ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113939-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Mystery Haze x White Haze shatter
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000009008
Metrc Source Pkg#: 1A4010300016E07000008306
Test Conditions

Prepsheet ID#: ORP181228a
Scale: XS205-OR1
Temp: 21.9 °C
Baro Pressure: 1013 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113939

Lot #: MHWH9008
Batch #: 113939
Batch Weight (g): 344.31
Harvest/Process Date: 11/27/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/18/2018
Test Date: 12/28/2018
Sample #113939
Sample #113939 Sample #113939
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Avg
Avg. Amount N/D 42.71 mg/g N/D 3.36 mg/g 7.14 mg/g 13.93 mg/g 86.43 mg/g 747.42 mg/g 2.07 mg/g CBD 37.46 mg/g
LOQ 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g THC 741.91 mg/g
Amount per Serving~ N/D 4.27 mg/srv N/D 0.34 mg/srv 0.71 mg/srv 1.39 mg/srv 8.64 mg/srv 74.74 mg/srv 0.21 mg/srv Serving Size~ (g): 0.10 g
Uncertainty 5.16% RPD 1.82% RPD 4.59% RPD 0.33% RPD 2.39% RPD 1.71% RPD 100.03% RPD 1.60% RPD 1.03% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113939-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Mystery Haze x White Haze shatter
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000009008
Metrc Source Pkg#: 1A4010300016E07000008306
Test Conditions

Prepsheet ID#: ORP181228a
Scale: XS205-OR1
Temp: 21.9 °C
Baro Pressure: 1013 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113939

Lot #: MHWH9008
Batch #: 113939
Batch Weight (g): 344.31
Harvest/Process Date: 11/27/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/18/2018
Test Date: 12/28/2018
Sample #113939
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.93 5.47 92.24 5.76 97.13 5.16%
Cannabidiolic Acid (CBDA) N.D. 5.54 5.17 93.32 5.38 97.11 3.98%
Cannabigerol (CBG) N.D. 6.03 5.56 92.21 5.88 97.51 5.59%
Cannabidiol (CBD) N.D. 5.06 4.68 92.49 4.9 96.84 4.59%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.88 5.48 93.20 5.77 98.13 5.16%
Cannabinol (CBN) N.D. 5.16 4.83 93.60 5.1 98.84 5.44%
Δ9-Tetrahydrocannabinol (THC) N.D. 5.06 4.72 93.28 5.06 100.00 6.95%
Cannabichromene (CBC) N.D. 5.41 5.12 94.64 5.38 99.45 4.95%
Tetrahydrocannabinolic acid (THCA) N.D. 5.18 4.87 94.02 5.15 99.42 5.59%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113939-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Mystery Haze x White Haze shatter
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000009008
Metrc Source Pkg#: 1A4010300016E07000008306
Test Conditions

Prepsheet ID#: ORPS181219a
Scale: Veritas-OR1
Temp: 22.1 °C
Baro PE: 1004 hPa
Analyst: JDM
Technician: JDM
Sample ID#: 113939

