ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 115487-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue City Diesel Shatter / Sugar Wax
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000013034
Metrc Source Pkg#: 1A4010300016E07000013021
Test Conditions

Prepsheet ID#: ORP190311a
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 999 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 115487

Lot #: BCD13021
Batch #: 115487
Batch Weight (g): 1417
Harvest/Process Date: 02/26/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/06/2019
Test Date: 03/08/2019
Sample #115487
Sample #115487 Sample #115487
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Avg
Avg. Amount N/D 2.19 mg/g N/D 3.10 mg/g 5.54 mg/g 32.29 mg/g 58.83 mg/g 802.65 mg/g 4.44 mg/g CBD 1.92 mg/g
LOQ 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g THC 762.75 mg/g
Amount per Serving~ N/D 0.22 mg/srv N/D 0.31 mg/srv 0.55 mg/srv 3.23 mg/srv 5.88 mg/srv 80.27 mg/srv 0.44 mg/srv Serving Size~ (g): 0.10 g
Uncertainty 7.70% RPD 3.20% RPD 7.11% RPD 81.10% RPD 7.94% RPD 4.86% RPD 126.41% RPD 0.60% RPD 71.93% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 115487-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue City Diesel Shatter / Sugar Wax
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000013034
Metrc Source Pkg#: 1A4010300016E07000013021
Test Conditions

Prepsheet ID#: ORP190311a
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 999 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 115487

Lot #: BCD13021
Batch #: 115487
Batch Weight (g): 1417
Harvest/Process Date: 02/26/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/06/2019
Test Date: 03/08/2019
Sample #115487
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 6.52 6.12 93.87 6.61 101.38 7.70%
Cannabidiolic Acid (CBDA) N.D. 6.05 5.58 92.23 5.96 98.51 6.59%
Cannabigerol (CBG) N.D. 6.51 6.08 93.39 6.46 99.23 6.06%
Cannabidiol (CBD) N.D. 6.62 5.97 90.18 6.41 96.83 7.11%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 6.68 6.23 93.26 6.63 99.25 6.22%
Cannabinol (CBN) N.D. 6.89 6.44 93.47 6.83 99.13 5.88%
Δ9-Tetrahydrocannabinol (THC) N.D. 6.91 7.96 115.20 8.55 123.73 7.15%
Cannabichromene (CBC) N.D. 7.64 7.17 93.85 7.48 97.91 4.23%
Tetrahydrocannabinolic acid (THCA) N.D. 6.51 6.07 93.24 6.4 98.31 5.29%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 115487-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue City Diesel Shatter / Sugar Wax
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000013034
Metrc Source Pkg#: 1A4010300016E07000013021
Test Conditions

Prepsheet ID#: ORPS190308a
Scale: Veritas-OR1
Temp: 23.8 °C
Baro PE: 1000 hPa
Analyst: JDM
Technician: JDM
Sample ID#: 115487

