IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Michigan Compliant Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 113995-001
Client Name, Sample Details

Breedsville Provisioning Center
Breedsville, MI 49027
Sample: Gelato
License: pc-000139
Type: Flower
Method: FE04M HPLC1100-1
Metrc Test Pkg#: 1A405010000089A000000124
***Water Activity: 0.51
***Moisture: 13.06%

Test Conditions

Prepsheet ID#: MIP181228a
Scale: XS205-MI2
Temp: 21.7 °C
Baro Pressure: 969.5 hPa
Analyst: MEH
Technician: JRT

Sample ID#: 113995

Harvest/Process Date: 12/21/2018
Serving Size (g): 1
Date Received: 12/21/2018
Test Date: 12/28/2018
Valid Through: 12/28/2019
Report Issued: 12/31/2018

Sample #113995
Sample #113995 Sample #113995
Test
Compounds
CBDV* CBDA CBD CBC* CBG* CBN THC THCA THCV*   Calc. Max CBD Decarb. % THC Decarb. %
Amount N/D 8.3 mg/g N/D N/D N/D N/D 8.9 mg/g 171.0 mg/g N/D THC 158.9 mg/g 0% 5
LOQ 1 mg/g 1 mg/g 1 mg/g 1 mg/g 1 mg/g 1 mg/g 1 mg/g 1 mg/g 1 mg/g CBD 7.3 mg/g - -
Amount per Serving~ N/D 8.3 mg/srv N/D N/D N/D N/D 8.9 mg/srv 171.0 mg/srv N/D - Serving Size~ (g): 1.00 g -
Uncertainty 1.13%RSD 0.57%RSD 0.24%RSD 0.36%RSD 0.49%RSD 0.06%RSD ±5%RSD 1.12%RSD 9.66%RSD - - - -

LOQ = Limit of Quantitation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates compounds that are not currently included in Iron Laboratories' accredited scope.

*** Designates tests that use the method FE-45.

Calc. Max is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the CBDA or THCA value.

THC and CBD Decarb. % refers to the percentage of THC or CBD relative to THCA or CBDA, respectively.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 8

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Michigan Compliant QC Report

Testing Accreditation #: 77802 Test Certificate #: 113995-001
Client Name, Sample Details

Breedsville Provisioning Center
Breedsville, MI 49027
Sample: Gelato
License: pc-000139
Type: Flower
Method: FE04M HPLC1100-1
Metrc Test Pkg#: 1A405010000089A000000124
***Water Activity: 0.51
***Moisture: 13.06%

Test Conditions

Prepsheet ID#: MIP181228a
Scale: XS205-MI2
Temp: 21.7 °C
Baro Pressure: 969.5 hPa
Analyst: MEH
Technician: JRT

Sample ID#: 113995

Harvest/Process Date: 12/21/2018
Serving Size (g): 1
Date Received: 12/21/2018
Test Date: 12/28/2018
Valid Through: 12/28/2019
Report Issued: 12/31/2018

Sample #113995
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N/D 6.9507 7.01279 100.89 6.93382 99.76 1.13%
Cannabidiolic Acid (CBDA) N/D 8.07232 8.12779 100.69 8.17456 101.27 0.57%
Cannabigerol (CBG) N/D 0.951048 0.875657 92.07 0.87994 92.52 0.49%
Cannabidiol (CBD) N/D 4.23346 4.23349 100.00 4.24381 100.24 0.24%
Δ9-Tetrahydrocannabivarin (THCV) N/D 0.327878 0.278163 84.84 0.306404 93.45 9.66%
Cannabinol (CBN) N/D 9.79469 9.812 100.18 9.81752 100.23 0.06%
Δ9-Tetrahydrocannabinol (THC) N/D 11.1065 11.2745 101.51 11.0965 99.91 1.59%
Cannabichromene (CBC) N/D 10.0814 10.1853 101.03 10.1483 100.66 0.36%
Tetrahydrocannabinolic acid (THCA) N/D 6.77569 6.55205 96.70 6.62576 97.79 1.12%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 8

