ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113680-001
Client Name, Sample Details

Firehorse Trading
Springfield , OR 97478
Sample: Gorilla Glue #4
License: 020-10059262 C66
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A401030000DAC2000000108
Metrc Source Pkg#: 1A401030000DAC2000000107
***Water Activity: 0.503
***Moisture: 12.943%
Test Conditions

Prepsheet ID#: ORP181207a
Scale: XS205-OR1
Temp: 21.3 °C
Baro Pressure: 1005 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113680

Lot #: HRV4GG4BCPO81318
Batch #: 113680
Batch Weight (g): 3855.54
Harvest/Process Date: 08/13/2018
Date Received: 11/23/2018
Test Date: 12/07/2018
Sample #113680
Sample #113680 Sample #113680
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV Total THC Total CBD
Amount N/D 0.10% N/D 0.08% 0.10% 0.13% 3.55% 20.47% N/D 21.50% 0.09%
LOQ 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05%
Uncertainty 0% RPD 0.00% RPD 0.00% RPD 6.90% RPD 0.00% RPD 0.00% RPD ±5% RPD 4.15% RPD 0% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113680-001
Client Name, Sample Details

Firehorse Trading
Springfield , OR 97478
Sample: Gorilla Glue #4
License: 020-10059262 C66
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A401030000DAC2000000108
Metrc Source Pkg#: 1A401030000DAC2000000107
***Water Activity: 0.503
***Moisture: 12.943%
Test Conditions

Prepsheet ID#: ORP181207a
Scale: XS205-OR1
Temp: 21.3 °C
Baro Pressure: 1005 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113680

Lot #: HRV4GG4BCPO81318
Batch #: 113680
Batch Weight (g): 3855.54
Harvest/Process Date: 08/13/2018
Date Received: 11/23/2018
Test Date: 12/07/2018
Sample #113680
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0%
Cannabidiolic Acid (CBDA) N.D. 1.06 1.07 100.94 1.07 100.94 0.00%
Cannabigerol (CBG) N.D. 0.15 0.15 100.00 0.15 100.00 0.00%
Cannabidiol (CBD) N.D. 0.77 0.75 97.40 0.75 97.40 0.00%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0%
Cannabinol (CBN) N.D. 0.05 0.12 240.00 0.12 240.00 0.00%
Δ9-Tetrahydrocannabinol (THC) N.D. 3.34 3.05 91.32 3.18 95.21 4.17%
Cannabichromene (CBC) N.D. 0.24 0.15 62.50 0.14 58.33 6.90%
Tetrahydrocannabinolic acid (THCA) N.D. 6.45 6.13 95.04 6.39 99.07 4.15%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113680-001
Client Name, Sample Details

Firehorse Trading
Springfield , OR 97478
Sample: Gorilla Glue #4
License: 020-10059262 C66
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030000DAC2000000108
Metrc Source Pkg#: 1A401030000DAC2000000107
Test Conditions

Prepsheet ID#: ORPST181207a
Scale: Veritas-OR1
Temp: 22.2 °C
Baro PE: 1006 hPa
Analyst: JER
Technician: JDM
Sample ID#: 113680

