IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 114832-001
Client Name, Sample Details

James Hammonds
Buchanan, NY 10511
Sample: PL2
Type: Concentrate
Method: FE04U HPLC1100-1

Test Conditions

Prepsheet ID#: MIP190204a
Scale: XS205-MI2
Temp: 22.1 °C
Baro PE: 971.6 hPa
Analyst: JRT
Technician: JRT

Sample ID#: 114832

Harvest/Process Date: 02/04/2019
Serving Size (g): 1
Date Received: 02/04/2019
Test Date: 02/04/2019
Valid Through: 02/04/2020

Sample #114832
Sample #114832 Sample #114832
Test
Compounds
THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 2.4 N/D 51.7 0.5 N/D 2.0 3.2 N/D N/D 59.9 2.4 52.2 59.9
Amount (mg/g) 24.4 N/D 517.3 5.2 N/D 20.1 32.2 N/D N/D 599.2 24.4 521.9 598.6
Amount per Serving (mg) 24.4 N\D 517.3 5.2 N\D 20.1 32.2 N\D N\D 599.2 Serving Size~ (g): 1.0
LOQ (mg/g) 3.64 3.64 3.64 3.64 3.64 3.64 3.64 3.64 3.64   %Decarb. THC CBD
±%RPD 2.2 0.5 1.3 3.3 3.6 4.4 7.0 9.6 2.8 100% 99

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refers to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 114832-001
Client Name, Sample Details

James Hammonds
Buchanan, NY 10511
Sample: PL2
Type: Concentrate
Method: FE04U HPLC1100-1

Test Conditions

Prepsheet ID#: MIP190204a
Scale: XS205-MI2
Temp: 22.1 °C
Baro PE: 971.6 hPa
Analyst: JRT
Technician: JRT

Sample ID#: 114832

Harvest/Process Date: 02/04/2019
Serving Size (g): 1
Date Received: 02/04/2019
Test Date: 02/04/2019
Valid Through: 02/04/2020

Sample #114832
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 1.667247422 1.963740192 117.78 1.910505771 114.59 2.75%
Cannabidiolic Acid (CBDA) 0 4.994851699 5.252223936 105.15 5.081940791 101.74 3.30%
Cannabigerol (CBG) 0 3.917289507 3.807840904 97.21 3.645034093 93.05 4.37%
Cannabidiol (CBD) 0 5.318428414 5.207421976 97.91 5.277221695 99.23 1.33%
Δ9-Tetrahydrocannabivarin (THCV) 0 2.758260975 2.426161818 87.96 2.670690164 96.83 9.60%
Cannabinol (CBN) 0 4.915628897 4.752343559 96.68 4.926678057 100.22 3.60%
Δ9-Tetrahydrocannabinol (THC) 0 7.825698955 6.393018509 81.69 6.256466883 79.95 2.16%
Cannabichromene (CBC) 0 4.399167378 3.845649064 87.42 4.125484132 93.78 7.02%
Tetrahydrocannabinolic acid (THCA) 0 5.493778322 5.310254811 96.66 5.335452588 97.12 0.47%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 2