ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113964-001
Client Name, Sample Details

HeavyLids LLC
Fall Creek, OR 97438
Sample: 9lb Hammer
License: 020-10022352D81
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A401030000E7A5000000180
Metrc Source Pkg#: 1A401030000E7A5000000174
***Water Activity: 0.469
***Moisture: 12.43%
Test Conditions

Prepsheet ID#: ORP181231a
Scale: XS205-OR1
Temp: 21.6 °C
Baro Pressure: 1013 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113964

Lot #: 2018-10-16-Dry Room -I-H
Batch #: 113964
Batch Weight (g): 6810
Harvest/Process Date: 10/16/2018
Date Received: 12/19/2018
Test Date: 12/31/2018
Sample #113964
Sample #113964 Sample #113964
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV Total THC Total CBD
Amount N/D 0.09% N/D 0.09% 0.16% 0.17% 1.99% 26.69% N/D 25.40% 0.08%
LOQ 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05%
Uncertainty 0% RPD 4.83% RPD 0.00% RPD 0.00% RPD 0.00% RPD 8.70% RPD ±5% RPD 4.40% RPD 0% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 3

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113964-001
Client Name, Sample Details

HeavyLids LLC
Fall Creek, OR 97438
Sample: 9lb Hammer
License: 020-10022352D81
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A401030000E7A5000000180
Metrc Source Pkg#: 1A401030000E7A5000000174
***Water Activity: 0.469
***Moisture: 12.43%
Test Conditions

Prepsheet ID#: ORP181231a
Scale: XS205-OR1
Temp: 21.6 °C
Baro Pressure: 1013 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113964

Lot #: 2018-10-16-Dry Room -I-H
Batch #: 113964
Batch Weight (g): 6810
Harvest/Process Date: 10/16/2018
Date Received: 12/19/2018
Test Date: 12/31/2018
Sample #113964
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0%
Cannabidiolic Acid (CBDA) N.D. 1.06 1.06 100.00 1.01 95.28 4.83%
Cannabigerol (CBG) N.D. 0.15 0.14 93.33 0.14 93.33 0.00%
Cannabidiol (CBD) N.D. 0.77 0.73 94.81 0.73 94.81 0.00%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0%
Cannabinol (CBN) N.D. 0.05 0.11 220.00 0.12 240.00 8.70%
Δ9-Tetrahydrocannabinol (THC) N.D. 3.34 2.95 88.32 3.1 92.81 4.96%
Cannabichromene (CBC) N.D. 0.24 0.14 58.33 0.14 58.33 0.00%
Tetrahydrocannabinolic acid (THCA) N.D. 6.45 6 93.02 6.27 97.21 4.40%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 3

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113964-001
Client Name, Sample Details

HeavyLids LLC
Fall Creek, OR 97438
Sample: 9lb Hammer
License: 020-10022352D81
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030000E7A5000000180
Metrc Source Pkg#: 1A401030000E7A5000000174
Test Conditions

Prepsheet ID#: ORPS181221a
Scale: Veritas-OR1
Temp: 22.1 °C
Baro PE: 1007 hPa
Analyst: JDM
Technician: JDM
Sample ID#: 113964