Lot #: HRV4GG4BCPO81318
Batch #: 113680
Batch Weight (g): 3855.54
Harvest/Process Date: 08/13/2018
Date Received: 11/23/2018
Test Date: 12/08/2018
Sample #113680
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.122 Pass/<LOD Abamectin**** 0.500 0.122 Pass/<LOD
Acephate 0.400 0.122 Pass/<LOD Acequinocyl 2.000 0.244 Pass/<LOD
Acetamiprid 0.200 0.122 Pass/<LOD Azoxystrobin 0.200 0.122 Pass/<LOD
Bifenazate 0.200 0.122 Pass/<LOD Bifenthrin 0.200 0.122 Pass/<LOD
Boscalid 0.400 0.122 Pass/<LOD Carbaryl 0.200 0.122 Pass/<LOD
Carbofuran 0.200 0.122 Pass/<LOD Chlorantraniliprole 0.200 0.122 Pass/<LOD
Chlorfenapyr 1.000 0.488 Pass/<LOD Chlorpyrifos 0.200 0.122 Pass/<LOD
Clofentezine 0.200 0.122 Pass/<LOD Cyfluthrin** 1.000 0.488 Pass/<LOD
Cypermethrin*** 1.000 0.488 Pass/<LOD Daminozide 1.000 0.122 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.244 Pass/<LOD Diazinon 0.200 0.122 Pass/<LOD
Dimethoate 0.200 0.122 Pass/<LOD Ethoprophos 0.200 0.122 Pass/<LOD
Etofenprox 0.400 0.122 Pass/<LOD Etoxazole 0.200 0.122 Pass/<LOD
Fenoxycarb 0.200 0.122 Pass/<LOD Fenpyroximate 0.400 0.122 Pass/<LOD
Fipronil 0.400 0.122 Pass/<LOD Flonicamid 1.000 0.122 Pass/<LOD
Fludioxonil 0.400 0.122 Pass/<LOD Hexythiazox 1.000 0.122 Pass/<LOD
Imazalil 0.200 0.122 Pass/<LOD Imidacloprid 0.400 0.122 Pass/<LOD
Kresoxim Methyl 0.400 0.122 Pass/<LOD Malathion 0.200 0.122 Pass/<LOD
Metalaxyl 0.200 0.122 Pass/<LOD Methiocarb 0.200 0.122 Pass/<LOD
Methomyl 0.400 0.122 Pass/<LOD Methyl Parathion 0.200 0.122 Pass/<LOD
MGK-264‡ 0.200 0.122 Pass/<LOD Myclobutanil 0.000 0.122 Pass/<LOD
Naled 0.500 0.122 Pass/<LOD Oxamyl 1.000 0.122 Pass/<LOD
Paclobutrazol 0.400 0.122 Pass/<LOD Permethrins† 0.200 0.122 Pass/<LOD
Phosmet 0.200 0.122 Pass/<LOD Piperonyl Butoxide 2.000 0.122 Pass/<LOD
Prallethrin 0.200 0.122 Pass/<LOD Propiconazole 0.400 0.122 Pass/<LOD
Propoxur 0.200 0.122 Pass/<LOD Pyrethrins* 1.000 0.122 Pass/<LOD
Pyridaben 0.200 0.122 Pass/<LOD Spinosad***** 0.200 0.122 Pass/<LOD
Spiromesifen 0.200 0.122 Pass/<LOD Spirotetramat 0.200 0.122 Pass/<LOD
Spiroxamine‡ 0.400 0.122 Pass/<LOD Tebuconazole 0.400 0.122 Pass/<LOD
Thiacloprid 0.200 0.122 Pass/<LOD Thiamethoxam 0.200 0.122 Pass/<LOD
Trifloxystrobin 0.200 0.122 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113680-001
Client Name, Sample Details

Firehorse Trading
Springfield , OR 97478
Sample: Gorilla Glue #4
License: 020-10059262 C66
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030000DAC2000000108
Metrc Source Pkg#: 1A401030000DAC2000000107
Test Conditions

Prepsheet ID#: ORPST181207a
Scale: Veritas-OR1
Temp: 22.2 °C
Baro PE: 1006 hPa
Analyst: JER
Technician: JDM
Sample ID#: 113680

