IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Michigan Compliant Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 114248-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Crunchberry Live Resin
License: PR-000014
Type: Tincture
Method: FE04M HPLC1100-1
Metrc Test Pkg#: 1A4050100000BBA000000014
Metrc Source Pkg#: 1A4050100000BBA000000010
Test Conditions

Prepsheet ID#: MIP190110a
Scale: XS205-MI2
Temp: 21.1 °C
Baro Pressure: 988.1 hPa
Analyst: MEH
Technician: JRT
Sample ID#: 114248

Harvest/Process Date: 01/09/2019
Serving Size (g): 1
Date Received: 01/09/2019
Test Date: 01/10/2018
Valid Through: 01/10/2019
Report Issued: 01/11/2019
Sample #114248
Sample #114248 Sample #114248
Test
Compounds		 CBDV* CBDA CBD CBC* CBG* CBN THC THCA THCV*   Calc. Max CBD Decarb. % THC Decarb. %
Amount N/D 33.7 mg/g N/D N/D N/D N/D 23.3 mg/g 789.2 mg/g N/D THC 715.4 mg/g 0% 3
LOQ 3.3 mg/g 3.3 mg/g 3.3 mg/g 3.3 mg/g 3.3 mg/g 3.3 mg/g 3.3 mg/g 3.3 mg/g 3.3 mg/g CBD 29.6 mg/g - -
Amount per Serving~ N/D 33.7 mg/srv N/D N/D N/D N/D 23.3 mg/srv 789.2 mg/srv N/D - Serving Size~ (g): 1.00 g -
Uncertainty 8.04%RSD 1.47%RSD 0.91%RSD 10.80%RSD 0.19%RSD 3.58%RSD ±5%RSD 4.74%RSD 1.51%RSD - - - -

LOQ = Limit of Quantitation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates compounds that are not currently included in Iron Laboratories' accredited scope.

*** Designates tests that use the method FE-45.

Calc. Max is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the CBDA or THCA value.

THC and CBD Decarb. % refers to the percentage of THC or CBD relative to THCA or CBDA, respectively.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 7

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Michigan Compliant QC Report
Testing Accreditation #: 77802 Test Certificate #: 114248-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Crunchberry Live Resin
License: PR-000014
Type: Tincture
Method: FE04M HPLC1100-1
Metrc Test Pkg#: 1A4050100000BBA000000014
Metrc Source Pkg#: 1A4050100000BBA000000010
Test Conditions

Prepsheet ID#: MIP190110a
Scale: XS205-MI2
Temp: 21.1 °C
Baro Pressure: 988.1 hPa
Analyst: MEH
Technician: JRT
Sample ID#: 114248

Harvest/Process Date: 01/09/2019
Serving Size (g): 1
Date Received: 01/09/2019
Test Date: 01/10/2018
Valid Through: 01/10/2019
Report Issued: 01/11/2019
Sample #114248
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N/D 3.19659 3.50297 109.58 3.23221 101.11 8.04%
Cannabidiolic Acid (CBDA) N/D 9.94045 10.1778 102.39 10.0292 100.89 1.47%
Cannabigerol (CBG) N/D 7.05207 7.17999 101.81 7.16646 101.62 0.19%
Cannabidiol (CBD) N/D 9.71216 10.1689 104.70 10.0768 103.75 0.91%
Δ9-Tetrahydrocannabivarin (THCV) N/D 3.65409 3.72238 101.87 3.66648 100.34 1.51%
Cannabinol (CBN) N/D 9.8892 9.74298 98.52 9.40046 95.06 3.58%
Δ9-Tetrahydrocannabinol (THC) N/D 12.734 13.3662 104.96 11.368 89.27 16.16%
Cannabichromene (CBC) N/D 7.3567 7.82833 106.41 7.02622 95.51 10.80%
Tetrahydrocannabinolic acid (THCA) N/D 18.3368 19.3132 105.32 18.4191 100.45 4.74%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 7
IRON Laboratories