IRON Laboratories

Michigan Compliant Pesticide Analysis by
Mass Spectrometer

Test Certificate #: 113995-001
Client Name, Sample Details

Breedsville Provisioning Center
Breedsville, MI 49027
Sample: Gelato
License: pc-000139
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A405010000089A000000124

Test Conditions

Prepsheet ID#: MIPS181227a
Scale: XS205-MI1
Temp: 21.6 °C
Baro PE: 976.1 hPa
Analyst: MEH
Technician: MEH

Sample ID#: 113995

Harvest/Process Date: 12/21/2018
Serving Size (g): 1
Date Received: 12/21/2018
Test Date: 12/28/2018
Valid Through: 12/28/2019
Report Issued: 12/28/2018

Sample #113995
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.119 Pass/<LOD Abamectin**** 0.500 0.119 Failed/2.054
Acephate 0.400 0.119 Pass/<LOD Acequinocyl 2.000 0.238 Pass/<LOD
Acetamiprid 0.200 0.119 Pass/<LOD Azoxystrobin 0.200 0.119 Pass/<LOD
Bifenazate 0.200 0.119 Pass/<LOD Bifenthrin 0.200 0.119 Pass/<LOD
Boscalid 0.400 0.119 Pass/<LOD Carbaryl 0.200 0.119 Pass/<LOD
Carbofuran 0.200 0.119 Pass/<LOD Chlorantraniliprole 0.200 0.119 Pass/<LOD
Chlorfenapyr 1.000 0.477 Pass/<LOD Chlorpyrifos 0.200 0.119 Pass/<LOD
Clofentezine 0.200 0.119 Pass/<LOD Cyfluthrin** 1.000 0.477 Pass/<LOD
Cypermethrin*** 1.000 0.477 Pass/<LOD Daminozide 1.000 0.477 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.238 Pass/<LOD Diazinon 0.200 0.119 Pass/<LOD
Dimethoate 0.200 0.119 Pass/<LOD Ethoprophos 0.200 0.119 Pass/<LOD
Etofenprox 0.400 0.119 Pass/<LOD Etoxazole 0.200 0.119 Pass/<LOD
Fenoxycarb 0.200 0.119 Pass/<LOD Fenpyroximate 0.400 0.119 Pass/<LOD
Fipronil 0.400 0.119 Pass/<LOD Flonicamid 1.000 0.119 Pass/<LOD
Fludioxonil 0.400 0.119 Pass/<LOD Hexythiazox 1.000 0.119 Pass/<LOD
Imazalil 0.200 0.119 Pass/<LOD Imidacloprid 0.400 0.119 Pass/<LOD
Kresoxim Methyl 0.400 0.119 Pass/<LOD Malathion 0.200 0.119 Failed/93.691
Metalaxyl 0.200 0.119 Pass/<LOD Methiocarb 0.200 0.119 Pass/<LOD
Methomyl 0.400 0.119 Pass/<LOD Methyl Parathion 0.200 0.119 Pass/<LOD
MGK-264‡ 0.200 0.119 Pass/<LOD Myclobutanil 0.200 0.119 Pass/<LOD
Naled 0.500 0.119 Pass/<LOD Oxamyl 1.000 0.119 Pass/<LOD
Paclobutrazol 0.400 0.119 Pass/<LOD Permethrins† 0.200 0.119 Pass/<LOD
Phosmet 0.200 0.119 Pass/<LOD Piperonyl Butoxide 2.000 0.954 Pass/<LOD
Prallethrin 0.200 0.119 Pass/<LOD Propiconazole 0.400 0.119 Pass/<LOD
Propoxur 0.200 0.119 Pass/<LOD Pyrethrins* 1.000 0.119 Pass/<LOD
Pyridaben 0.200 0.119 Pass/<LOD Spinosad***** 0.200 0.119 Pass/<LOD
Spiromesifen 0.200 0.119 Pass/<LOD Spirotetramat 0.200 0.119 Pass/<LOD
Spiroxamine‡ 0.400 0.119 Pass/<LOD Tebuconazole 0.400 0.119 Pass/<LOD
Thiacloprid 0.200 0.119 Pass/<LOD Thiamethoxam 0.200 0.119 Pass/<LOD
Trifloxystrobin 0.200 0.119 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 8

