ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113769-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: OB1
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000008735
Metrc Source Pkg#: 1A4010300016E07000007667
Test Conditions

Prepsheet ID#: ORP181219b
Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113769

Lot #: OB17667
Batch #: 113769
Batch Weight (g): 456.72
Harvest/Process Date: 11/08/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/19/2018
Sample #113769
Sample #113769 Sample #113769
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Avg
Avg. Amount N/D 2.44 mg/g N/D 2.88 mg/g 6.78 mg/g 6.60 mg/g 109.22 mg/g 859.95 mg/g 0.90 mg/g CBD 2.14 mg/g
LOQ 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g THC 863.39 mg/g
Amount per Serving~ N/D 0.24 mg/srv N/D 0.29 mg/srv 0.68 mg/srv 0.66 mg/srv 10.92 mg/srv 86.00 mg/srv 0.09 mg/srv Serving Size~ (g): 0.10 g
Uncertainty 1.97% RPD 8.53% RPD 2.12% RPD 1.50% RPD 7.11% RPD 1.31% RPD 104.01% RPD 1.53% RPD 200.00% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113769-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: OB1
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000008735
Metrc Source Pkg#: 1A4010300016E07000007667
Test Conditions

Prepsheet ID#: ORP181219b
Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113769

Lot #: OB17667
Batch #: 113769
Batch Weight (g): 456.72
Harvest/Process Date: 11/08/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/19/2018
Sample #113769
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.85 5.53 94.53 5.64 96.41 1.97%
Cannabidiolic Acid (CBDA) N.D. 5.42 5.18 95.57 5.27 97.23 1.72%
Cannabigerol (CBG) N.D. 5.82 5.62 96.56 5.68 97.59 1.06%
Cannabidiol (CBD) N.D. 4.92 4.66 94.72 4.76 96.75 2.12%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.72 5.56 97.20 5.61 98.08 0.90%
Cannabinol (CBN) N.D. 5.05 4.89 96.83 4.95 98.02 1.22%
Δ9-Tetrahydrocannabinol (THC) N.D. 4.89 4.76 97.34 4.85 99.18 1.87%
Cannabichromene (CBC) N.D. 5.26 5.21 99.05 5.38 102.28 3.21%
Tetrahydrocannabinolic acid (THCA) N.D. 5.08 4.98 98.03 5.05 99.41 1.40%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113769-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: OB1
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000008735
Metrc Source Pkg#: 1A4010300016E07000007667
Test Conditions

Prepsheet ID#: ORPS181217b
Scale: Veritas-OR1
Temp: 21.9 °C
Baro PE: 999.5 hPa
Analyst: JDM
Technician: JDM
Sample ID#: 113769