Lot #: MHWH9008
Batch #: 113939
Batch Weight (g): 344.31
Harvest/Process Date: 11/27/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/18/2018
Test Date: 12/21/2018
Sample #113939
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.119 Pass/<LOD Abamectin**** 0.500 0.119 Pass/<LOD
Acephate 0.400 0.119 Pass/<LOD Acequinocyl 2.000 0.238 Pass/<LOD
Acetamiprid 0.200 0.119 Pass/<LOD Azoxystrobin 0.200 0.119 Pass/<LOD
Bifenazate 0.200 0.119 Pass/<LOD Bifenthrin 0.200 0.119 Pass/<LOD
Boscalid 0.400 0.119 Pass/<LOD Carbaryl 0.200 0.119 Pass/<LOD
Carbofuran 0.200 0.119 Pass/<LOD Chlorantraniliprole 0.200 0.119 Pass/<LOD
Chlorfenapyr 1.000 0.476 Pass/<LOD Chlorpyrifos 0.200 0.119 Pass/<LOD
Clofentezine 0.200 0.119 Pass/<LOD Cyfluthrin** 1.000 0.476 Pass/<LOD
Cypermethrin*** 1.000 0.476 Pass/<LOD Daminozide 1.000 0.119 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.238 Pass/<LOD Diazinon 0.200 0.119 Pass/<LOD
Dimethoate 0.200 0.119 Pass/<LOD Ethoprophos 0.200 0.119 Pass/<LOD
Etofenprox 0.400 0.119 Pass/<LOD Etoxazole 0.200 0.119 Pass/<LOD
Fenoxycarb 0.200 0.119 Pass/<LOD Fenpyroximate 0.400 0.119 Pass/<LOD
Fipronil 0.400 0.119 Pass/<LOD Flonicamid 1.000 0.119 Pass/<LOD
Fludioxonil 0.400 0.119 Pass/<LOD Hexythiazox 1.000 0.119 Pass/<LOD
Imazalil 0.200 0.119 Pass/<LOD Imidacloprid 0.400 0.119 Pass/<LOD
Kresoxim Methyl 0.400 0.119 Pass/<LOD Malathion 0.200 0.119 Pass/<LOD
Metalaxyl 0.200 0.119 Pass/<LOD Methiocarb 0.200 0.119 Pass/<LOD
Methomyl 0.400 0.119 Pass/<LOD Methyl Parathion 0.200 0.119 Pass/<LOD
MGK-264‡ 0.200 0.119 Pass/<LOD Myclobutanil 0.000 0.119 Pass/<LOD
Naled 0.500 0.119 Pass/<LOD Oxamyl 1.000 0.119 Pass/<LOD
Paclobutrazol 0.400 0.119 Pass/<LOD Permethrins† 0.200 0.119 Pass/<LOD
Phosmet 0.200 0.119 Pass/<LOD Piperonyl Butoxide 2.000 0.119 Pass/<LOD
Prallethrin 0.200 0.119 Pass/<LOD Propiconazole 0.400 0.119 Pass/<LOD
Propoxur 0.200 0.119 Pass/<LOD Pyrethrins* 1.000 0.119 Pass/<LOD
Pyridaben 0.200 0.119 Pass/<LOD Spinosad***** 0.200 0.119 Pass/<LOD
Spiromesifen 0.200 0.119 Pass/<LOD Spirotetramat 0.200 0.119 Pass/<LOD
Spiroxamine‡ 0.400 0.119 Pass/<LOD Tebuconazole 0.400 0.119 Pass/<LOD
Thiacloprid 0.200 0.119 Pass/<LOD Thiamethoxam 0.200 0.119 Pass/<LOD
Trifloxystrobin 0.200 0.119 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113939-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Mystery Haze x White Haze shatter
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000009008
Metrc Source Pkg#: 1A4010300016E07000008306
Test Conditions

Prepsheet ID#: ORPS181219a
Scale: Veritas-OR1
Temp: 22.1 °C
Baro PE: 1004 hPa
Analyst: JDM
Technician: JDM
Sample ID#: 113939