IRON Laboratories

Michigan Compliant Pesticide QC Report

Test Certificate #: 113995-001
Client Name, Sample Details

Breedsville Provisioning Center
Breedsville, MI 49027
Sample: Gelato
License: pc-000139
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A405010000089A000000124

Test Conditions

Prepsheet ID#: MIPS181227a
Scale: XS205-MI1
Temp: 21.6 °C
Baro PE: 976.1 hPa
Analyst: MEH
Technician: MEH

Sample ID#: 113995

Harvest/Process Date: 12/21/2018
Serving Size (g): 1
Date Received: 12/21/2018
Test Date: 12/28/2018
Valid Through: 12/28/2019
Report Issued: 12/28/2018

Sample #113995
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.988 0.904 98.80 90.40 8.88
Acequinocyl N.D. 1 0.973 0.914 97.30 91.40 6.25
Acetamiprid N.D. 1 1.23 1.13 123.00 113.00 8.47
Aldicarb N.D. 1 1.22 1.2 122.00 120.00 1.65
Avermectin B1a N.D. 0.97 1.1 1.06 113.40 109.28 3.70
Azoxystrobin N.D. 1 1.27 1.22 127.00 122.00 4.02
Bifenazate N.D. 1 0.966 0.988 96.60 98.80 2.25
Bifenthrin N.D. 1 1.24 1.21 124.00 121.00 2.45
Boscalid N.D. 1 1.14 1.14 114.00 114.00 0.00
Carbaryl N.D. 1 1.18 1.09 118.00 109.00 7.93
Carbofuran N.D. 1 1.18 1.05 118.00 105.00 11.66
Chlorantraniliprole N.D. 1 1.18 1.13 118.00 113.00 4.33
Chlorfenapyr N.D. 1 1.26 1.16 126.00 116.00 8.26
Chlorpyriphos N.D. 1 1.26 1.15 126.00 115.00 9.13
Clofentezine N.D. 1 1.22 1.29 122.00 129.00 5.58
Cyfluthrin N.D. 1 0.878 0.872 87.80 87.20 0.69
Cypermethrin N.D. 1 1.07 1.08 107.00 108.00 0.93
Daminoside N.D. 1 0.91 0.872 91.00 87.20 4.26
Diazanon N.D. 1 3.77 3.56 377.00 356.00 5.73 HR
Dichlorvos N.D. 1 1.29 1.19 129.00 119.00 8.06
Dimethoate N.D. 1 1.11 1.08 111.00 108.00 2.74
Ethoprophos N.D. 1 1.13 1.16 113.00 116.00 2.62
Etofenprox N.D. 1 1.82 1.58 182.00 158.00 14.12 HR
Etoxazole N.D. 1 1.82 1.78 182.00 178.00 2.22 HR