Lot #: BCD13021
Batch #: 115487
Batch Weight (g): 1417
Harvest/Process Date: 02/26/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/06/2019
Test Date: 03/09/2019
Sample #115487
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.122 Pass/<LOD Abamectin**** 0.500 0.122 Pass/<LOD
Acephate 0.400 0.122 Pass/<LOD Acequinocyl 2.000 0.244 Pass/<LOD
Acetamiprid 0.200 0.122 Pass/<LOD Azoxystrobin 0.200 0.122 Pass/<LOD
Bifenazate 0.200 0.122 Pass/<LOD Bifenthrin 0.200 0.122 Pass/<LOD
Boscalid 0.400 0.122 Pass/<LOD Carbaryl 0.200 0.122 Pass/<LOD
Carbofuran 0.200 0.122 Pass/<LOD Chlorantraniliprole 0.200 0.122 Pass/<LOD
Chlorfenapyr 1.000 0.489 Pass/<LOD Chlorpyrifos 0.200 0.122 Pass/<LOD
Clofentezine 0.200 0.122 Pass/<LOD Cyfluthrin** 1.000 0.489 Pass/<LOD
Cypermethrin*** 1.000 0.489 Pass/<LOD Daminozide 1.000 0.122 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.244 Pass/<LOD Diazinon 0.200 0.122 Pass/<LOD
Dimethoate 0.200 0.122 Pass/<LOD Ethoprophos 0.200 0.122 Pass/<LOD
Etofenprox 0.400 0.122 Pass/<LOD Etoxazole 0.200 0.122 Pass/<LOD
Fenoxycarb 0.200 0.122 Pass/<LOD Fenpyroximate 0.400 0.122 Pass/<LOD
Fipronil 0.400 0.122 Pass/<LOD Flonicamid 1.000 0.122 Pass/<LOD
Fludioxonil 0.400 0.122 Pass/<LOD Hexythiazox 1.000 0.122 Pass/<LOD
Imazalil 0.200 0.122 Pass/<LOD Imidacloprid 0.400 0.122 Pass/<LOD
Kresoxim Methyl 0.400 0.122 Pass/<LOD Malathion 0.200 0.122 Pass/<LOD
Metalaxyl 0.200 0.122 Pass/<LOD Methiocarb 0.200 0.122 Pass/<LOD
Methomyl 0.400 0.122 Pass/<LOD Methyl Parathion 0.200 0.122 Pass/<LOD
MGK-264‡ 0.200 0.122 Pass/<LOD Myclobutanil 0.000 0.122 Pass/<LOD
Naled 0.500 0.122 Pass/<LOD Oxamyl 1.000 0.122 Pass/<LOD
Paclobutrazol 0.400 0.122 Pass/<LOD Permethrins† 0.200 0.122 Pass/<LOD
Phosmet 0.200 0.122 Pass/<LOD Piperonyl Butoxide 2.000 0.122 Pass/<LOD
Prallethrin 0.200 0.122 Pass/<LOD Propiconazole 0.400 0.122 Pass/<LOD
Propoxur 0.200 0.122 Pass/<LOD Pyrethrins* 1.000 0.122 Pass/<LOD
Pyridaben 0.200 0.122 Pass/<LOD Spinosad***** 0.200 0.122 Pass/<LOD
Spiromesifen 0.200 0.122 Pass/<LOD Spirotetramat 0.200 0.122 Pass/<LOD
Spiroxamine‡ 0.400 0.122 Pass/<LOD Tebuconazole 0.400 0.122 Pass/<LOD
Thiacloprid 0.200 0.122 Pass/<LOD Thiamethoxam 0.200 0.122 Pass/<LOD
Trifloxystrobin 0.200 0.122 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 115487-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue City Diesel Shatter / Sugar Wax
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000013034
Metrc Source Pkg#: 1A4010300016E07000013021
Test Conditions

Prepsheet ID#: ORPS190308a
Scale: Veritas-OR1
Temp: 23.8 °C
Baro PE: 1000 hPa
Analyst: JDM
Technician: JDM
Sample ID#: 115487