Michigan Compliant Pesticide Analysis by
Mass Spectrometer
Test Certificate #: 114248-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Crunchberry Live Resin
License: PR-000014
Type: Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4050100000BBA000000014
Metrc Source Pkg#: 1A4050100000BBA000000010
Test Conditions

Prepsheet ID#: MIPS190110a
Scale: XS205-MI1
Temp: 21.6 °C
Baro PE: 976.1 hPa
Analyst: MEH
Technician: MEH
Sample ID#: 114248

Harvest/Process Date: 01/09/2019
Serving Size (g): 1
Date Received: 01/09/2019
Test Date: 01/11/2018
Valid Through: 01/11/2019
Report Issued: 01/14/2019
Sample #114248
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.126 Pass/<LOD Abamectin**** 0.500 0.126 Pass/<LOD
Acephate 0.400 0.126 Pass/<LOD Acequinocyl 2.000 0.252 Pass/<LOD
Acetamiprid 0.200 0.126 Pass/<LOD Azoxystrobin 0.200 0.126 Pass/<LOD
Bifenazate 0.200 0.126 Pass/<LOD Bifenthrin 0.200 0.126 Pass/<LOD
Boscalid 0.400 0.126 Pass/<LOD Carbaryl 0.200 0.126 Pass/<LOD
Carbofuran 0.200 0.126 Pass/<LOD Chlorantraniliprole 0.200 0.126 Pass/<LOD
Chlorfenapyr 1.000 0.503 Pass/<LOD Chlorpyrifos 0.200 0.126 Pass/<LOD
Clofentezine 0.200 0.126 Pass/<LOD Cyfluthrin** 1.000 0.503 Pass/<LOD
Cypermethrin*** 1.000 0.503 Pass/<LOD Daminozide 1.000 0.503 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.252 Pass/<LOD Diazinon 0.200 0.126 Pass/<LOD
Dimethoate 0.200 0.126 Pass/<LOD Ethoprophos 0.200 0.126 Pass/<LOD
Etofenprox 0.400 0.126 Pass/<LOD Etoxazole 0.200 0.126 Pass/<LOD
Fenoxycarb 0.200 0.126 Pass/<LOD Fenpyroximate 0.400 0.126 Pass/<LOD
Fipronil 0.400 0.126 Pass/<LOD Flonicamid 1.000 0.126 Pass/<LOD
Fludioxonil 0.400 0.126 Pass/<LOD Hexythiazox 1.000 0.126 Pass/<LOD
Imazalil 0.200 0.126 Pass/<LOD Imidacloprid 0.400 0.126 Pass/<LOD
Kresoxim Methyl 0.400 0.126 Pass/<LOD Malathion 0.200 0.126 Pass/<LOD
Metalaxyl 0.200 0.126 Pass/<LOD Methiocarb 0.200 0.126 Pass/<LOD
Methomyl 0.400 0.126 Pass/<LOD Methyl Parathion 0.200 0.126 Pass/<LOD
MGK-264‡ 0.200 0.126 Pass/<LOD Myclobutanil 0.200 0.126 Pass/<LOD
Naled 0.500 0.126 Pass/<LOD Oxamyl 1.000 0.126 Pass/<LOD
Paclobutrazol 0.400 0.126 Pass/<LOD Permethrins† 0.200 0.126 Pass/<LOD
Phosmet 0.200 0.126 Pass/<LOD Piperonyl Butoxide 2.000 1.007 Pass/<LOD
Prallethrin 0.200 0.126 Pass/<LOD Propiconazole 0.400 0.126 Pass/<LOD
Propoxur 0.200 0.126 Pass/<LOD Pyrethrins* 1.000 0.126 Pass/<LOD
Pyridaben 0.200 0.126 Pass/<LOD Spinosad***** 0.200 0.126 Pass/<LOD
Spiromesifen 0.200 0.126 Pass/<LOD Spirotetramat 0.200 0.126 Pass/<LOD
Spiroxamine‡ 0.400 0.126 Pass/<LOD Tebuconazole 0.400 0.126 Pass/<LOD
Thiacloprid 0.200 0.126 Pass/<LOD Thiamethoxam 0.200 0.126 Pass/<LOD
Trifloxystrobin 0.200 0.126 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 7
IRON Laboratories