Fenoxycarb N.D. 1 1.23 1.26 123.00 126.00 2.41
Fenpyroximate N.D. 1 1.28 1.23 128.00 123.00 3.98
Fipronil N.D. 1 1.22 1.23 122.00 123.00 0.82
Flonicamid N.D. 1 1.13 1.03 113.00 103.00 9.26
Fludioxonil N.D. 1 0.98 1.11 98.00 111.00 12.44
Hexythiazox N.D. 1 1.17 1.16 117.00 116.00 0.86
Imazalil N.D. 1 0.942 0.865 94.20 86.50 8.52
Imidacloprid N.D. 1 1.18 1.24 118.00 124.00 4.96
Kresoxim-methyl N.D. 1 1.2 1.15 120.00 115.00 4.26
Malathion N.D. 1 1.2 1.2 120.00 120.00 0.00
Metalaxyl N.D. 1 1.78 1.77 178.00 177.00 0.56 HR
Methiocarb N.D. 1 1.67 1.63 167.00 163.00 2.42 HR
Methomyl N.D. 1 1.13 1.03 113.00 103.00 9.26
MGK-264 N.D. 1 1.13 1.18 113.00 118.00 4.33
Myclobutanil N.D. 1 1.21 1.12 121.00 112.00 7.73
Naled (dibrom) N.D. 1 0.935 0.905 93.50 90.50 3.26
Oxamyl N.D. 1 0.901 1.03 90.10 103.00 13.36
Paclobutrazol N.D. 1 1.1 1.03 110.00 103.00 6.57
Parathion-methyl N.D. 1 1.19 1.27 119.00 127.00 6.50
Permethrins N.D. 1 1.27 1.26 127.00 126.00 0.79
Phosmet N.D. 1 1.23 1.23 123.00 123.00 0.00
Piperonyl butoxide N.D. 1 1.15 1.13 115.00 113.00 1.75
Prallethrin N.D. 1 1.22 1.18 122.00 118.00 3.33
Propiconazole N.D. 1 1.15 1.03 115.00 103.00 11.01
Propoxur N.D. 1 1.17 1.08 117.00 108.00 8.00
Pyrethrin N.D. 0.65 0.771 0.819 118.62 126.00 6.04
Pyridaben N.D. 1 1.24 1.17 124.00 117.00 5.81
SpinosynA N.D. 0.84 0.864 0.843 102.86 100.36 2.46
SpinosynD N.D. 0.16 0.181 0.169 113.13 105.63 6.86
Spiromesifen N.D. 1 0.295 0.293 29.50 29.30 0.68 LR
Spirotetramat N.D. 1 1.16 1.15 116.00 115.00 0.87
Spiroxamine N.D. 1 0.974 0.973 97.40 97.30 0.10
Tebuconazole N.D. 1 1.21 1.22 121.00 122.00 0.82
Thiacloprid N.D. 1 1.13 1.1 113.00 110.00 2.69
Thiamethoxam N.D. 1 1.07 1 107.00 100.00 6.76
Trifloxystrobin N.D. 1 1.25 1.16 125.00 116.00 7.47