Lot #: BCD13021
Batch #: 115487
Batch Weight (g): 1417
Harvest/Process Date: 02/26/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/06/2019
Test Date: 03/09/2019
Sample #115487
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.07 0.996 107.00 99.60 7.16
Acequinocyl N.D. 1 0.24 0.437 24.00 43.70 58.20 LRQ
Acetamiprid N.D. 1 1.08 0.968 108.00 96.80 10.94
Aldicarb N.D. 1 0.984 0.885 98.40 88.50 10.59
Avermectin B1a N.D. 0.97 1.42 1.24 146.39 127.84 13.53 HR
Azoxystrobin N.D. 1 1.25 1.16 125.00 116.00 7.47
Bifenazate N.D. 1 1.1 0.967 110.00 96.70 12.87
Bifenthrin N.D. 1 0.963 0.889 96.30 88.90 7.99
Boscalid N.D. 1 1.23 1.17 123.00 117.00 5.00
Carbaryl N.D. 1 1.14 0.982 114.00 98.20 14.89
Carbofuran N.D. 1 1.22 1.07 122.00 107.00 13.10
Chlorantraniliprole N.D. 1 1.61 1.4 161.00 140.00 13.95 HR
Chlorfenapyr N.D. 1 0.812 0.811 81.20 81.10 0.12
Chlorpyriphos N.D. 1 1.06 0.934 106.00 93.40 12.64
Clofentezine N.D. 1 1.31 1.2 131.00 120.00 8.76 HR
Cyfluthrin N.D. 1 1.11 0.972 111.00 97.20 13.26
Cypermethrin N.D. 1 1.05 0.97 105.00 97.00 7.92
Daminoside N.D. 1 0.731 0.737 73.10 73.70 0.82
Diazanon N.D. 1 1.48 1.26 148.00 126.00 16.06 HR
Dichlorvos N.D. 1 1.15 0.934 115.00 93.40 20.73 Q
Dimethoate N.D. 1 1.12 0.966 112.00 96.60 14.77
Ethoprophos N.D. 1 1.01 0.913 101.00 91.30 10.09
Etofenprox N.D. 1 0.846 0.798 84.60 79.80 5.84
Etoxazole N.D. 1 1.24 1.02 124.00 102.00 19.47
Fenoxycarb N.D. 1 1.64 1.34 164.00 134.00 20.13 HRQ
Fenpyroximate N.D. 1 1.02 0.918 102.00 91.80 10.53
Fipronil N.D. 1 1.13 0.993 113.00 99.30 12.91
Flonicamid N.D. 1 1.06 0.986 106.00 98.60 7.23
Fludioxonil N.D. 1 1.07 0.904 107.00 90.40 16.82
Hexythiazox N.D. 1 0.831 0.815 83.10 81.50 1.94
Imazalil N.D. 1 1.68 1.24 168.00 124.00 30.14 HRQ
Imidacloprid N.D. 1 1.19 1.03 119.00 103.00 14.41
Kresoxim-methyl N.D. 1 1.8 1.52 180.00 152.00 16.87 HR
Malathion N.D. 1 1.42 1.42 142.00 142.00 0.00 HR
Metalaxyl N.D. 1 1.42 1.31 142.00 131.00 8.06 HR
Methiocarb N.D. 1 1.16 0.981 116.00 98.10 16.72
Methomyl N.D. 1 1.4 1.25 140.00 125.00 11.32 HR
MGK-264 N.D. 1 0.909 0.858 90.90 85.80 5.77
Myclobutanil N.D. 1 1.28 1.3 128.00 130.00 1.55
Naled (dibrom) N.D. 1 0.758 0.708 75.80 70.80 6.82
Oxamyl N.D. 1 1.06 0.973 106.00 97.30 8.56
Paclobutrazol N.D. 1 1.59 1.48 159.00 148.00 7.17 HR
Parathion-methyl N.D. 1 0.855 0.897 85.50 89.70 4.79
Permethrins N.D. 1 0.95 0.87 95.00 87.00 8.79
Phosmet N.D. 1 1.57 1.34 157.00 134.00 15.81 HR
Piperonyl butoxide N.D. 1 1.18 1.01 118.00 101.00 15.53
Prallethrin N.D. 1 1.67 1.33 167.00 133.00 22.67 HRQ
Propiconazole N.D. 1 1.44 1.2 144.00 120.00 18.18 HR
Propoxur N.D. 1 1.12 0.926 112.00 92.60 18.96
Pyrethrin N.D. 0.65 0.933 0.764 143.54 117.54 19.92 HR
Pyridaben N.D. 1 0.921 0.865 92.10 86.50 6.27
SpinosynA N.D. 0.84 1.34 1.22 159.52 145.24 9.38 HR
SpinosynD N.D. 0.16 0.263 0.227 164.38 141.88 14.69 HR
Spiromesifen N.D. 1 0.246 0.228 24.60 22.80 7.59 LR
Spirotetramat N.D. 1 1.19 1.04 119.00 104.00 13.45
Spiroxamine N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Tebuconazole N.D. 1 1.65 1.5 165.00 150.00 9.52 HR
Thiacloprid N.D. 1 1.19 1.07 119.00 107.00 10.62
Thiamethoxam N.D. 1 1.52 1.29 152.00 129.00 16.37 HR
Trifloxystrobin N.D. 1 1.17 1.06 117.00 106.00 9.87

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 115487-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue City Diesel Shatter / Sugar Wax
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000013034
Metrc Source Pkg#: 1A4010300016E07000013021
Test Conditions

Prepsheet ID#: ORHS190307a
Scale: XS205-OR1
Temp: 19.4 °C
Baro Pressure: 1008 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 115487

Lot #: BCD13021
Batch #: 115487
Batch Weight (g): 1417
Harvest/Process Date: 02/26/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/06/2019
Test Date: 03/07/2019
Sample #115487
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 50 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 50 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 50 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 5,000 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/57
2-Propanone (Acetone) 50 50 Pass/117 3-Methylpentane (Hexanes) 50 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 1 100 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 6 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 115487-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue City Diesel Shatter / Sugar Wax
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000013034
Metrc Source Pkg#: 1A4010300016E07000013021
Test Conditions

Prepsheet ID#: ORHS190307a
Scale: XS205-OR1
Temp: 19.4 °C
Baro Pressure: 1008 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 115487

