ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113840-001
Client Name, Sample Details

HeavyLids LLC
Fall Creek, OR 97438
Sample: Blue Diesel
License: 020-10022352D81
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A401030000E7A5000000170
Metrc Source Pkg#: 1A401030000E7A5000000158
***Water Activity: 0.396
***Moisture: 11.76%
Test Conditions

Prepsheet ID#: ORP181220a
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1000 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113840

Lot #: Blue D -Dry
Batch #: 113840
Batch Weight (g): 6728.08
Harvest/Process Date: 10/23/2018
Date Received: 12/12/2018
Test Date: 12/20/2018
Sample #113840
Sample #113840 Sample #113840
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV Total THC Total CBD
Amount N/D 0.10% N/D 0.11% 0.21% 0.16% 0.82% 26.35% N/D 23.93% 0.09%
LOQ 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05%
Uncertainty 0% RPD 2.93% RPD 1.40% RPD 6.90% RPD 6.90% RPD 52.63% RPD ±5% RPD 2.80% RPD 0% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 3

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113840-001
Client Name, Sample Details

HeavyLids LLC
Fall Creek, OR 97438
Sample: Blue Diesel
License: 020-10022352D81
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A401030000E7A5000000170
Metrc Source Pkg#: 1A401030000E7A5000000158
***Water Activity: 0.396
***Moisture: 11.76%
Test Conditions

Prepsheet ID#: ORP181220a
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1000 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113840

Lot #: Blue D -Dry
Batch #: 113840
Batch Weight (g): 6728.08
Harvest/Process Date: 10/23/2018
Date Received: 12/12/2018
Test Date: 12/20/2018
Sample #113840
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0%
Cannabidiolic Acid (CBDA) N.D. 1.06 1.01 95.28 1.04 98.11 2.93%
Cannabigerol (CBG) N.D. 0.15 0.15 100.00 0.14 93.33 6.90%
Cannabidiol (CBD) N.D. 0.77 0.72 93.51 0.71 92.21 1.40%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0%
Cannabinol (CBN) N.D. 0.05 0.07 140.00 0.12 240.00 52.63%
Δ9-Tetrahydrocannabinol (THC) N.D. 3.34 3.21 96.11 3.12 93.41 2.84%
Cannabichromene (CBC) N.D. 0.24 0.14 58.33 0.15 62.50 6.90%
Tetrahydrocannabinolic acid (THCA) N.D. 6.45 6.52 101.09 6.34 98.29 2.80%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 3

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113840-001
Client Name, Sample Details

HeavyLids LLC
Fall Creek, OR 97438
Sample: Blue Diesel
License: 020-10022352D81
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030000E7A5000000170
Metrc Source Pkg#: 1A401030000E7A5000000158
Test Conditions

Prepsheet ID#: ORPS181212a
Scale: Veritas-OR1
Temp: 21.7 °C
Baro PE: 1011 hPa
Analyst: JER
Technician: JDM
Sample ID#: 113840