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 8

IRON Laboratories

Michigan Compliant Pesticide Analysis by
Mass Spectrometer

Test Certificate #: 113995-001
Client Name, Sample Details

Breedsville Provisioning Center
Breedsville, MI 49027
Sample: Gelato
License: pc-000139
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A405010000089A000000124

Test Conditions

Prepsheet ID#: MIPS190108a
Scale: XS205-MI1
Temp: 21.6 °C
Baro PE: 976.1 hPa
Analyst: MEH
Technician: MEH

Sample ID#: 113995

Harvest/Process Date: 12/21/2018
Serving Size (g): 1
Date Received: 12/21/2018
Test Date: 01/09/2018
Valid Through: 01/09/2019
Report Issued: 01/11/2019

Sample #113995
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.123 Pass/<LOD Abamectin**** 0.500 0.123 Failed/1.499
Acephate 0.400 0.123 Pass/<LOD Acequinocyl 2.000 0.245 Pass/<LOD
Acetamiprid 0.200 0.123 Pass/<LOD Azoxystrobin 0.200 0.123 Pass/<LOD
Bifenazate 0.200 0.123 Pass/<LOD Bifenthrin 0.200 0.123 Pass/<LOD
Boscalid 0.400 0.123 Pass/<LOD Carbaryl 0.200 0.123 Pass/<LOD
Carbofuran 0.200 0.123 Pass/<LOD Chlorantraniliprole 0.200 0.123 Pass/<LOD
Chlorfenapyr 1.000 0.490 Pass/<LOD Chlorpyrifos 0.200 0.123 Pass/<LOD
Clofentezine 0.200 0.123 Pass/<LOD Cyfluthrin** 1.000 0.490 Pass/<LOD
Cypermethrin*** 1.000 0.490 Pass/<LOD Daminozide 1.000 0.490 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.245 Pass/<LOD Diazinon 0.200 0.123 Pass/<LOD
Dimethoate 0.200 0.123 Pass/<LOD Ethoprophos 0.200 0.123 Pass/<LOD
Etofenprox 0.400 0.123 Pass/<LOD Etoxazole 0.200 0.123 Pass/<LOD
Fenoxycarb 0.200 0.123 Pass/<LOD Fenpyroximate 0.400 0.123 Pass/<LOD
Fipronil 0.400 0.123 Pass/<LOD Flonicamid 1.000 0.123 Pass/<LOD
Fludioxonil 0.400 0.123 Pass/<LOD Hexythiazox 1.000 0.123 Pass/<LOD
Imazalil 0.200 0.123 Pass/<LOD Imidacloprid 0.400 0.123 Pass/<LOD
Kresoxim Methyl 0.400 0.123 Pass/<LOD Malathion 0.200 0.123 Failed/73.644
Metalaxyl 0.200 0.123 Pass/<LOD Methiocarb 0.200 0.123 Pass/<LOD
Methomyl 0.400 0.123 Pass/<LOD Methyl Parathion 0.200 0.123 Pass/<LOD
MGK-264‡ 0.200 0.123 Pass/<LOD Myclobutanil 0.200 0.123 Pass/<LOD
Naled 0.500 0.123 Pass/<LOD Oxamyl 1.000 0.123 Pass/<LOD
Paclobutrazol 0.400 0.123 Pass/<LOD Permethrins† 0.200 0.123 Pass/<LOD
Phosmet 0.200 0.123 Pass/<LOD Piperonyl Butoxide 2.000 0.981 Pass/<LOD
Prallethrin 0.200 0.123 Pass/<LOD Propiconazole 0.400 0.123 Pass/<LOD
Propoxur 0.200 0.123 Pass/<LOD Pyrethrins* 1.000 0.123 Pass/<LOD
Pyridaben 0.200 0.123 Pass/<LOD Spinosad***** 0.200 0.123 Pass/<LOD
Spiromesifen 0.200 0.123 Pass/<LOD Spirotetramat 0.200 0.123 Pass/<LOD
Spiroxamine‡ 0.400 0.123 Pass/<LOD Tebuconazole 0.400 0.123 Pass/<LOD
Thiacloprid 0.200 0.123 Pass/<LOD Thiamethoxam 0.200 0.123 Pass/<LOD
Trifloxystrobin 0.200 0.123 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 8

IRON Laboratories

Michigan Compliant Pesticide QC Report

Test Certificate #: 113995-001
Client Name, Sample Details

Breedsville Provisioning Center
Breedsville, MI 49027
Sample: Gelato
License: pc-000139
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A405010000089A000000124

Test Conditions

Prepsheet ID#: MIPS190108a
Scale: XS205-MI1
Temp: 21.6 °C
Baro PE: 976.1 hPa
Analyst: MEH
Technician: MEH

Sample ID#: 113995

Harvest/Process Date: 12/21/2018
Serving Size (g): 1
Date Received: 12/21/2018
Test Date: 01/09/2018
Valid Through: 01/09/2019
Report Issued: 01/11/2019