Lot #: 2018-10-16-Dry Room -I-H
Batch #: 113964
Batch Weight (g): 6810
Harvest/Process Date: 10/16/2018
Date Received: 12/19/2018
Test Date: 12/24/2018
Sample #113964
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.124 Pass/<LOD Abamectin**** 0.500 0.124 Pass/<LOD
Acephate 0.400 0.124 Pass/<LOD Acequinocyl 2.000 0.247 Pass/<LOD
Acetamiprid 0.200 0.124 Pass/<LOD Azoxystrobin 0.200 0.124 Pass/<LOD
Bifenazate 0.200 0.124 Pass/<LOD Bifenthrin 0.200 0.124 Pass/<LOD
Boscalid 0.400 0.124 Pass/<LOD Carbaryl 0.200 0.124 Pass/<LOD
Carbofuran 0.200 0.124 Pass/<LOD Chlorantraniliprole 0.200 0.124 Pass/<LOD
Chlorfenapyr 1.000 0.494 Pass/<LOD Chlorpyrifos 0.200 0.124 Pass/<LOD
Clofentezine 0.200 0.124 Pass/<LOD Cyfluthrin** 1.000 0.494 Pass/<LOD
Cypermethrin*** 1.000 0.494 Pass/<LOD Daminozide 1.000 0.124 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.247 Pass/<LOD Diazinon 0.200 0.124 Pass/<LOD
Dimethoate 0.200 0.124 Pass/<LOD Ethoprophos 0.200 0.124 Pass/<LOD
Etofenprox 0.400 0.124 Pass/<LOD Etoxazole 0.200 0.124 Pass/<LOD
Fenoxycarb 0.200 0.124 Pass/<LOD Fenpyroximate 0.400 0.124 Pass/<LOD
Fipronil 0.400 0.124 Pass/<LOD Flonicamid 1.000 0.124 Pass/<LOD
Fludioxonil 0.400 0.124 Pass/<LOD Hexythiazox 1.000 0.124 Pass/<LOD
Imazalil 0.200 0.124 Pass/<LOD Imidacloprid 0.400 0.124 Pass/<LOD
Kresoxim Methyl 0.400 0.124 Pass/<LOD Malathion 0.200 0.124 Pass/<LOD
Metalaxyl 0.200 0.124 Pass/<LOD Methiocarb 0.200 0.124 Pass/<LOD
Methomyl 0.400 0.124 Pass/<LOD Methyl Parathion 0.200 0.124 Pass/<LOD
MGK-264‡ 0.200 0.124 Pass/<LOD Myclobutanil 0.000 0.124 Pass/<LOD
Naled 0.500 0.124 Pass/<LOD Oxamyl 1.000 0.124 Pass/<LOD
Paclobutrazol 0.400 0.124 Pass/<LOD Permethrins† 0.200 0.124 Pass/<LOD
Phosmet 0.200 0.124 Pass/<LOD Piperonyl Butoxide 2.000 0.124 Pass/<LOD
Prallethrin 0.200 0.124 Pass/<LOD Propiconazole 0.400 0.124 Pass/<LOD
Propoxur 0.200 0.124 Pass/<LOD Pyrethrins* 1.000 0.124 Pass/<LOD
Pyridaben 0.200 0.124 Pass/<LOD Spinosad***** 0.200 0.124 Pass/<LOD
Spiromesifen 0.200 0.124 Pass/<LOD Spirotetramat 0.200 0.124 Pass/<LOD
Spiroxamine‡ 0.400 0.124 Pass/<LOD Tebuconazole 0.400 0.124 Pass/<LOD
Thiacloprid 0.200 0.124 Pass/<LOD Thiamethoxam 0.200 0.124 Pass/<LOD
Trifloxystrobin 0.200 0.124 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 3

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113964-001
Client Name, Sample Details

HeavyLids LLC
Fall Creek, OR 97438
Sample: 9lb Hammer
License: 020-10022352D81
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030000E7A5000000180
Metrc Source Pkg#: 1A401030000E7A5000000174
Test Conditions

Prepsheet ID#: ORPS181221a
Scale: Veritas-OR1
Temp: 22.1 °C
Baro PE: 1007 hPa
Analyst: JDM
Technician: JDM
Sample ID#: 113964