Michigan Compliant Pesticide QC Report
Test Certificate #: 114248-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Crunchberry Live Resin
License: PR-000014
Type: Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4050100000BBA000000014
Metrc Source Pkg#: 1A4050100000BBA000000010
Test Conditions

Prepsheet ID#: MIPS190110a
Scale: XS205-MI1
Temp: 21.6 °C
Baro PE: 976.1 hPa
Analyst: MEH
Technician: MEH
Sample ID#: 114248

Harvest/Process Date: 01/09/2019
Serving Size (g): 1
Date Received: 01/09/2019
Test Date: 01/11/2018
Valid Through: 01/11/2019
Report Issued: 01/14/2019
Sample #114248
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate 1 1.13 0.963 113.00 96.30 15.96
Acequinocyl 1 0.776 0.813 77.60 81.30 4.66
Acetamiprid 1 1.17 1.1 117.00 110.00 6.17
Aldicarb 1 1.19 1.09 119.00 109.00 8.77
Avermectin B1a 0.97 1.09 0.946 112.37 97.53 14.15
Azoxystrobin 1 1.09 0.955 109.00 95.50 13.20
Bifenazate 1 0.149 0.553 14.90 55.30 115.10
Bifenthrin 1 0.805 0.826 80.50 82.60 2.58
Boscalid 1 1.03 1.07 103.00 107.00 3.81
Carbaryl 1 1.14 1.1 114.00 110.00 3.57
Carbofuran 1 1.18 1.08 118.00 108.00 8.85
Chlorantraniliprole 1 0.995 0.983 99.50 98.30 1.21
Chlorfenapyr 1 1.19 1.09 119.00 109.00 8.77
Chlorpyriphos 1 0.93 0.936 93.00 93.60 0.64
Clofentezine 1 0.837 0.832 83.70 83.20 0.60
Cyfluthrin 1 1.11 0.988 111.00 98.80 11.63
Cypermethrin 1 1.1 1.12 110.00 112.00 1.80
Daminoside 1 0.9 0.963 90.00 96.30 6.76
Diazanon 1 0.928 0.939 92.80 93.90 1.18
Dichlorvos 1 1.01 0.907 101.00 90.70 10.75
Dimethoate 1 1.09 0.988 109.00 98.80 9.82
Ethoprophos 1 1.02 0.931 102.00 93.10 9.12
Etofenprox 1 0.785 0.819 78.50 81.90 4.24
Etoxazole 1 1.08 1.02 108.00 102.00 5.71
Fenoxycarb 1 1.02 1.06 102.00 106.00 3.85
Fenpyroximate 1 0.941 0.931 94.10 93.10 1.07
Fipronil 1 1.29 1.14 129.00 114.00 12.35
Flonicamid 1 1.19 1.02 119.00 102.00 15.38
Fludioxonil 1 1.22 1.14 122.00 114.00 6.78
Hexythiazox 1 0.868 0.894 86.80 89.40 2.95
Imazalil 1 1.18 1.12 118.00 112.00 5.22
Imidacloprid 1 1.29 1.11 129.00 111.00 15.00
Kresoxim-methyl 1 0.935 0.885 93.50 88.50 5.49
Malathion 1 1 1.07 100.00 107.00 6.76
Metalaxyl 1 1.08 1.24 108.00 124.00 13.79
Methiocarb 1 1.07 1.14 107.00 114.00 6.33
Methomyl 1 1.15 1.07 115.00 107.00 7.21
MGK-264 1 0.767 0.871 76.70 87.10 12.70
Myclobutanil 1 1.07 0.973 107.00 97.30 9.50
Naled (dibrom) 1 0.953 1.02 95.30 102.00 6.79
Oxamyl 1 1.09 1.03 109.00 103.00 5.66
Paclobutrazol 1 1.1 1.12 110.00 112.00 1.80
Parathion-methyl 1 0.966 0.914 96.60 91.40 5.53
Permethrins 1 0.783 0.767 78.30 76.70 2.06
Phosmet 1 1.12 1.06 112.00 106.00 5.50
Piperonyl butoxide 1 0.942 0.836 94.20 83.60 11.92
Prallethrin 1 1.02 0.986 102.00 98.60 3.39
Propiconazole 1 1.04 0.912 104.00 91.20 13.11
Propoxur 1 1.16 1.08 116.00 108.00 7.14
Pyrethrin 0.65 0.675 0.671 103.85 103.23 0.59
Pyridaben 1 0.89 0.853 89.00 85.30 4.25
SpinosynA 0.84 0.954 0.84 113.57 100.00 12.71
SpinosynD 0.16 0.17 0.168 106.25 105.00 1.18
Spiromesifen 1 1.07 0.96 107.00 96.00 10.84
Spirotetramat 1 1.04 1.05 104.00 105.00 0.96
Spiroxamine 1 1.18 1.07 118.00 107.00 9.78
Tebuconazole 1 0.95 0.999 95.00 99.90 5.03
Thiacloprid 1 1.14 1.15 114.00 115.00 0.87
Thiamethoxam 1 1.2 1.13 120.00 113.00 6.01
Trifloxystrobin 1 1.06 0.941 106.00 94.10 11.89

