ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113768-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue Cookies
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000008734
Metrc Source Pkg#: 1A4010300016E07000007148
Test Conditions

Prepsheet ID#: ORP181219a
Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113768

Lot #: BC7148
Batch #: 113768
Batch Weight (g): 552.73
Harvest/Process Date: 10/31/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/19/2018
Sample #113768
Sample #113768 Sample #113768
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Avg
Avg. Amount N/D 30.85 mg/g N/D 2.56 mg/g 4.96 mg/g 4.10 mg/g 51.46 mg/g 875.92 mg/g N/D CBD 27.06 mg/g
LOQ 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g THC 819.64 mg/g
Amount per Serving~ N/D 3.09 mg/srv N/D 0.26 mg/srv 0.50 mg/srv 0.41 mg/srv 5.15 mg/srv 87.59 mg/srv N/D Serving Size~ (g): 0.10 g
Uncertainty 4.02% RPD 4.28% RPD 3.95% RPD 21.60% RPD 10.59% RPD 7.26% RPD 106.08% RPD 1.80% RPD 3.87% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113768-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue Cookies
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000008734
Metrc Source Pkg#: 1A4010300016E07000007148
Test Conditions

Prepsheet ID#: ORP181219a
Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113768

Lot #: BC7148
Batch #: 113768
Batch Weight (g): 552.73
Harvest/Process Date: 10/31/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/19/2018
Sample #113768
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.91 5.61 94.92 5.84 98.82 4.02%
Cannabidiolic Acid (CBDA) N.D. 5.49 5.22 95.08 5.43 98.91 3.94%
Cannabigerol (CBG) N.D. 5.96 5.65 94.80 5.84 97.99 3.31%
Cannabidiol (CBD) N.D. 5.07 4.71 92.90 4.9 96.65 3.95%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.85 5.57 95.21 5.79 98.97 3.87%
Cannabinol (CBN) N.D. 5.11 4.92 96.28 5.09 99.61 3.40%
Δ9-Tetrahydrocannabinol (THC) N.D. 5 4.81 96.20 4.97 99.40 3.27%
Cannabichromene (CBC) N.D. 5.46 5.25 96.15 5.31 97.25 1.14%
Tetrahydrocannabinolic acid (THCA) N.D. 5.22 5.04 96.55 5.1 97.70 1.18%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113768-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue Cookies
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000008734
Metrc Source Pkg#: 1A4010300016E07000007148
Test Conditions

Prepsheet ID#: ORPS181217b
Scale: Veritas-OR1
Temp: 21.9 °C
Baro PE: 999.5 hPa
Analyst: JDM
Technician: JDM
Sample ID#: 113768