Lot #: 2018-10-16-Dry Room -I-H
Batch #: 113964
Batch Weight (g): 6810
Harvest/Process Date: 10/16/2018
Date Received: 12/19/2018
Test Date: 12/24/2018
Sample #113964
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.913 0.956 91.30 95.60 4.60
Acequinocyl N.D. 1 0.984 1.01 98.40 101.00 2.61
Acetamiprid N.D. 1 0.95 1.01 95.00 101.00 6.12
Aldicarb N.D. 1 0.902 0.912 90.20 91.20 1.10
Avermectin B1a N.D. 0.97 0.963 1.01 99.28 104.12 4.76
Azoxystrobin N.D. 1 0.923 0.964 92.30 96.40 4.35
Bifenazate N.D. 1 1.01 1.02 101.00 102.00 0.99
Bifenthrin N.D. 1 0.964 0.99 96.40 99.00 2.66
Boscalid N.D. 1 1.1 1.06 110.00 106.00 3.70
Carbaryl N.D. 1 0.917 0.867 91.70 86.70 5.61
Carbofuran N.D. 1 0.939 0.971 93.90 97.10 3.35
Chlorantraniliprole N.D. 1 0.998 0.994 99.80 99.40 0.40
Chlorfenapyr N.D. 1 0.924 0.947 92.40 94.70 2.46
Chlorpyriphos N.D. 1 0.951 0.905 95.10 90.50 4.96
Clofentezine N.D. 1 0.914 0.907 91.40 90.70 0.77
Cyfluthrin N.D. 1 1.04 1.03 104.00 103.00 0.97
Cypermethrin N.D. 1 1.04 0.967 104.00 96.70 7.27
Daminoside N.D. 1 1.29 1.41 129.00 141.00 8.89 HR
Diazanon N.D. 1 6.17 6.61 617.00 661.00 6.89 HR
Dichlorvos N.D. 1 0.973 1.04 97.30 104.00 6.66
Dimethoate N.D. 1 0.947 0.939 94.70 93.90 0.85
Ethoprophos N.D. 1 0.844 0.89 84.40 89.00 5.31
Etofenprox N.D. 1 0.873 0.895 87.30 89.50 2.49
Etoxazole N.D. 1 1.16 1.16 116.00 116.00 0.00
Fenoxycarb N.D. 1 0.883 0.899 88.30 89.90 1.80
Fenpyroximate N.D. 1 1.13 1.16 113.00 116.00 2.62
Fipronil N.D. 1 0.964 0.985 96.40 98.50 2.15
Flonicamid N.D. 1 0.924 0.95 92.40 95.00 2.77
Fludioxonil N.D. 1 1.02 1.03 102.00 103.00 0.98
Hexythiazox N.D. 1 0.795 0.812 79.50 81.20 2.12
Imazalil N.D. 1 0.983 0.945 98.30 94.50 3.94
Imidacloprid N.D. 1 1.14 1.17 114.00 117.00 2.60
Kresoxim-methyl N.D. 1 1 1.09 100.00 109.00 8.61
Malathion N.D. 1 1.04 1.08 104.00 108.00 3.77
Metalaxyl N.D. 1 1.24 1.24 124.00 124.00 0.00
Methiocarb N.D. 1 0.92 0.9 92.00 90.00 2.20
Methomyl N.D. 1 1.01 0.993 101.00 99.30 1.70
MGK-264 N.D. 1 1.16 1.1 116.00 110.00 5.31
Myclobutanil N.D. 1 1.07 1.06 107.00 106.00 0.94
Naled (dibrom) N.D. 1 1.02 1.09 102.00 109.00 6.64
Oxamyl N.D. 1 0.965 1.02 96.50 102.00 5.54
Paclobutrazol N.D. 1 0.969 0.99 96.90 99.00 2.14
Parathion-methyl N.D. 1 0.932 0.897 93.20 89.70 3.83
Permethrins N.D. 1 0.916 0.994 91.60 99.40 8.17
Phosmet N.D. 1 1.02 1 102.00 100.00 1.98
Piperonyl butoxide N.D. 1 1.11 1.14 111.00 114.00 2.67
Prallethrin N.D. 1 0.873 0.89 87.30 89.00 1.93
Propiconazole N.D. 1 0.645 0.664 64.50 66.40 2.90
Propoxur N.D. 1 0.762 0.876 76.20 87.60 13.92
Pyrethrin N.D. 0.65 0.596 0.634 91.69 97.54 6.18
Pyridaben N.D. 1 0.998 1 99.80 100.00 0.20
SpinosynA N.D. 0.84 0.966 0.977 115.00 116.31 1.13
SpinosynD N.D. 0.16 0.0669 0.0709 41.81 44.31 5.81 LR
Spiromesifen N.D. 1 1.87 1.76 187.00 176.00 6.06 HR
Spirotetramat N.D. 1 1.29 1.33 129.00 133.00 3.05 HR
Spiroxamine N.D. 1 0.974 0.978 97.40 97.80 0.41
Tebuconazole N.D. 1 0.876 0.946 87.60 94.60 7.68
Thiacloprid N.D. 1 1.04 1.07 104.00 107.00 2.84
Thiamethoxam N.D. 1 1.07 1.13 107.00 113.00 5.45
Trifloxystrobin N.D. 1 1 1.01 100.00 101.00 1.00

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 3