Sample #113995
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.02 1.17 102.00 117.00 13.70
Acequinocyl N.D. 1 0.85 0.795 85.00 79.50 6.69
Acetamiprid N.D. 1 1.02 1.08 102.00 108.00 5.71
Aldicarb N.D. 1 1.15 1.17 115.00 117.00 1.72
Avermectin B1a N.D. 0.97 0.967 0.984 99.69 101.44 1.74
Azoxystrobin N.D. 1 1.26 1.17 126.00 117.00 7.41
Bifenazate N.D. 1 0.94 0.852 94.00 85.20 9.82
Bifenthrin N.D. 1 1.25 1.23 125.00 123.00 1.61
Boscalid N.D. 1 2.01 1.53 201.00 153.00 27.12 HRQ
Carbaryl N.D. 1 1.14 1.16 114.00 116.00 1.74
Carbofuran N.D. 1 1.42 1.39 142.00 139.00 2.14 HR
Chlorantraniliprole N.D. 1 1.25 1.15 125.00 115.00 8.33
Chlorfenapyr N.D. 1 1.14 1.26 114.00 126.00 10.00
Chlorpyriphos N.D. 1 1.58 1.44 158.00 144.00 9.27 HR
Clofentezine N.D. 1 1.28 1.27 128.00 127.00 0.78
Cyfluthrin N.D. 1 1.06 1.05 106.00 105.00 0.95
Cypermethrin N.D. 1 0.865 0.845 86.50 84.50 2.34
Daminoside N.D. 1 0.736 0.738 73.60 73.80 0.27
Diazanon N.D. 1 4.17 3.24 417.00 324.00 25.10 HRQ
Dichlorvos N.D. 1 1.18 1.24 118.00 124.00 4.96
Dimethoate N.D. 1 1.15 1.02 115.00 102.00 11.98
Ethoprophos N.D. 1 1.22 1.2 122.00 120.00 1.65
Etofenprox N.D. 1 1.89 1.4 189.00 140.00 29.79 HRQ
Etoxazole N.D. 1 1.64 1.49 164.00 149.00 9.58 HR
Fenoxycarb N.D. 1 1.39 1.38 139.00 138.00 0.72 HR
Fenpyroximate N.D. 1 1.14 1.09 114.00 109.00 4.48
Fipronil N.D. 1 1.05 1.02 105.00 102.00 2.90
Flonicamid N.D. 1 1.26 1.14 126.00 114.00 10.00
Fludioxonil N.D. 1 1.13 1.02 113.00 102.00 10.23
Hexythiazox N.D. 1 1.24 1.15 124.00 115.00 7.53
Imazalil N.D. 1 0.929 0.898 92.90 89.80 3.39
Imidacloprid N.D. 1 1.21 1.2 121.00 120.00 0.83
Kresoxim-methyl N.D. 1 1.07 1.22 107.00 122.00 13.10
Malathion N.D. 1 1.84 1.36 184.00 136.00 30.00 HRQ
Metalaxyl N.D. 1 1.23 1.25 123.00 125.00 1.61
Methiocarb N.D. 1 1.47 1.33 147.00 133.00 10.00 HR
Methomyl N.D. 1 1.17 1.01 117.00 101.00 14.68
MGK-264 N.D. 1 1.24 1.25 124.00 125.00 0.80
Myclobutanil N.D. 1 1.22 1.12 122.00 112.00 8.55
Naled (dibrom) N.D. 1 0.82 0.782 82.00 78.20 4.74
Oxamyl N.D. 1 1.11 1.17 111.00 117.00 5.26
Paclobutrazol N.D. 1 1.24 1.13 124.00 113.00 9.28
Parathion-methyl N.D. 1 1.27 1.12 127.00 112.00 12.55
Permethrins N.D. 1 2.07 1.51 207.00 151.00 31.28 HRQ
Phosmet N.D. 1 1.29 1.21 129.00 121.00 6.40
Piperonyl butoxide N.D. 1 1.18 1.27 118.00 127.00 7.35
Prallethrin N.D. 1 1.2 1.05 120.00 105.00 13.33
Propiconazole N.D. 1 1.07 1.01 107.00 101.00 5.77
Propoxur N.D. 1 1.24 1.18 124.00 118.00 4.96
Pyrethrin N.D. 0.65 0.834 0.83 128.31 127.69 0.48
Pyridaben N.D. 1 1.19 1.24 119.00 124.00 4.12
SpinosynA N.D. 0.84 0.958 0.985 114.05 117.26 2.78
SpinosynD N.D. 0.16 0.205 0.198 128.13 123.75 3.47
Spiromesifen N.D. 1 0.272 0.245 27.20 24.50 10.44 LR
Spirotetramat N.D. 1 1.17 1.22 117.00 122.00 4.18
Spiroxamine N.D. 1 1.07 1.1 107.00 110.00 2.76
Tebuconazole N.D. 1 1.8 1.32 180.00 132.00 30.77 HRQ
Thiacloprid N.D. 1 1.18 1.08 118.00 108.00 8.85
Thiamethoxam N.D. 1 1.17 1.08 117.00 108.00 8.00
Trifloxystrobin N.D. 1 1.94 1.38 194.00 138.00 33.73 HRQ