Lot #: Blue D -Dry
Batch #: 113840
Batch Weight (g): 6728.08
Harvest/Process Date: 10/23/2018
Date Received: 12/12/2018
Test Date: 12/14/2018
Sample #113840
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.121 Pass/<LOD Abamectin**** 0.500 0.121 Pass/<LOD
Acephate 0.400 0.121 Pass/<LOD Acequinocyl 2.000 0.242 Pass/<LOD
Acetamiprid 0.200 0.121 Pass/<LOD Azoxystrobin 0.200 0.121 Pass/<LOD
Bifenazate 0.200 0.121 Pass/<LOD Bifenthrin 0.200 0.121 Pass/<LOD
Boscalid 0.400 0.121 Pass/<LOD Carbaryl 0.200 0.121 Pass/<LOD
Carbofuran 0.200 0.121 Pass/<LOD Chlorantraniliprole 0.200 0.121 Pass/<LOD
Chlorfenapyr 1.000 0.484 Pass/<LOD Chlorpyrifos 0.200 0.121 Pass/<LOD
Clofentezine 0.200 0.121 Pass/<LOD Cyfluthrin** 1.000 0.484 Pass/<LOD
Cypermethrin*** 1.000 0.484 Pass/<LOD Daminozide 1.000 0.121 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.242 Pass/<LOD Diazinon 0.200 0.121 Pass/<LOD
Dimethoate 0.200 0.121 Pass/<LOD Ethoprophos 0.200 0.121 Pass/<LOD
Etofenprox 0.400 0.121 Pass/<LOD Etoxazole 0.200 0.121 Pass/<LOD
Fenoxycarb 0.200 0.121 Pass/<LOD Fenpyroximate 0.400 0.121 Pass/<LOD
Fipronil 0.400 0.121 Pass/<LOD Flonicamid 1.000 0.121 Pass/<LOD
Fludioxonil 0.400 0.121 Pass/<LOD Hexythiazox 1.000 0.121 Pass/<LOD
Imazalil 0.200 0.121 Pass/<LOD Imidacloprid 0.400 0.121 Pass/<LOD
Kresoxim Methyl 0.400 0.121 Pass/<LOD Malathion 0.200 0.121 Pass/<LOD
Metalaxyl 0.200 0.121 Pass/<LOD Methiocarb 0.200 0.121 Pass/<LOD
Methomyl 0.400 0.121 Pass/<LOD Methyl Parathion 0.200 0.121 Pass/<LOD
MGK-264‡ 0.200 0.121 Pass/<LOD Myclobutanil 0.000 0.121 Pass/<LOD
Naled 0.500 0.121 Pass/<LOD Oxamyl 1.000 0.121 Pass/<LOD
Paclobutrazol 0.400 0.121 Pass/<LOD Permethrins† 0.200 0.121 Pass/<LOD
Phosmet 0.200 0.121 Pass/<LOD Piperonyl Butoxide 2.000 0.121 Pass/<LOD
Prallethrin 0.200 0.121 Pass/<LOD Propiconazole 0.400 0.121 Pass/<LOD
Propoxur 0.200 0.121 Pass/<LOD Pyrethrins* 1.000 0.121 Pass/<LOD
Pyridaben 0.200 0.121 Pass/<LOD Spinosad***** 0.200 0.121 Pass/<LOD
Spiromesifen 0.200 0.121 Pass/<LOD Spirotetramat 0.200 0.121 Pass/<LOD
Spiroxamine‡ 0.400 0.121 Pass/<LOD Tebuconazole 0.400 0.121 Pass/<LOD
Thiacloprid 0.200 0.121 Pass/<LOD Thiamethoxam 0.200 0.121 Pass/<LOD
Trifloxystrobin 0.200 0.121 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 3

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113840-001
Client Name, Sample Details

HeavyLids LLC
Fall Creek, OR 97438
Sample: Blue Diesel
License: 020-10022352D81
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030000E7A5000000170
Metrc Source Pkg#: 1A401030000E7A5000000158
Test Conditions

Prepsheet ID#: ORPS181212a
Scale: Veritas-OR1
Temp: 21.7 °C
Baro PE: 1011 hPa
Analyst: JER
Technician: JDM
Sample ID#: 113840