Lot #: BC7148
Batch #: 113768
Batch Weight (g): 552.73
Harvest/Process Date: 10/31/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/23/2018
Sample #113768
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.119 Pass/<LOD Abamectin**** 0.500 0.119 Pass/<LOD
Acephate 0.400 0.119 Pass/<LOD Acequinocyl 2.000 0.239 Pass/<LOD
Acetamiprid 0.200 0.119 Pass/<LOD Azoxystrobin 0.200 0.119 Pass/<LOD
Bifenazate 0.200 0.119 Pass/<LOD Bifenthrin 0.200 0.119 Pass/<LOD
Boscalid 0.400 0.119 Pass/<LOD Carbaryl 0.200 0.119 Pass/<LOD
Carbofuran 0.200 0.119 Pass/<LOD Chlorantraniliprole 0.200 0.119 Pass/<LOD
Chlorfenapyr 1.000 0.478 Pass/<LOD Chlorpyrifos 0.200 0.119 Pass/<LOD
Clofentezine 0.200 0.119 Pass/<LOD Cyfluthrin** 1.000 0.478 Pass/<LOD
Cypermethrin*** 1.000 0.478 Pass/<LOD Daminozide 1.000 0.119 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.239 Pass/<LOD Diazinon 0.200 0.119 Pass/<LOD
Dimethoate 0.200 0.119 Pass/<LOD Ethoprophos 0.200 0.119 Pass/<LOD
Etofenprox 0.400 0.119 Pass/<LOD Etoxazole 0.200 0.119 Pass/<LOD
Fenoxycarb 0.200 0.119 Pass/<LOD Fenpyroximate 0.400 0.119 Pass/<LOD
Fipronil 0.400 0.119 Pass/<LOD Flonicamid 1.000 0.119 Pass/<LOD
Fludioxonil 0.400 0.119 Pass/<LOD Hexythiazox 1.000 0.119 Pass/<LOD
Imazalil 0.200 0.119 Pass/<LOD Imidacloprid 0.400 0.119 Pass/<LOD
Kresoxim Methyl 0.400 0.119 Pass/<LOD Malathion 0.200 0.119 Pass/<LOD
Metalaxyl 0.200 0.119 Pass/<LOD Methiocarb 0.200 0.119 Pass/<LOD
Methomyl 0.400 0.119 Pass/<LOD Methyl Parathion 0.200 0.119 Pass/<LOD
MGK-264‡ 0.200 0.119 Pass/<LOD Myclobutanil 0.000 0.119 Pass/<LOD
Naled 0.500 0.119 Pass/<LOD Oxamyl 1.000 0.119 Pass/<LOD
Paclobutrazol 0.400 0.119 Failed/0.709 Permethrins† 0.200 0.119 Pass/<LOD
Phosmet 0.200 0.119 Pass/<LOD Piperonyl Butoxide 2.000 0.119 Pass/<LOD
Prallethrin 0.200 0.119 Pass/<LOD Propiconazole 0.400 0.119 Pass/<LOD
Propoxur 0.200 0.119 Pass/<LOD Pyrethrins* 1.000 0.119 Pass/<LOD
Pyridaben 0.200 0.119 Pass/<LOD Spinosad***** 0.200 0.119 Pass/<LOD
Spiromesifen 0.200 0.119 Pass/<LOD Spirotetramat 0.200 0.119 Pass/<LOD
Spiroxamine‡ 0.400 0.119 Pass/<LOD Tebuconazole 0.400 0.119 Pass/<LOD
Thiacloprid 0.200 0.119 Pass/<LOD Thiamethoxam 0.200 0.119 Pass/<LOD
Trifloxystrobin 0.200 0.119 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113768-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue Cookies
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000008734
Metrc Source Pkg#: 1A4010300016E07000007148
Test Conditions

Prepsheet ID#: ORPS181217b
Scale: Veritas-OR1
Temp: 21.9 °C
Baro PE: 999.5 hPa
Analyst: JDM
Technician: JDM
Sample ID#: 113768