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 7
IRON Laboratories

Michigan Compliant Residual Solvents Analysis by
Mass Spectrometer
Test Certificate #: 114248-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Crunchberry Live Resin
License: PR-000014
Type: Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4050100000BBA000000014
Metrc Source Pkg#: 1A4050100000BBA000000010
Test Conditions

Prepsheet ID#: MIHS190116a
Scale: XS205-MI2
Temp: 20 °C
Baro PE: 990 hPa
Analyst: MEH
Technician: JRT
Sample ID#: 114248

Harvest/Process Date: 01/09/2019
Serving Size (g): 1
Date Received: 01/09/2019
Test Date: 01/16/2019
Valid Through: 01/16/2020
Report Issued: 01/21/2019
Sample #114248
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 50 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/164 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 50 Pass/98 Chloroform 1 100 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 150 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 50 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 200 160 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 6 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total PPM: 262.00
* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 7
IRON Laboratories

Michigan Compliant Residual Solvents QC Report
Test Certificate #: 114248-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Crunchberry Live Resin
License: PR-000014
Type: Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4050100000BBA000000014
Metrc Source Pkg#: 1A4050100000BBA000000010
Test Conditions

Prepsheet ID#: MIHS190116a
Scale: XS205-MI2
Temp: 20 °C
Baro PE: 990 hPa
Analyst: MEH
Technician: JRT
Sample ID#: 114248