Lot #: OB17667
Batch #: 113769
Batch Weight (g): 456.72
Harvest/Process Date: 11/08/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/25/2018
Sample #113769
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.121 Pass/<LOD Abamectin**** 0.500 0.121 Pass/<LOD
Acephate 0.400 0.121 Pass/<LOD Acequinocyl 2.000 0.243 Pass/<LOD
Acetamiprid 0.200 0.121 Pass/<LOD Azoxystrobin 0.200 0.121 Pass/<LOD
Bifenazate 0.200 0.121 Pass/<LOD Bifenthrin 0.200 0.121 Pass/<LOD
Boscalid 0.400 0.121 Pass/<LOD Carbaryl 0.200 0.121 Pass/<LOD
Carbofuran 0.200 0.121 Pass/<LOD Chlorantraniliprole 0.200 0.121 Pass/<LOD
Chlorfenapyr 1.000 0.485 Pass/<LOD Chlorpyrifos 0.200 0.121 Pass/<LOD
Clofentezine 0.200 0.121 Pass/<LOD Cyfluthrin** 1.000 0.485 Pass/<LOD
Cypermethrin*** 1.000 0.485 Pass/<LOD Daminozide 1.000 0.121 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.243 Pass/<LOD Diazinon 0.200 0.121 Pass/<LOD
Dimethoate 0.200 0.121 Pass/<LOD Ethoprophos 0.200 0.121 Pass/<LOD
Etofenprox 0.400 0.121 Pass/<LOD Etoxazole 0.200 0.121 Pass/<LOD
Fenoxycarb 0.200 0.121 Pass/<LOD Fenpyroximate 0.400 0.121 Pass/<LOD
Fipronil 0.400 0.121 Pass/<LOD Flonicamid 1.000 0.121 Pass/<LOD
Fludioxonil 0.400 0.121 Pass/<LOD Hexythiazox 1.000 0.121 Pass/<LOD
Imazalil 0.200 0.121 Pass/<LOD Imidacloprid 0.400 0.121 Pass/<LOD
Kresoxim Methyl 0.400 0.121 Pass/<LOD Malathion 0.200 0.121 Pass/<LOD
Metalaxyl 0.200 0.121 Pass/<LOD Methiocarb 0.200 0.121 Pass/<LOD
Methomyl 0.400 0.121 Pass/<LOD Methyl Parathion 0.200 0.121 Pass/<LOD
MGK-264‡ 0.200 0.121 Pass/<LOD Myclobutanil 0.000 0.121 Pass/<LOD
Naled 0.500 0.121 Pass/<LOD Oxamyl 1.000 0.121 Pass/<LOD
Paclobutrazol 0.400 0.121 Failed/1.260 Permethrins† 0.200 0.121 Pass/<LOD
Phosmet 0.200 0.121 Pass/<LOD Piperonyl Butoxide 2.000 0.121 Pass/<LOD
Prallethrin 0.200 0.121 Pass/<LOD Propiconazole 0.400 0.121 Pass/<LOD
Propoxur 0.200 0.121 Pass/<LOD Pyrethrins* 1.000 0.121 Pass/<LOD
Pyridaben 0.200 0.121 Pass/<LOD Spinosad***** 0.200 0.121 Pass/<LOD
Spiromesifen 0.200 0.121 Pass/<LOD Spirotetramat 0.200 0.121 Pass/<LOD
Spiroxamine‡ 0.400 0.121 Pass/<LOD Tebuconazole 0.400 0.121 Pass/<LOD
Thiacloprid 0.200 0.121 Pass/<LOD Thiamethoxam 0.200 0.121 Pass/<LOD
Trifloxystrobin 0.200 0.121 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113769-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: OB1
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000008735
Metrc Source Pkg#: 1A4010300016E07000007667
Test Conditions

Prepsheet ID#: ORPS181217b
Scale: Veritas-OR1
Temp: 21.9 °C
Baro PE: 999.5 hPa
Analyst: JDM
Technician: JDM
Sample ID#: 113769

