 0 6.49291 6.75362 104.02 6.78242 104.46 0.43%
Cannabinol (CBN) 0 6.35509 6.55479 103.14 6.60778 103.98 0.81%
Δ9-Tetrahydrocannabinol (THC) 0 7.89308 8.0678 102.21 8.13409 103.05 0.82%
Cannabichromene (CBC) 0 4.7329 4.72822 99.90 4.83271 102.11 2.19%
Tetrahydrocannabinolic acid (THCA) 0 6.32463 6.54092 103.42 6.59554 104.28 0.83%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 115511-001
Client Name, Sample Details

Octo Consulting LLC
Eugene, OR 97403
Sample: B21519a
Type: AU Tincture
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: ORP190507a
Scale: XS205-OR1
Temp: 21.9 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: JER
Sample ID#: 115511

Batch #: 115511
Harvest/Process Date: 03/07/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/07/2019
Test Date: 05/07/2019
Sample #115511
Sample #115511 Sample #115511
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 2.38 N/D 80.79 0.79 0.27 1.11 4.15 N/D 1.03 90.53 2.38 81.49 90.44
Amount (mg/g) 23.77 N/D 807.94 7.93 2.74 11.13 41.48 N/D 10.34 905.33 23.77 814.89 904.35
Amount per Serving (mg) 2.38 N\D 80.79 0.79 0.27 1.11 4.15 N\D 1.03 90.53 Serving Size~ (g): 0.10
LOQ (mg/g) 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02 0.02   %Decarb. THC CBD
±%RPD 4.00 3.14 5.05 3.91 1.16 4.62 1.38 3.06 4.25 100 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 115511-001
Client Name, Sample Details

Octo Consulting LLC
Eugene, OR 97403
Sample: B21519a
Type: AU Tincture
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: ORP190507a
Scale: XS205-OR1
Temp: 21.9 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: JER
Sample ID#: 115511

Batch #: 115511
Harvest/Process Date: 03/07/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/07/2019
Test Date: 05/07/2019
Sample #115511
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.2 5.29 101.73 5.07 97.50 4.25
Cannabidiolic Acid (CBDA) N.D. 5.14 5.22 101.56 5.02 97.67 3.91
Cannabigerol (CBG) N.D. 5.26 5.31 100.95 5.07 96.39 4.62
Cannabidiol (CBD) N.D. 5.21 5.28 101.34 5.02 96.35 5.05
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.3 5.31 100.19 5.15 97.17 3.06
Cannabinol (CBN) N.D. 5.05 5.19 102.77 5.13 101.58 1.16
Δ9-Tetrahydrocannabinol (THC) N.D. 5.42 5.61 103.51 5.39 99.45 4.00
Cannabichromene (CBC) N.D. 5.05 5.1 100.99 5.03 99.60 1.38
Tetrahydrocannabinolic acid (THCA) N.D. 5.17 5.17 100.00 5.01 96.91 3.14

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 4