Lot #: Blue D -Dry
Batch #: 113840
Batch Weight (g): 6728.08
Harvest/Process Date: 10/23/2018
Date Received: 12/12/2018
Test Date: 12/14/2018
Sample #113840
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.919 0.969 91.90 96.90 5.30
Acequinocyl N.D. 1 0.913 0.97 91.30 97.00 6.05
Acetamiprid N.D. 1 1 1.04 100.00 104.00 3.92
Aldicarb N.D. 1 0.898 0.949 89.80 94.90 5.52
Avermectin B1a N.D. 0.97 0.967 1.05 99.69 108.25 8.23
Azoxystrobin N.D. 1 0.876 0.884 87.60 88.40 0.91
Bifenazate N.D. 1 0.872 0.922 87.20 92.20 5.57
Bifenthrin N.D. 1 0.854 0.952 85.40 95.20 10.85
Boscalid N.D. 1 0.824 0.914 82.40 91.40 10.36
Carbaryl N.D. 1 0.863 0.894 86.30 89.40 3.53
Carbofuran N.D. 1 0.845 0.904 84.50 90.40 6.75
Chlorantraniliprole N.D. 1 0.784 0.875 78.40 87.50 10.97
Chlorfenapyr N.D. 1 0.609 0.677 60.90 67.70 10.58
Chlorpyriphos N.D. 1 0.99 1.03 99.00 103.00 3.96
Clofentezine N.D. 1 0.683 0.741 68.30 74.10 8.15 LR
Cyfluthrin N.D. 1 0.793 0.861 79.30 86.10 8.22
Cypermethrin N.D. 1 0.87 0.956 87.00 95.60 9.42
Daminoside N.D. 1 1.38 1.5 138.00 150.00 8.33
Diazanon N.D. 1 4.8 5.14 480.00 514.00 6.84 HR
Dichlorvos N.D. 1 0.951 0.992 95.10 99.20 4.22
Dimethoate N.D. 1 0.986 1.04 98.60 104.00 5.33
Ethoprophos N.D. 1 0.801 0.851 80.10 85.10 6.05
Etofenprox N.D. 1 0.87 0.902 87.00 90.20 3.61
Etoxazole N.D. 1 1.1 1.14 110.00 114.00 3.57
Fenoxycarb N.D. 1 0.763 0.798 76.30 79.80 4.48
Fenpyroximate N.D. 1 1.06 1.14 106.00 114.00 7.27
Fipronil N.D. 1 0.888 0.982 88.80 98.20 10.05
Flonicamid N.D. 1 0.928 0.965 92.80 96.50 3.91
Fludioxonil N.D. 1 0.899 0.948 89.90 94.80 5.31
Hexythiazox N.D. 1 0.646 0.71 64.60 71.00 9.44 LR
Imazalil N.D. 1 0.809 0.883 80.90 88.30 8.75
Imidacloprid N.D. 1 1.09 1.12 109.00 112.00 2.71
Kresoxim-methyl N.D. 1 0.792 0.854 79.20 85.40 7.53
Malathion N.D. 1 0.903 0.903 90.30 90.30 0.00
Metalaxyl N.D. 1 1 1.07 100.00 107.00 6.76
Methiocarb N.D. 1 0.877 0.953 87.70 95.30 8.31
Methomyl N.D. 1 0.942 1 94.20 100.00 5.97
MGK-264 N.D. 1 0.87 0.94 87.00 94.00 7.73
Myclobutanil N.D. 1 0.812 0.865 81.20 86.50 6.32
Naled (dibrom) N.D. 1 1.05 1.09 105.00 109.00 3.74
Oxamyl N.D. 1 0.979 1.05 97.90 105.00 7.00
Paclobutrazol N.D. 1 0.801 0.85 80.10 85.00 5.94
Parathion-methyl N.D. 1 0.889 0.752 88.90 75.20 16.70
Permethrins N.D. 1 0.875 0.926 87.50 92.60 5.66
Phosmet N.D. 1 0.927 0.965 92.70 96.50 4.02
Piperonyl butoxide N.D. 1 0.984 1.07 98.40 107.00 8.37
Prallethrin N.D. 1 0.923 0.977 92.30 97.70 5.68
Propiconazole N.D. 1 0.72 0.753 72.00 75.30 4.48
Propoxur N.D. 1 0.865 0.913 86.50 91.30 5.40
Pyrethrin N.D. 0.65 0.619 0.655 95.23 100.77 5.65
Pyridaben N.D. 1 0.952 1.02 95.20 102.00 6.90
SpinosynA N.D. 0.84 0.929 0.97 110.60 115.48 4.32
SpinosynD N.D. 0.16 0.0728 0.0739 45.50 46.19 1.50 LR
Spiromesifen N.D. 1 1.89 2.03 189.00 203.00 7.14 HR
Spirotetramat N.D. 1 1.17 1.2 117.00 120.00 2.53
Spiroxamine N.D. 1 0.904 0.982 90.40 98.20 8.27
Tebuconazole N.D. 1 0.755 0.809 75.50 80.90 6.91
Thiacloprid N.D. 1 0.947 1.02 94.70 102.00 7.42
Thiamethoxam N.D. 1 0.935 0.985 93.50 98.50 5.21
Trifloxystrobin N.D. 1 0.972 1.02 97.20 102.00 4.82

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 3