Lot #: OB17667
Batch #: 113769
Batch Weight (g): 456.72
Harvest/Process Date: 11/08/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/25/2018
Sample #113769
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.951 0.96 95.10 96.00 0.94
Acequinocyl N.D. 1 0.649 0.687 64.90 68.70 5.69 LR
Acetamiprid N.D. 1 1.03 1.06 103.00 106.00 2.87
Aldicarb N.D. 1 0.824 0.856 82.40 85.60 3.81
Avermectin B1a N.D. 0.97 1.26 1.12 129.90 115.46 11.76
Azoxystrobin N.D. 1 1.17 1.11 117.00 111.00 5.26
Bifenazate N.D. 1 1.2 1.25 120.00 125.00 4.08
Bifenthrin N.D. 1 0.885 0.914 88.50 91.40 3.22
Boscalid N.D. 1 1.18 0.987 118.00 98.70 17.81
Carbaryl N.D. 1 0.89 0.898 89.00 89.80 0.89
Carbofuran N.D. 1 1.05 1.05 105.00 105.00 0.00
Chlorantraniliprole N.D. 1 1.24 1.23 124.00 123.00 0.81
Chlorfenapyr N.D. 1 0.765 0.775 76.50 77.50 1.30
Chlorpyriphos N.D. 1 0.958 0.997 95.80 99.70 3.99
Clofentezine N.D. 1 1.03 1.09 103.00 109.00 5.66
Cyfluthrin N.D. 1 1.1 1.01 110.00 101.00 8.53
Cypermethrin N.D. 1 1.14 1.08 114.00 108.00 5.41
Daminoside N.D. 1 1.62 1.68 162.00 168.00 3.64 HR
Diazanon N.D. 1 6.68 6.41 668.00 641.00 4.13 HR
Dichlorvos N.D. 1 0.958 0.953 95.80 95.30 0.52
Dimethoate N.D. 1 1.03 0.992 103.00 99.20 3.76
Ethoprophos N.D. 1 1.02 1.03 102.00 103.00 0.98
Etofenprox N.D. 1 0.68 0.719 68.00 71.90 5.58
Etoxazole N.D. 1 1.16 1.09 116.00 109.00 6.22
Fenoxycarb N.D. 1 1.18 1.13 118.00 113.00 4.33
Fenpyroximate N.D. 1 1.06 1.04 106.00 104.00 1.90
Fipronil N.D. 1 0.958 1 95.80 100.00 4.29
Flonicamid N.D. 1 1.05 1.06 105.00 106.00 0.95
Fludioxonil N.D. 1 0.972 1.02 97.20 102.00 4.82
Hexythiazox N.D. 1 0.804 0.833 80.40 83.30 3.54
Imazalil N.D. 1 1.24 1.2 124.00 120.00 3.28
Imidacloprid N.D. 1 1.13 1.15 113.00 115.00 1.75
Kresoxim-methyl N.D. 1 1.4 1.44 140.00 144.00 2.82 HR
Malathion N.D. 1 1.32 1.3 132.00 130.00 1.53 HR
Metalaxyl N.D. 1 1.43 1.41 143.00 141.00 1.41 HR
Methiocarb N.D. 1 0.986 0.975 98.60 97.50 1.12
Methomyl N.D. 1 1.25 1.28 125.00 128.00 2.37
MGK-264 N.D. 1 0.874 0.871 87.40 87.10 0.34
Myclobutanil N.D. 1 1.28 1.28 128.00 128.00 0.00
Naled (dibrom) N.D. 1 1.16 1.09 116.00 109.00 6.22
Oxamyl N.D. 1 1.03 1.03 103.00 103.00 0.00
Paclobutrazol N.D. 1 1.27 1.22 127.00 122.00 4.02
Parathion-methyl N.D. 1 0.855 0.872 85.50 87.20 1.97
Permethrins N.D. 1 0.792 0.82 79.20 82.00 3.47
Phosmet N.D. 1 1.23 1.28 123.00 128.00 3.98
Piperonyl butoxide N.D. 1 1.05 1.01 105.00 101.00 3.88
Prallethrin N.D. 1 1.32 1.28 132.00 128.00 3.08 HR
Propiconazole N.D. 1 0.989 0.967 98.90 96.70 2.25
Propoxur N.D. 1 0.768 0.762 76.80 76.20 0.78
Pyrethrin N.D. 0.65 0.745 0.744 114.62 114.46 0.13
Pyridaben N.D. 1 0.827 0.804 82.70 80.40 2.82
SpinosynA N.D. 0.84 1.13 1.13 134.52 134.52 0.00 HR
SpinosynD N.D. 0.16 0.0855 0.0803 53.44 50.19 6.27 LR
Spiromesifen N.D. 1 2.15 2.12 215.00 212.00 1.41 HR
Spirotetramat N.D. 1 1.39 1.31 139.00 131.00 5.93 HR
Spiroxamine N.D. 1 1.27 1.25 127.00 125.00 1.59
Tebuconazole N.D. 1 1.24 1.13 124.00 113.00 9.28
Thiacloprid N.D. 1 1.12 1.15 112.00 115.00 2.64
Thiamethoxam N.D. 1 1.42 1.46 142.00 146.00 2.78 HR
Trifloxystrobin N.D. 1 1.05 1.04 105.00 104.00 0.96

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113769-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: OB1
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000008735
Metrc Source Pkg#: 1A4010300016E07000007667
Test Conditions

Prepsheet ID#: ORHS181217A
Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1010 hPa
Analyst: JER
Technician: HRM
Sample ID#: 113769

Lot #: OB17667
Batch #: 113769
Batch Weight (g): 456.72
Harvest/Process Date: 11/08/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/18/2018
Sample #113769
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 50 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 50 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 50 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 5,000 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/94
2-Propanone (Acetone) 50 50 Pass/<LOD 3-Methylpentane (Hexanes) 50 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 1 100 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 6 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113769-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: OB1
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000008735
Metrc Source Pkg#: 1A4010300016E07000007667
Test Conditions

Prepsheet ID#: ORHS181217A
Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1010 hPa
Analyst: JER
Technician: HRM
Sample ID#: 113769