Lot #: BCD13021
Batch #: 115487
Batch Weight (g): 1417
Harvest/Process Date: 02/26/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/06/2019
Test Date: 03/07/2019
Sample #115487
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 0 0 0.00 0.00
Isobutane N.D. 250 0 42 0.00 16.80 200.00 Q
Methanol N.D. 250 194 195 77.60 78.00 0.51
n-Butane N.D. 250 45 41 18.00 16.40 9.30
2,2-Dimethylpropane N.D. 250 36 36 14.40 14.40 0.00
Ethanol N.D. 250 187 194 74.80 77.60 3.67
Isopentane N.D. 250 77 73 30.80 29.20 5.33
Acetonitrile N.D. 250 259 250 103.60 100.00 3.54
Diethyl ether N.D. 250 164 163 65.60 65.20 0.61
2-propanone N.D. 250 206 210 82.40 84.00 1.92
2-propanol N.D. 250 227 265 90.80 106.00 15.45
n-Pentane N.D. 250 216 204 86.40 81.60 5.71
2,2-Dimethylbutane N.D. 250 106 107 42.40 42.80 0.94
2,3-Dimethylbutane N.D. 250 129 137 51.60 54.80 6.02
Methylene chloride N.D. 250 200 203 80.00 81.20 1.49
2-Methylpentane N.D. 250 111 114 44.40 45.60 2.67
3-Methylpentane N.D. 250 122 126 48.80 50.40 3.23
2-Butanol N.D. 250 223 230 89.20 92.00 3.09
n-Hexane N.D. 250 138 137 55.20 54.80 0.73
Ethyl acetate N.D. 250 213 217 85.20 86.80 1.86
Tetrahydrofuran N.D. 250 195 199 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 218 225 0.00 0.00 0.00
Benzene N.D. 250 203 204 81.20 81.60 0.49
Chloroform N.D. 250 0 0 0.00 0.00
Cyclohexane N.D. 250 172 175 68.80 70.00 1.73
Ethylene glycol N.D. 250 191 198 76.40 79.20 3.60
Heptane N.D. 250 167 164 66.80 65.60 1.81 Q
2-Ethoxyethanol N.D. 250 218 267 87.20 106.80 20.21
1,4-Dioxane N.D. 250 206 217 82.40 86.80 5.20
Pyridine N.D. 250 0 0 0.00 0.00 0.00
Toluene N.D. 250 205 211 82.00 84.40 2.88
Chlorobenzene N.D. 250 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 218 229 87.20 91.60 4.92
m-Xylene/p-Xylene N.D. 250 443 472 177.20 188.80 6.34
o-Xylene N.D. 250 221 234 88.40 93.60 5.71
Cumene N.D. 250 217 217 86.80 86.80 0.00
Ethylene oxide N.D. 250 169 177 67.60 70.80 4.62

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 115487-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue City Diesel Shatter / Sugar Wax
Type: AU Tincture
Metrc Test Pkg#: 1A4010300016E07000013034
Metrc Source Pkg#: 1A4010300016E07000013021
Sample ID#: 115487

Lot #: BCD13021
Batch #: 115487
Batch Weight (g): 1417
Harvest/Process Date: 02/26/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/06/2019
Sample #115487
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 749.34 1.95 43.29 805.07 2.84 N.D. 1.84 2.22 N.D. 5.32 33.07
Increment 2 776.16 1.89 74.36 800.23 6.03 N.D. 4.35 2.15 N.D. 5.76 31.50
Average Value 762.75 1.92 58.83 802.65 4.44 N.D. 3.10 2.19 N.D. 5.54 32.29
Max Value 776.16 1.95 74.36 805.07 6.03 N.D. 4.35 2.22 N.D. 5.76 33.07
Min Value 749.34 1.89 43.29 800.23 2.84 N.D. 1.84 2.15 N.D. 5.32 31.50
Relative Percent Difference (RPD) ±3.52 ±3.20 ±52.82 ±0.60 ±71.93 N.D. ±81.10 ±3.20 N.D. ±7.94 ±4.86
Average Cannabinoids Per Package 762.75 1.92 58.83 802.65 4.44 N.D. 3.10 2.19 N.D. 5.54 32.29
Average Cannabinoids Per Serving 76.27 0.19 5.88 80.27 0.44 N.D. 0.31 0.22 N.D. 0.55 3.23
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ721
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 7
IRON Laboratories

Oregon Compliant Terpene Report by
Mass Spectrometer
Test Certificate #: 115487-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue City Diesel Shatter / Sugar Wax
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000013034
Metrc Source Pkg#: 1A4010300016E07000013021
Test Conditions

Scale: XS205-OR1
Temp: 19.4 °C
Baro Pressure: 1008 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 115487

Lot #: BCD13021
Batch #: 115487
Batch Weight (g): 1417
Harvest/Process Date: 02/26/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 03/06/2019
Test Date: 03/07/2019
Sample #115487

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.150 %

β-Ocimene:

0.090 %

Camphene:

0.040 %

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

0.020 %

Myrcene:

0.370 %

α-Terpinolene:

0.120 %

β-Pinene:

0.180 %

Linalool:

0.080 %

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

0.040 %

Fenchol:

0.120 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.290 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.600 %

α-Humulene:

0.300 %

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

0.030 %

Caryophyllene Oxide:

0.080 %

α-Bisabolol:

0.180 %

Other Terpenes

Total: 2.690%
a-Phellandrene = 0.14 % a-Terpineol = 0.11 % Valencene = 0.32 %

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 7