Lot #: MHWH9008
Batch #: 113939
Batch Weight (g): 344.31
Harvest/Process Date: 11/27/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/18/2018
Test Date: 12/21/2018
Sample #113939
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.03 0.947 103.00 94.70 8.40
Acequinocyl N.D. 1 0.488 0.558 48.80 55.80 13.38 LR
Acetamiprid N.D. 1 1.18 1.11 118.00 111.00 6.11
Aldicarb N.D. 1 0.93 0.878 93.00 87.80 5.75
Avermectin B1a N.D. 0.97 1.68 1.26 173.20 129.90 28.57 HRQ
Azoxystrobin N.D. 1 1.19 1.17 119.00 117.00 1.69
Bifenazate N.D. 1 0.277 0.248 27.70 24.80 11.05 LR
Bifenthrin N.D. 1 0.633 0.809 63.30 80.90 24.41 LRQ
Boscalid N.D. 1 1.08 1.13 108.00 113.00 4.52
Carbaryl N.D. 1 1.06 0.997 106.00 99.70 6.13
Carbofuran N.D. 1 1.11 1.07 111.00 107.00 3.67
Chlorantraniliprole N.D. 1 1.29 1.31 129.00 131.00 1.54 HR
Chlorfenapyr N.D. 1 0.702 0.693 70.20 69.30 1.29 LR
Chlorpyriphos N.D. 1 0.965 0.969 96.50 96.90 0.41
Clofentezine N.D. 1 1.03 1.04 103.00 104.00 0.97
Cyfluthrin N.D. 1 1.08 1.05 108.00 105.00 2.82
Cypermethrin N.D. 1 1.11 1.2 111.00 120.00 7.79
Daminoside N.D. 1 1.57 1.36 157.00 136.00 14.33 HRQ
Diazanon N.D. 1 6.71 6.45 671.00 645.00 3.95 HR
Dichlorvos N.D. 1 1.1 1.06 110.00 106.00 3.70
Dimethoate N.D. 1 1.18 1.1 118.00 110.00 7.02
Ethoprophos N.D. 1 1.11 1.05 111.00 105.00 5.56
Etofenprox N.D. 1 0.702 0.72 70.20 72.00 2.53
Etoxazole N.D. 1 1.24 1.18 124.00 118.00 4.96
Fenoxycarb N.D. 1 1.2 1.17 120.00 117.00 2.53
Fenpyroximate N.D. 1 1.2 1.18 120.00 118.00 1.68
Fipronil N.D. 1 0.945 0.872 94.50 87.20 8.04
Flonicamid N.D. 1 1.15 1.07 115.00 107.00 7.21
Fludioxonil N.D. 1 0.997 0.996 99.70 99.60 0.10
Hexythiazox N.D. 1 0.748 0.813 74.80 81.30 8.33
Imazalil N.D. 1 1.28 1.25 128.00 125.00 2.37
Imidacloprid N.D. 1 1.3 1.29 130.00 129.00 0.77
Kresoxim-methyl N.D. 1 1.37 1.33 137.00 133.00 2.96 HR
Malathion N.D. 1 1.37 1.31 137.00 131.00 4.48 HR
Metalaxyl N.D. 1 1.49 1.45 149.00 145.00 2.72 HR
Methiocarb N.D. 1 1.13 1.09 113.00 109.00 3.60
Methomyl N.D. 1 1.27 1.22 127.00 122.00 4.02
MGK-264 N.D. 1 0.872 0.892 87.20 89.20 2.27
Myclobutanil N.D. 1 1.2 1.18 120.00 118.00 1.68
Naled (dibrom) N.D. 1 1.22 1.12 122.00 112.00 8.55
Oxamyl N.D. 1 1.19 1.13 119.00 113.00 5.17
Paclobutrazol N.D. 1 1.33 1.26 133.00 126.00 5.41 HR
Parathion-methyl N.D. 1 0.924 0.821 92.40 82.10 11.81
Permethrins N.D. 1 0.5 0.671 50.00 67.10 29.21 LRQ
Phosmet N.D. 1 1.34 1.33 134.00 133.00 0.75 HR
Piperonyl butoxide N.D. 1 1.04 1.05 104.00 105.00 0.96
Prallethrin N.D. 1 1.37 1.34 137.00 134.00 2.21 HR
Propiconazole N.D. 1 0.99 0.975 99.00 97.50 1.53
Propoxur N.D. 1 0.897 0.796 89.70 79.60 11.93
Pyrethrin N.D. 0.65 0.726 0.708 111.69 108.92 2.51
Pyridaben N.D. 1 0.817 0.914 81.70 91.40 11.21
SpinosynA N.D. 0.84 1.25 1.22 148.81 145.24 2.43 HR
SpinosynD N.D. 0.16 0.0929 0.0906 58.06 56.63 2.51 LR
Spiromesifen N.D. 1 2.02 2.01 202.00 201.00 0.50 HR
Spirotetramat N.D. 1 1.5 1.36 150.00 136.00 9.79 HR
Spiroxamine N.D. 1 1.31 1.23 131.00 123.00 6.30 HR
Tebuconazole N.D. 1 1.28 1.2 128.00 120.00 6.45
Thiacloprid N.D. 1 1.28 1.23 128.00 123.00 3.98
Thiamethoxam N.D. 1 1.43 1.38 143.00 138.00 3.56 HR
Trifloxystrobin N.D. 1 1.18 1.16 118.00 116.00 1.71