Harvest/Process Date: 01/09/2019
Serving Size (g): 1
Date Received: 01/09/2019
Test Date: 01/16/2019
Valid Through: 01/16/2020
Report Issued: 01/21/2019
Sample #114248
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 241 252 96.40 100.80 4.46
Isobutane N.D. 250 239 250 95.60 100.00 4.50
Methanol N.D. 250 227 237 90.80 94.80 4.31
n-Butane N.D. 250 249 264 99.60 105.60 5.85
2,2-Dimethylpropane N.D. 0 0 0 nan nan
Ethanol N.D. 250 264 252 105.60 100.80 4.65
Isopentane N.D. 250 250 250 100.00 100.00 0.00
Acetonitrile N.D. 250 230 224 92.00 89.60 2.64
Diethyl ether N.D. 250 254 252 101.60 100.80 0.79
2-propanone N.D. 250 237 268 94.80 107.20 12.28
2-propanol N.D. 250 255 250 102.00 100.00 1.98
n-Pentane N.D. 250 252 260 100.80 104.00 3.13
2,2-Dimethylbutane N.D. 250 248 245 99.20 98.00 1.22
2,3-Dimethylbutane N.D. 250 251 258 100.40 103.20 2.75
Methylene chloride N.D. 250 251 246 100.40 98.40 2.01
2-Methylpentane N.D. 250 246 250 98.40 100.00 1.61
3-Methylpentane N.D. 250 254 250 101.60 100.00 1.59
2-Butanol N.D. 250 256 246 102.40 98.40 3.98
n-Hexane N.D. 250 250 255 100.00 102.00 1.98
Ethyl acetate N.D. 250 246 236 98.40 94.40 4.15
Tetrahydrofuran N.D. 250 259 252 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 261 254 0.00 0.00 0.00
Benzene N.D. 250 246 237 98.40 94.80 3.73
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 256 254 102.40 101.60 0.78
Ethylene glycol N.D. 250 272 269 108.80 107.60 1.11
Heptane N.D. 250 249 248 99.60 99.20 0.40
2-Ethoxyethanol N.D. 250 253 236 101.20 94.40 6.95
1,4-Dioxane N.D. 250 249 238 99.60 95.20 4.52
Pyridine N.D. 250 246 240 98.40 96.00 0.00
Toluene N.D. 250 248 239 99.20 95.60 3.70
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 248 236 99.20 94.40 4.96
m-Xylene/p-Xylene N.D. 500 487 472 97.40 94.40 3.13
o-Xylene N.D. 250 248 236 99.20 94.40 4.96
Cumene N.D. 250 243 231 97.20 92.40 5.06
Ethylene oxide N.D. 0 0 0 0.00 0.00 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 7
IRON Laboratories

Michigan Compliant Terpene Report by
Mass Spectrometer
Test Certificate #: 114248-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Crunchberry Live Resin
License: PR-000014
Type: Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4050100000BBA000000014
Metrc Source Pkg#: 1A4050100000BBA000000010
Test Conditions

Scale: XS205-MI2
Temp: 20 °C
Baro Pressure: 990 hPa
Analyst: JER
Technician: JRT
Sample ID#: 114248

Harvest/Process Date: 01/09/2019
Serving Size (g): 1
Date Received: 01/09/2019
Test Date: 01/16/2019
Valid Through: 01/16/2020
Report Issued: 01/21/2019
Sample #114248

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.110 %

β-Ocimene:

0.040 %

Camphene:

0.020 %

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

0.020 %

Myrcene:

0.680 %

α-Terpinolene:

0.320 %

β-Pinene:

0.060 %

Linalool:

0.360 %

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.580 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

1.330 %

α-Humulene:

0.260 %

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

0.020 %

Other Terpenes

Total: 3.800%
#NAME?

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 6 of 7
IRON Laboratories

Michigan Compliant Heavy Metals Analysis
Test Certificate #: 114248-001
Client Name, Sample Details

HumbleBee PR-000014
Frederic, MI 49733
Sample: Crunchberry Live Resin
License: PR-000014
Type: Tincture
Method: FE60 ICPMS-MI
Metrc Test Pkg#: 1A4050100000BBA000000014
Metrc Source Pkg#: 1A4050100000BBA000000010
Test Conditions

Analyst: JER
Technician: MEH
Sample ID#: 114248

Harvest/Process Date: 01/09/2019
Serving Size (g): 1
Date Received: 01/09/2019
Report Issued: 01/25/2019
Sample #114248
Sample #114248 Sample #114248
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Arsenic 0.2 0.04 Pass/<LOD
Copper Not Tested
Cadmium 0.2 0.04 Pass/<LOD
Chromium 0.6 0.1 Pass/<LOD
Lead 0.5 0.05 Pass/<LOD
Mercury 0.1 0.05 Pass/<LOD
Nickel Not Tested

MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 7 of 7