Lot #: OB17667
Batch #: 113769
Batch Weight (g): 456.72
Harvest/Process Date: 11/08/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/18/2018
Sample #113769
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 107 112 42.80 44.80 4.57 LR
Isobutane N.D. 250 164 170 65.60 68.00 3.59 LR
Methanol N.D. 250 306 306 122.40 122.40 0.00
n-Butane N.D. 250 178 197 71.20 78.80 10.13
2,2-Dimethylpropane N.D. 250 211 223 84.40 89.20 5.53
Ethanol N.D. 250 260 284 104.00 113.60 8.82
Isopentane N.D. 250 252 253 100.80 101.20 0.40
Acetonitrile N.D. 250 241 237 96.40 94.80 1.67
Diethyl ether N.D. 250 299 320 119.60 128.00 6.79
2-propanone N.D. 250 280 295 112.00 118.00 5.22
2-propanol N.D. 250 541 530 216.40 212.00 2.05 HR
n-Pentane N.D. 250 170 193 68.00 77.20 12.67
2,2-Dimethylbutane N.D. 250 283 277 113.20 110.80 2.14
2,3-Dimethylbutane N.D. 250 265 269 106.00 107.60 1.50
Methylene chloride N.D. 250 290 282 116.00 112.80 2.80
2-Methylpentane N.D. 250 294 292 117.60 116.80 0.68
3-Methylpentane N.D. 250 286 239 114.40 95.60 17.90
2-Butanol N.D. 250 280 294 112.00 117.60 4.88
n-Hexane N.D. 250 278 276 111.20 110.40 0.72
Ethyl acetate N.D. 250 280 297 112.00 118.80 5.89
Tetrahydrofuran N.D. 250 294 299 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 300 308 0.00 0.00 0.00
Benzene N.D. 250 406 405 162.40 162.00 0.25 HR
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 282 289 112.80 115.60 2.45
Ethylene glycol N.D. 250 210 304 84.00 121.60 36.58 Q
Heptane N.D. 250 385 395 154.00 158.00 2.56 HR
2-Ethoxyethanol N.D. 250 214 282 85.60 112.80 27.42 Q
1,4-Dioxane N.D. 250 410 422 164.00 168.80 2.88 HR
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 398 392 159.20 156.80 1.52 HR
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 419 414 167.60 165.60 1.20 HR
m-Xylene/p-Xylene N.D. 500 838 830 167.60 166.00 0.96 HR
o-Xylene N.D. 250 434 431 173.60 172.40 0.69 HR
Cumene N.D. 250 470 443 188.00 177.20 5.91 HR
Ethylene oxide N.D. 250 222 261 88.80 104.40 16.15

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113769-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: OB1
Type: AU Tincture
Metrc Test Pkg#: 1A4010300016E07000008735
Metrc Source Pkg#: 1A4010300016E07000007667
Sample ID#: 113769

Lot #: OB17667
Batch #: 113769
Batch Weight (g): 456.72
Harvest/Process Date: 11/08/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Sample #113769
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 864.80 2.23 104.84 866.54 N.D. N.D. 2.86 2.54 N.D. 6.54 6.64
Increment 2 861.99 2.04 113.59 853.36 N.D. N.D. 2.90 2.33 N.D. 7.02 6.55
Average Value 863.39 2.14 109.22 859.95 N.D. N.D. 2.88 2.44 N.D. 6.78 6.60
Max Value 864.80 2.23 113.59 866.54 N.D. N.D. 2.90 2.54 N.D. 7.02 6.64
Min Value 861.99 2.04 104.84 853.36 N.D. N.D. 2.86 2.33 N.D. 6.54 6.55
Relative Percent Difference (RPD) ±0.33 ±8.62 ±8.01 ±1.53 N.D. N.D. ±1.39 ±8.62 N.D. ±7.08 ±1.36
Average Cannabinoids Per Package 863.39 2.14 109.22 859.95 N.D. N.D. 2.88 2.44 N.D. 6.78 6.60
Average Cannabinoids Per Serving 86.34 0.21 10.92 86.00 N.D. N.D. 0.29 0.24 N.D. 0.68 0.66
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ721
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 7
IRON Laboratories

Oregon Compliant Terpene Report by
Mass Spectrometer
Test Certificate #: 113769-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: OB1
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000008735
Metrc Source Pkg#: 1A4010300016E07000007667
Test Conditions

Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1010 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 113769

Lot #: OB17667
Batch #: 113769
Batch Weight (g): 456.72
Harvest/Process Date: 11/08/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/18/2018
Sample #113769

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.210 %

β-Ocimene:

0.070 %

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

0.040 %

Myrcene:

0.390 %

α-Terpinolene:

0.110 %

β-Pinene:

0.180 %

Linalool:

0.120 %

∆3-Carene:

 N/D

Fenchone:

0.040 %

α-Terpinene:

0.040 %

Fenchol:

0.170 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.190 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.670 %

α-Humulene:

0.280 %

Nerolidol 1:

 N/D

Nerolidol 2:

0.040 %

Guaiol:

0.350 %

Caryophyllene Oxide:

0.100 %

α-Bisabolol:

0.180 %

Other Terpenes

Total: 3.180%
a-Phellandrene = 0.06 % a-Terpineol = 0.19 % Valencene = 0.17 %

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 7