IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 114897-001
Client Name, Sample Details

Secrets of Hemp
Columbus , IN 47201
Sample: Alchemy Flower
Type: Flower
Method: FE04U HPLC1100-1
***Moisture: 12.02%

Test Conditions

Prepsheet ID#: MIP190207
Scale: XS205-MI2
Temp: 21.2 °C
Baro PE: 972.5 hPa
Analyst: JRT
Technician: JRT

Sample ID#: 114897

Harvest/Process Date: 02/07/2019
Serving Size (g): 1
Date Received: 02/07/2019
Test Date: 02/07/2019
Valid Through: 02/07/2020

Sample #114897
Sample #114897 Sample #114897
Test
Compounds
THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.1 0.7 0.8 17.0 N/D N/D 0.1 N/D N/D 18.6 0.7 15.6 16.5
Amount (mg/g) 1.1 6.7 7.7 169.6 N/D N/D 1.2 N/D N/D 186.3 6.9 156.4 164.5
Amount per Serving (mg) 1.1 6.7 7.7 169.6 N\D N\D 1.2 N\D N\D 186.3 Serving Size~ (g): 1.0
LOQ (mg/g) 0.97 0.97 0.97 0.97 0.97 0.97 0.97 0.97 0.97   %Decarb. THC CBD
±%RPD 4.4 5.6 1.4 0.3 0.9 1.5 27.3 3.5 2.1 14 4

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refers to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 114897-001
Client Name, Sample Details

Secrets of Hemp
Columbus , IN 47201
Sample: Alchemy Flower
Type: Flower
Method: FE04U HPLC1100-1
***Moisture: 12.02%

Test Conditions

Prepsheet ID#: MIP190207
Scale: XS205-MI2
Temp: 21.2 °C
Baro PE: 972.5 hPa
Analyst: JRT
Technician: JRT

Sample ID#: 114897

Harvest/Process Date: 02/07/2019
Serving Size (g): 1
Date Received: 02/07/2019
Test Date: 02/07/2019
Valid Through: 02/07/2020

Sample #114897
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 2.105244645 2.181369434 103.62 2.226862092 105.78 2.06%
Cannabidiolic Acid (CBDA) 0 5.549747663 5.705474237 102.81 5.720475251 103.08 0.26%
Cannabigerol (CBG) 0 4.127457111 4.324484353 104.77 4.25958151 103.20 1.51%
Cannabidiol (CBD) 0 5.599646848 5.764368074 102.94 5.847773832 104.43 1.44%
Δ9-Tetrahydrocannabivarin (THCV) 0 2.625873227 2.846655883 108.41 2.948299945 112.28 3.51%
Cannabinol (CBN) 0 5.106035397 5.31629672 104.12 5.2680781 103.17 0.91%
Δ9-Tetrahydrocannabinol (THC) 0 6.103615273 7.077892532 115.96 6.776422728 111.02 4.35%
Cannabichromene (CBC) 0 5.601401177 6.854592382 122.37 5.210621208 93.02 27.25% Q
Tetrahydrocannabinolic acid (THCA) 0 5.568353853 6.100481737 109.56 6.448602279 115.81 5.55%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 2