Lot #: BC7148
Batch #: 113768
Batch Weight (g): 552.73
Harvest/Process Date: 10/31/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/23/2018
Sample #113768
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.951 0.96 95.10 96.00 0.94
Acequinocyl N.D. 1 0.649 0.687 64.90 68.70 5.69 LR
Acetamiprid N.D. 1 1.03 1.06 103.00 106.00 2.87
Aldicarb N.D. 1 0.824 0.856 82.40 85.60 3.81
Avermectin B1a N.D. 0.97 1.26 1.12 129.90 115.46 11.76
Azoxystrobin N.D. 1 1.17 1.11 117.00 111.00 5.26
Bifenazate N.D. 1 1.2 1.25 120.00 125.00 4.08
Bifenthrin N.D. 1 0.885 0.914 88.50 91.40 3.22
Boscalid N.D. 1 1.18 0.987 118.00 98.70 17.81
Carbaryl N.D. 1 0.89 0.898 89.00 89.80 0.89
Carbofuran N.D. 1 1.05 1.05 105.00 105.00 0.00
Chlorantraniliprole N.D. 1 1.24 1.23 124.00 123.00 0.81
Chlorfenapyr N.D. 1 0.765 0.775 76.50 77.50 1.30
Chlorpyriphos N.D. 1 0.958 0.997 95.80 99.70 3.99
Clofentezine N.D. 1 1.03 1.09 103.00 109.00 5.66
Cyfluthrin N.D. 1 1.1 1.01 110.00 101.00 8.53
Cypermethrin N.D. 1 1.14 1.08 114.00 108.00 5.41
Daminoside N.D. 1 1.62 1.68 162.00 168.00 3.64 HR
Diazanon N.D. 1 6.68 6.41 668.00 641.00 4.13 HR
Dichlorvos N.D. 1 0.958 0.953 95.80 95.30 0.52
Dimethoate N.D. 1 1.03 0.992 103.00 99.20 3.76
Ethoprophos N.D. 1 1.02 1.03 102.00 103.00 0.98
Etofenprox N.D. 1 0.68 0.719 68.00 71.90 5.58
Etoxazole N.D. 1 1.16 1.09 116.00 109.00 6.22
Fenoxycarb N.D. 1 1.18 1.13 118.00 113.00 4.33
Fenpyroximate N.D. 1 1.06 1.04 106.00 104.00 1.90
Fipronil N.D. 1 0.958 1 95.80 100.00 4.29
Flonicamid N.D. 1 1.05 1.06 105.00 106.00 0.95
Fludioxonil N.D. 1 0.972 1.02 97.20 102.00 4.82
Hexythiazox N.D. 1 0.804 0.833 80.40 83.30 3.54
Imazalil N.D. 1 1.24 1.2 124.00 120.00 3.28
Imidacloprid N.D. 1 1.13 1.15 113.00 115.00 1.75
Kresoxim-methyl N.D. 1 1.4 1.44 140.00 144.00 2.82 HR
Malathion N.D. 1 1.32 1.3 132.00 130.00 1.53 HR
Metalaxyl N.D. 1 1.43 1.41 143.00 141.00 1.41 HR
Methiocarb N.D. 1 0.986 0.975 98.60 97.50 1.12
Methomyl N.D. 1 1.25 1.28 125.00 128.00 2.37
MGK-264 N.D. 1 0.874 0.871 87.40 87.10 0.34
Myclobutanil N.D. 1 1.28 1.28 128.00 128.00 0.00
Naled (dibrom) N.D. 1 1.16 1.09 116.00 109.00 6.22
Oxamyl N.D. 1 1.03 1.03 103.00 103.00 0.00
Paclobutrazol N.D. 1 1.27 1.22 127.00 122.00 4.02
Parathion-methyl N.D. 1 0.855 0.872 85.50 87.20 1.97
Permethrins N.D. 1 0.792 0.82 79.20 82.00 3.47
Phosmet N.D. 1 1.23 1.28 123.00 128.00 3.98
Piperonyl butoxide N.D. 1 1.05 1.01 105.00 101.00 3.88
Prallethrin N.D. 1 1.32 1.28 132.00 128.00 3.08 HR
Propiconazole N.D. 1 0.989 0.967 98.90 96.70 2.25
Propoxur N.D. 1 0.768 0.762 76.80 76.20 0.78
Pyrethrin N.D. 0.65 0.745 0.744 114.62 114.46 0.13
Pyridaben N.D. 1 0.827 0.804 82.70 80.40 2.82
SpinosynA N.D. 0.84 1.13 1.13 134.52 134.52 0.00 HR
SpinosynD N.D. 0.16 0.0855 0.0803 53.44 50.19 6.27 LR
Spiromesifen N.D. 1 2.15 2.12 215.00 212.00 1.41 HR
Spirotetramat N.D. 1 1.39 1.31 139.00 131.00 5.93 HR
Spiroxamine N.D. 1 1.27 1.25 127.00 125.00 1.59
Tebuconazole N.D. 1 1.24 1.13 124.00 113.00 9.28
Thiacloprid N.D. 1 1.12 1.15 112.00 115.00 2.64
Thiamethoxam N.D. 1 1.42 1.46 142.00 146.00 2.78 HR
Trifloxystrobin N.D. 1 1.05 1.04 105.00 104.00 0.96

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113768-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue Cookies
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000008734
Metrc Source Pkg#: 1A4010300016E07000007148
Test Conditions

Prepsheet ID#: ORHS181217b
Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1010 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 113768

Lot #: BC7148
Batch #: 113768
Batch Weight (g): 552.73
Harvest/Process Date: 10/31/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/18/2018
Sample #113768
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 50 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 50 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 50 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 5,000 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 50 50 Pass/<LOD 3-Methylpentane (Hexanes) 50 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 1 100 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 6 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113768-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue Cookies
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000008734
Metrc Source Pkg#: 1A4010300016E07000007148
Test Conditions

Prepsheet ID#: ORHS181217b
Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1010 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 113768