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113939-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Mystery Haze x White Haze shatter
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000009008
Metrc Source Pkg#: 1A4010300016E07000008306
Test Conditions

Prepsheet ID#: ORHS181228a
Scale: XS205-OR1
Temp: 19 °C
Baro Pressure: 1010 hPa
Analyst: JER
Technician: HRM
Sample ID#: 113939

Lot #: MHWH9008
Batch #: 113939
Batch Weight (g): 344.31
Harvest/Process Date: 11/27/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/18/2018
Test Date: 12/29/2018
Sample #113939
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 50 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 50 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 50 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 5,000 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 50 50 Pass/<LOD 3-Methylpentane (Hexanes) 50 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 1 100 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 6 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113939-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Mystery Haze x White Haze shatter
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000009008
Metrc Source Pkg#: 1A4010300016E07000008306
Test Conditions

Prepsheet ID#: ORHS181228a
Scale: XS205-OR1
Temp: 19 °C
Baro Pressure: 1010 hPa
Analyst: JER
Technician: HRM
Sample ID#: 113939

Lot #: MHWH9008
Batch #: 113939
Batch Weight (g): 344.31
Harvest/Process Date: 11/27/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/18/2018
Test Date: 12/29/2018
Sample #113939
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 30 24 12.00 9.60 22.22 LRQ
Isobutane N.D. 250 395 385 158.00 154.00 2.56 HR
Methanol N.D. 250 340 369 136.00 147.60 8.18 HR
n-Butane N.D. 250 222 354 88.80 141.60 45.83 Q
2,2-Dimethylpropane N.D. 250 343 375 137.20 150.00 8.91 HR
Ethanol N.D. 250 301 315 120.40 126.00 4.55
Isopentane N.D. 250 396 354 158.40 141.60 11.20 HR
Acetonitrile N.D. 250 268 331 107.20 132.40 21.04 Q
Diethyl ether N.D. 250 315 352 126.00 140.80 11.09
2-propanone N.D. 250 298 319 119.20 127.60 6.81 HR
2-propanol N.D. 250 369 305 147.60 122.00 18.99 Q
n-Pentane N.D. 250 133 331 53.20 132.40 85.34 Q
2,2-Dimethylbutane N.D. 250 236 335 94.40 134.00 34.68 Q
2,3-Dimethylbutane N.D. 250 249 345 99.60 138.00 32.32
Methylene chloride N.D. 250 292 319 116.80 127.60 8.84
2-Methylpentane N.D. 250 274 330 109.60 132.00 18.54
3-Methylpentane N.D. 250 271 319 108.40 127.60 16.27
2-Butanol N.D. 250 282 315 112.80 126.00 11.06
n-Hexane N.D. 250 270 325 108.00 130.00 18.49
Ethyl acetate N.D. 250 296 316 118.40 126.40 6.54
Tetrahydrofuran N.D. 250 302 317 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 303 317 0.00 0.00 0.00
Benzene N.D. 250 240 371 96.00 148.40 42.88 Q
Chloroform N.D. 250 16 10 6.40 4.00 46.15
Cyclohexane N.D. 250 283 312 113.20 124.80 9.75
Ethylene glycol N.D. 250 279 234 111.60 93.60 17.54 HR
Heptane N.D. 250 360 388 144.00 155.20 7.49
2-Ethoxyethanol N.D. 250 270 281 108.00 112.40 3.99
1,4-Dioxane N.D. 250 423 344 169.20 137.60 20.60 Q
Pyridine N.D. 250 0 0 0.00 0.00 0.00
Toluene N.D. 250 408 345 163.20 138.00 16.73 HR
Chlorobenzene N.D. 250 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 391 337 156.40 134.80 14.84 HR
m-Xylene/p-Xylene N.D. 250 684 669 273.60 267.60 2.22 HR
o-Xylene N.D. 250 394 325 157.60 130.00 19.19 HR
Cumene N.D. 250 402 409 160.80 163.60 1.73 Q
Ethylene oxide N.D. 250 248 316 99.20 126.40 24.11