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 8

IRON Laboratories

Michigan Compliant Microbiology Analysis

Test Certificate #: 113995-001
Client Name, Sample Details

Breedsville Provisioning Center
Breedsville, MI 49027
Sample: Gelato
License: pc-000139
Type: Flower
Metrc Test Pkg#: 1A405010000089A000000124

Test Conditions

Scale: XS-205MI1
Temp: 21.3 °C
Baro Pressure: 987 hPa
Analyst: ACR
Technician: ACR

Sample ID#: 113995

Harvest/Process Date: 12/21/2018
Serving Size (g): 1
Date Received: 12/21/2018
Test Date: 12/27/2018
Valid Through: 12/27/2019
Report Issued: 12/31/2018

Sample #113995
Test Method MCFU (CFU/g) LOD (CFU/g) Status (CFU/g)
Total Aerobic FE-37 100,000 453 Pass/906
Yeast & Mold FE-37 10,000 453 Failed/22,649
Bile-tolerant gram-negative bacteria FE-37 1,000 45 Pass/<LOD
Total Coliforms FE-37 1,000 45 Failed/1,087
E. Coli FE-37 100 45 Pass/<LOD
Salmonella FE-56 100 94 Pass/<LOD
Aspergillus spp. Not Tested N/A 0 Not Tested

Test Method MRL (µg/g) LOD (µg/g) Status (µg/g)
Total Aflatoxin (B1, B2, G1, and G2) FE-61 0.02 0.02 Pass/<0.02µg/g

TNTC = Too Numerous To Count. Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 6 of 8

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Michigan Compliant Bio Analysis by
Microscopic Visual Inspection

Testing Accreditation #: 77802 Test Certificate #: 113995-001
Client Name, Sample Details

Breedsville Provisioning Center
Breedsville, MI 49027
Sample: Gelato
License: pc-000139
Type: Flower
Method: FE02 Microscope Dissection
Metrc Test Pkg#: 1A405010000089A000000124

Test Conditions

Analyst: ACR
Technician: JRT

Sample ID#: 113995

Harvest/Process Date: 12/21/2018
Serving Size (g): 1
Date Received: 12/21/2018
Test Date: 12/27/2018
Valid Through: 12/27/2019
Report Issued: 12/28/2018

Sample #113995
Sample #113995 Sample #113995
Impurities: Detected
Sporulating hyphae - mild, found on 1 node per gram Spider mites - severe, found 7+ per gram Predator mites - severe, found 15+ per gram See microbial analysis for a conclusive analysis. Less than 2% foreign matter. Less than 5% stem material.
Molds: Yes Types: Hyphae
Pests: Yes Types: Spider Mites, Predator Mites
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture -

The gland heads range from small to large in size and are moderately abundant. Slightly more of them are clear than milky with a moderate amount turning amber in color. Some of the trichomes are damaged and degrading. A few of the trichomes are reduced due to stress. See microbial analysis for a conclusive analysis. Less than 2% foreign matter. Less than 5% stem material.

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 7 of 8

IRON Laboratories

Michigan Compliant Heavy Metals Analysis

Test Certificate #: 113995-001
Client Name, Sample Details

Breedsville Provisioning Center
Breedsville, MI 49027
Sample: Gelato
License: pc-000139
Type: Flower
Method: FE60 ICPMS-MI
Metrc Test Pkg#: 1A405010000089A000000124

Test Conditions

Analyst: JER
Technician: MEH

Sample ID#: 113995

Harvest/Process Date: 12/21/2018
Serving Size (g): 1
Date Received: 12/21/2018
Report Issued: 01/03/2019

Sample #113995
Sample #113995 Sample #113995
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Arsenic 0.98 0.04 Pass/<LOD
Copper Not Tested
Cadmium 0.63 0.04 Pass/<LOD
Chromium Not Tested
Lead 2 0.05 Pass/<LOD
Mercury 2 0.05 Pass/<LOD
Nickel Not Tested

MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 8 of 8