Lot #: BC7148
Batch #: 113768
Batch Weight (g): 552.73
Harvest/Process Date: 10/31/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/18/2018
Sample #113768
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 110 109 44.00 43.60 0.91 LR
Isobutane N.D. 250 159 172 63.60 68.80 7.85 LR
Methanol N.D. 250 443 471 177.20 188.40 6.13 HR
n-Butane N.D. 250 183 197 73.20 78.80 7.37
2,2-Dimethylpropane N.D. 250 210 217 84.00 86.80 3.28
Ethanol N.D. 250 269 286 107.60 114.40 6.13
Isopentane N.D. 250 240 233 96.00 93.20 2.96
Acetonitrile N.D. 250 279 251 111.60 100.40 10.57
Diethyl ether N.D. 250 296 325 118.40 130.00 9.34
2-propanone N.D. 250 322 348 128.80 139.20 7.76 HR
2-propanol N.D. 250 541 582 216.40 232.80 7.30 HR
n-Pentane N.D. 250 202 237 80.80 94.80 15.95
2,2-Dimethylbutane N.D. 250 265 274 106.00 109.60 3.34
2,3-Dimethylbutane N.D. 250 275 264 110.00 105.60 4.08
Methylene chloride N.D. 250 286 284 114.40 113.60 0.70
2-Methylpentane N.D. 250 297 276 118.80 110.40 7.33
3-Methylpentane N.D. 250 294 279 117.60 111.60 5.24
2-Butanol N.D. 250 282 280 112.80 112.00 0.71
n-Hexane N.D. 250 282 267 112.80 106.80 5.46
Ethyl acetate N.D. 250 293 282 117.20 112.80 3.83
Tetrahydrofuran N.D. 250 289 279 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 297 286 0.00 0.00 0.00
Benzene N.D. 250 392 392 156.80 156.80 0.00 HR
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 283 274 113.20 109.60 3.23
Ethylene glycol N.D. 250 245 253 98.00 101.20 3.21
Heptane N.D. 250 382 373 152.80 149.20 2.38 HR
2-Ethoxyethanol N.D. 250 210 262 84.00 104.80 22.03 Q
1,4-Dioxane N.D. 250 398 389 159.20 155.60 2.29 HR
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 375 366 150.00 146.40 2.43 HR
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00 HR
Ethylbenzene N.D. 250 377 374 150.80 149.60 0.80 HR
m-Xylene/p-Xylene N.D. 500 748 747 149.60 149.40 0.13
o-Xylene N.D. 250 371 378 148.40 151.20 1.87
Cumene N.D. 250 372 384 148.80 153.60 3.17
Ethylene oxide N.D. 250 277 283 110.80 113.20 2.14

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113768-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue Cookies
Type: AU Tincture
Metrc Test Pkg#: 1A4010300016E07000008734
Metrc Source Pkg#: 1A4010300016E07000007148
Sample ID#: 113768

Lot #: BC7148
Batch #: 113768
Batch Weight (g): 552.73
Harvest/Process Date: 10/31/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Sample #113768
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 809.61 26.48 48.33 868.05 N.D. N.D. 2.28 30.19 N.D. 4.70 3.95
Increment 2 829.67 27.63 54.59 883.79 N.D. N.D. 2.83 31.51 N.D. 5.23 4.25
Average Value 819.64 27.06 51.46 875.92 N.D. N.D. 2.56 30.85 N.D. 4.97 4.10
Max Value 829.67 27.63 54.59 883.79 N.D. N.D. 2.83 31.51 N.D. 5.23 4.25
Min Value 809.61 26.48 48.33 868.05 N.D. N.D. 2.28 30.19 N.D. 4.70 3.95
Relative Percent Difference (RPD) ±2.45 ±4.28 ±12.16 ±1.80 N.D. N.D. ±21.53 ±4.28 N.D. ±10.67 ±7.32
Average Cannabinoids Per Package 819.64 27.06 51.46 875.92 N.D. N.D. 2.56 30.85 N.D. 4.97 4.10
Average Cannabinoids Per Serving 81.96 2.71 5.15 87.59 N.D. N.D. 0.26 3.09 N.D. 0.50 0.41
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ721
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 7
IRON Laboratories

Oregon Compliant Terpene Report by
Mass Spectrometer
Test Certificate #: 113768-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Blue Cookies
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000008734
Metrc Source Pkg#: 1A4010300016E07000007148
Test Conditions

Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1010 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 113768

Lot #: BC7148
Batch #: 113768
Batch Weight (g): 552.73
Harvest/Process Date: 10/31/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/11/2018
Test Date: 12/18/2018
Sample #113768

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.410 %

β-Ocimene:

0.080 %

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

0.020 %

Sabinene:

 N/D

γ-Terpinene:

0.070 %

Myrcene:

0.350 %

α-Terpinolene:

 N/D

β-Pinene:

0.500 %

Linalool:

0.340 %

∆3-Carene:

 N/D

Fenchone:

0.040 %

α-Terpinene:

0.080 %

Fenchol:

0.250 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.730 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

1.560 %

α-Humulene:

0.670 %

Nerolidol 1:

 N/D

Nerolidol 2:

0.050 %

Guaiol:

0.030 %

Caryophyllene Oxide:

0.060 %

α-Bisabolol:

0.160 %

Other Terpenes

Total: 5.400%
a-Phellandrene = 0.10 % a-Terpineol = 0.22 % Valencene = 0.33 %

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 7