Lot #: HRV4GG4BCPO81318
Batch #: 113680
Batch Weight (g): 3855.54
Harvest/Process Date: 08/13/2018
Date Received: 11/23/2018
Test Date: 12/08/2018
Sample #113680
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.06 1.06 106.00 106.00 0.00
Acequinocyl N.D. 1 0.51 0.575 51.00 57.50 11.98 LR
Acetamiprid N.D. 1 1.12 1.19 112.00 119.00 6.06
Aldicarb N.D. 1 1.09 1.13 109.00 113.00 3.60
Avermectin B1a N.D. 0.97 1.47 1.37 151.55 141.24 7.04 HR
Azoxystrobin N.D. 1 1 1.02 100.00 102.00 1.98
Bifenazate N.D. 1 0.844 0.821 84.40 82.10 2.76
Bifenthrin N.D. 1 1.2 1.26 120.00 126.00 4.88
Boscalid N.D. 1 0.97 1.03 97.00 103.00 6.00
Carbaryl N.D. 1 1.22 1.22 122.00 122.00 0.00
Carbofuran N.D. 1 1.21 1.21 121.00 121.00 0.00
Chlorantraniliprole N.D. 1 1.09 1.09 109.00 109.00 0.00
Chlorfenapyr N.D. 1 0.863 0.9 86.30 90.00 4.20
Chlorpyriphos N.D. 1 1.22 1.23 122.00 123.00 0.82
Clofentezine N.D. 1 0.885 0.966 88.50 96.60 8.75
Cyfluthrin N.D. 1 1.12 1.15 112.00 115.00 2.64
Cypermethrin N.D. 1 1.36 1.37 136.00 137.00 0.73 HR
Daminoside N.D. 1 0.744 0.671 74.40 67.10 10.32 LR
Diazanon N.D. 1 5.14 5.26 514.00 526.00 2.31 HR
Dichlorvos N.D. 1 1.05 1.1 105.00 110.00 4.65
Dimethoate N.D. 1 1.19 1.26 119.00 126.00 5.71
Ethoprophos N.D. 1 0.979 0.985 97.90 98.50 0.61
Etofenprox N.D. 1 1.19 1.23 119.00 123.00 3.31
Etoxazole N.D. 1 1.24 1.37 124.00 137.00 9.96 HR
Fenoxycarb N.D. 1 1 1.02 100.00 102.00 1.98
Fenpyroximate N.D. 1 1.27 1.36 127.00 136.00 6.84 HR
Fipronil N.D. 1 1.11 1.12 111.00 112.00 0.90
Flonicamid N.D. 1 1.19 1.25 119.00 125.00 4.92
Fludioxonil N.D. 1 1.12 1.11 112.00 111.00 0.90
Hexythiazox N.D. 1 0.507 0.637 50.70 63.70 22.73 LRQ
Imazalil N.D. 1 1.1 0.981 110.00 98.10 11.44
Imidacloprid N.D. 1 1.28 1.29 128.00 129.00 0.78
Kresoxim-methyl N.D. 1 0.881 0.932 88.10 93.20 5.63
Malathion N.D. 1 1.02 1.04 102.00 104.00 1.94
Metalaxyl N.D. 1 1.17 1.25 117.00 125.00 6.61
Methiocarb N.D. 1 1.1 1.11 110.00 111.00 0.90
Methomyl N.D. 1 1.13 1.13 113.00 113.00 0.00
MGK-264 N.D. 1 0.996 1 99.60 100.00 0.40
Myclobutanil N.D. 1 1.1 1.13 110.00 113.00 2.69
Naled (dibrom) N.D. 1 0.599 0.612 59.90 61.20 2.15 LR
Oxamyl N.D. 1 1.25 1.26 125.00 126.00 0.80
Paclobutrazol N.D. 1 1.12 1.14 112.00 114.00 1.77
Parathion-methyl N.D. 1 1.08 1.02 108.00 102.00 5.71
Permethrins N.D. 1 1.21 1.25 121.00 125.00 3.25
Phosmet N.D. 1 1.08 1.11 108.00 111.00 2.74
Piperonyl butoxide N.D. 1 1.15 1.18 115.00 118.00 2.58
Prallethrin N.D. 1 1.06 1.07 106.00 107.00 0.94
Propiconazole N.D. 1 0.964 0.958 96.40 95.80 0.62
Propoxur N.D. 1 1.07 1.1 107.00 110.00 2.76
Pyrethrin N.D. 0.65 0.673 0.668 103.54 102.77 0.75
Pyridaben N.D. 1 1.11 1.17 111.00 117.00 5.26
SpinosynA N.D. 0.84 0.61 0.819 72.62 97.50 29.25 Q
SpinosynD N.D. 0.16 0.106 0.155 66.25 96.88 37.55 Q
Spiromesifen N.D. 1 0.214 0.22 21.40 22.00 2.76 LR
Spirotetramat N.D. 1 0.73 0.767 73.00 76.70 4.94
Spiroxamine N.D. 1 1.09 1.13 109.00 113.00 3.60
Tebuconazole N.D. 1 0.979 1.01 97.90 101.00 3.12
Thiacloprid N.D. 1 1.2 1.22 120.00 122.00 1.65
Thiamethoxam N.D. 1 1.15 1.24 115.00 124.00 7.53
Trifloxystrobin N.D. 1 1.16 1.22 116.00 122.00 5.04

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4
IRON Laboratories

Michigan Compliant Terpene Report by
Mass Spectrometer
Test Certificate #: 113680-001
Client Name, Sample Details

Firehorse Trading
Springfield , OR 97478
Sample: Gorilla Glue #4
License: 020-10059262 C66
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030000DAC2000000108
Metrc Source Pkg#: 1A401030000DAC2000000107
Test Conditions

Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1010 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 113680

Lot #: HRV4GG4BCPO81318
Batch #: 113680
Batch Weight (g): 3855.54
Harvest/Process Date: 08/13/2018
Date Received: 11/23/2018
Test Date: 12/18/2018
Valid Through: 12/18/2019
Report Issued: 12/20/2018
Sample #113680

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.030 %

β-Ocimene:

0.020 %

Camphene:

0.010 %

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

0.010 %

Myrcene:

0.280 %

α-Terpinolene:

 N/D

β-Pinene:

0.060 %

Linalool:

0.060 %

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

0.010 %

Fenchol:

0.050 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.210 %

Geraniol:

0.010 %

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.850 %

α-Humulene:

0.410 %

Nerolidol 1:

 N/D

Nerolidol 2:

0.010 %

Guaiol:

 N/D

Caryophyllene Oxide:

0.060 %

α-Bisabolol:

0.230 %

Other Terpenes

Total: 2.310%
a-Phellandrene = 0.02 % a-Terpineol = 0.05 % Valencene = 0.14 %

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 4