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113939-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Mystery Haze x White Haze shatter
Type: AU Tincture
Metrc Test Pkg#: 1A4010300016E07000009008
Metrc Source Pkg#: 1A4010300016E07000008306
Sample ID#: 113939

Lot #: MHWH9008
Batch #: 113939
Batch Weight (g): 344.31
Harvest/Process Date: 11/27/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/18/2018
Sample #113939
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 736.65 37.11 86.40 741.45 2.08 N.D. 3.37 42.32 N.D. 7.05 13.81
Increment 2 747.18 37.80 86.46 753.38 2.06 N.D. 3.36 43.10 N.D. 7.22 14.05
Average Value 741.91 37.46 86.43 747.42 2.07 N.D. 3.37 42.71 N.D. 7.14 13.93
Max Value 747.18 37.80 86.46 753.38 2.08 N.D. 3.37 43.10 N.D. 7.22 14.05
Min Value 736.65 37.11 86.40 741.45 2.06 N.D. 3.36 42.32 N.D. 7.05 13.81
Relative Percent Difference (RPD) ±1.42 ±1.83 ±0.07 ±1.60 ±0.97 N.D. ±0.30 ±1.83 N.D. ±2.38 ±1.72
Average Cannabinoids Per Package 741.91 37.46 86.43 747.42 2.07 N.D. 3.37 42.71 N.D. 7.14 13.93
Average Cannabinoids Per Serving 74.19 3.75 8.64 74.74 0.21 N.D. 0.34 4.27 N.D. 0.71 1.39
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ721
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 7
IRON Laboratories

Oregon Compliant Terpene Report by
Mass Spectrometer
Test Certificate #: 113939-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Mystery Haze x White Haze shatter
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000009008
Metrc Source Pkg#: 1A4010300016E07000008306
Test Conditions

Scale: XS205-OR1
Temp: 19 °C
Baro Pressure: 1010 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 113939

Lot #: MHWH9008
Batch #: 113939
Batch Weight (g): 344.31
Harvest/Process Date: 11/27/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/18/2018
Test Date: 12/29/2018
Sample #113939

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.340 %

β-Ocimene:

0.860 %

Camphene:

0.050 %

Eucalyptol (1,8-Cineol):

0.070 %

Sabinene:

0.050 %

γ-Terpinene:

0.590 %

Myrcene:

0.360 %

α-Terpinolene:

2.450 %

β-Pinene:

0.430 %

Linalool:

0.120 %

∆3-Carene:

0.160 %

Fenchone:

0.020 %

α-Terpinene:

1.060 %

Fenchol:

0.160 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.340 %

Geraniol:

 N/D

4-Cymene:

0.040 %

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

1.300 %

α-Humulene:

0.640 %

Nerolidol 1:

 N/D

Nerolidol 2:

0.090 %

Guaiol:

0.860 %

Caryophyllene Oxide:

 N/D

α-Bisabolol:

0.550 %

Other Terpenes

Total: 10.540%
a-Phellandrene = 2.63 % a-Terpineol = 0.22 % Valencene = 0.17 %

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 7