ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 114521-001
Client Name, Sample Details

Black Tie CBD
Myrtle Creek, OR 97457
Sample: Orange Citrus Full Spectrum CBD
License: AG-R1045922IHH
Type: Tincture
Method: FE04E-OR4 HPLC1100-OR1
Test Conditions

Scale: XS205-OR1
Temp: 22.5 °C
Baro Pressure: 1001 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 114521

Lot #: R&D
Batch #: 114521
Harvest/Process Date: 01/16/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 01/17/2019
Test Date: 01/29/2019
Sample #114521
Sample #114521 Sample #114521
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV   AVG CBD Decarb. % THC Decarb. %
Amount 0.30 mg/g 0.19 mg/g 27.30 mg/g 2.46 mg/g 0.53 mg/g 0.13 mg/g 0.99 mg/g N/D N/D THC 0.99 mg/g 99 100%
LOQ 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g CBD 27.47 mg/g - -
Amount per Serving~ 0.03 mg/srv 0.02 mg/srv 2.73 mg/srv 0.25 mg/srv 0.05 mg/srv 0.01 mg/srv 0.10 mg/srv N/D N/D - Serving Size~ (g): 0.10 g -
Uncertainty ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD - - - -

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

THC and CBD Decarb. % referes to the percentage of THC or CBD relative to THCA or CBDA, respectively

Avg. is the calculated average of total CBD or total THC for all increments tested.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 114521-001
Client Name, Sample Details

Black Tie CBD
Myrtle Creek, OR 97457
Sample: Orange Citrus Full Spectrum CBD
License: AG-R1045922IHH
Type: Tincture
Method: SOP FE-44-OR3
Test Conditions

Scale: XS205-OR1
Temp: 19.1 °C
Baro Pressure: 1001 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 114521

Lot #: R&D
Batch #: 114521
Harvest/Process Date: 01/16/2019
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 01/17/2019
Test Date: 01/25/2019
Sample #114521
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 150 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/10,610 Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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