ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113571-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Ray Charles x Grease Monkey sugar wax
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000008337
Metrc Source Pkg#: 1A4010300016E07000007022
Test Conditions

Prepsheet ID#: ORP181206a
Scale: XS205-OR1
Temp: 22.5 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113571

Lot #: RCGM7022
Batch #: 113571
Batch Weight (g): 205.22
Harvest/Process Date: 10/23/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/03/2018
Test Date: 12/06/2018
Sample #113571
Sample #113571 Sample #113571
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Avg
Avg. Amount N/D 30.62 mg/g N/D 2.13 mg/g 6.40 mg/g 6.99 mg/g 59.47 mg/g 845.82 mg/g N/D CBD 26.86 mg/g
LOQ 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g THC 801.25 mg/g
Amount per Serving~ N/D 3.06 mg/srv N/D 0.21 mg/srv 0.64 mg/srv 0.70 mg/srv 5.95 mg/srv 84.58 mg/srv N/D Serving Size~ (g): 0.10 g
Uncertainty 6.44% RPD 3.18% RPD 6.42% RPD 0.36% RPD 8.89% RPD 2.30% RPD 93.30% RPD 1.43% RPD 5.31% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113571-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Ray Charles x Grease Monkey sugar wax
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000008337
Metrc Source Pkg#: 1A4010300016E07000007022
Test Conditions

Prepsheet ID#: ORP181206a
Scale: XS205-OR1
Temp: 22.5 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113571

Lot #: RCGM7022
Batch #: 113571
Batch Weight (g): 205.22
Harvest/Process Date: 10/23/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/03/2018
Test Date: 12/06/2018
Sample #113571
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.2 3.76 89.52 4.01 95.48 6.44%
Cannabidiolic Acid (CBDA) N.D. 4 3.62 90.50 3.84 96.00 5.90%
Cannabigerol (CBG) N.D. 4.27 3.86 90.40 4.1 96.02 6.03%
Cannabidiol (CBD) N.D. 3.86 3.47 89.90 3.7 95.85 6.42%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 4.21 3.85 91.45 4.06 96.44 5.31%
Cannabinol (CBN) N.D. 3.93 3.6 91.60 3.76 95.67 4.35%
Δ9-Tetrahydrocannabinol (THC) N.D. 3.84 3.44 89.58 3.64 94.79 5.65%
Cannabichromene (CBC) N.D. 3.99 3.6 90.23 3.83 95.99 6.19%
Tetrahydrocannabinolic acid (THCA) N.D. 3.67 3.3 89.92 3.51 95.64 6.17%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113571-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Ray Charles x Grease Monkey sugar wax
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000008337
Metrc Source Pkg#: 1A4010300016E07000007022
Test Conditions

Prepsheet ID#: ORPS181205b
Scale: Veritas-OR1
Temp: 22.3 °C
Baro PE: 1001 hPa
Analyst: JER
Technician: JDM
Sample ID#: 113571

Lot #: RCGM7022
Batch #: 113571
Batch Weight (g): 205.22
Harvest/Process Date: 10/23/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/03/2018
Test Date: 12/07/2018
Sample #113571
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.124 Pass/<LOD Abamectin**** 0.500 0.124 Pass/<LOD
Acephate 0.400 0.124 Pass/<LOD Acequinocyl 2.000 0.249 Pass/<LOD
Acetamiprid 0.200 0.124 Pass/<LOD Azoxystrobin 0.200 0.124 Pass/<LOD
Bifenazate 0.200 0.124 Pass/<LOD Bifenthrin 0.200 0.124 Pass/<LOD
Boscalid 0.400 0.124 Pass/<LOD Carbaryl 0.200 0.124 Pass/<LOD
Carbofuran 0.200 0.124 Pass/<LOD Chlorantraniliprole 0.200 0.124 Pass/<LOD
Chlorfenapyr 1.000 0.497 Pass/<LOD Chlorpyrifos 0.200 0.124 Pass/<LOD
Clofentezine 0.200 0.124 Pass/<LOD Cyfluthrin** 1.000 0.497 Pass/<LOD
Cypermethrin*** 1.000 0.497 Pass/<LOD Daminozide 1.000 0.124 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.249 Pass/<LOD Diazinon 0.200 0.124 Pass/<LOD
Dimethoate 0.200 0.124 Pass/<LOD Ethoprophos 0.200 0.124 Pass/<LOD
Etofenprox 0.400 0.124 Pass/<LOD Etoxazole 0.200 0.124 Pass/<LOD
Fenoxycarb 0.200 0.124 Pass/<LOD Fenpyroximate 0.400 0.124 Pass/<LOD
Fipronil 0.400 0.124 Pass/<LOD Flonicamid 1.000 0.124 Pass/<LOD
Fludioxonil 0.400 0.124 Pass/<LOD Hexythiazox 1.000 0.124 Pass/<LOD
Imazalil 0.200 0.124 Pass/<LOD Imidacloprid 0.400 0.124 Pass/<LOD
Kresoxim Methyl 0.400 0.124 Pass/<LOD Malathion 0.200 0.124 Pass/<LOD
Metalaxyl 0.200 0.124 Pass/<LOD Methiocarb 0.200 0.124 Pass/<LOD
Methomyl 0.400 0.124 Pass/<LOD Methyl Parathion 0.200 0.124 Pass/<LOD
MGK-264‡ 0.200 0.124 Pass/<LOD Myclobutanil 0.000 0.124 Pass/<LOD
Naled 0.500 0.124 Pass/<LOD Oxamyl 1.000 0.124 Pass/<LOD
Paclobutrazol 0.400 0.124 Pass/<LOD Permethrins† 0.200 0.124 Pass/<LOD
Phosmet 0.200 0.124 Pass/<LOD Piperonyl Butoxide 2.000 0.124 Pass/<LOD
Prallethrin 0.200 0.124 Pass/<LOD Propiconazole 0.400 0.124 Pass/<LOD
Propoxur 0.200 0.124 Pass/<LOD Pyrethrins* 1.000 0.124 Pass/<LOD
Pyridaben 0.200 0.124 Pass/<LOD Spinosad***** 0.200 0.124 Pass/<LOD
Spiromesifen 0.200 0.124 Pass/<LOD Spirotetramat 0.200 0.124 Pass/<LOD
Spiroxamine‡ 0.400 0.124 Pass/<LOD Tebuconazole 0.400 0.124 Pass/<LOD
Thiacloprid 0.200 0.124 Pass/<LOD Thiamethoxam 0.200 0.124 Pass/<LOD
Trifloxystrobin 0.200 0.124 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113571-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Ray Charles x Grease Monkey sugar wax
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000008337
Metrc Source Pkg#: 1A4010300016E07000007022
Test Conditions

Prepsheet ID#: ORPS181205b
Scale: Veritas-OR1
Temp: 22.3 °C
Baro PE: 1001 hPa
Analyst: JER
Technician: JDM
Sample ID#: 113571

Lot #: RCGM7022
Batch #: 113571
Batch Weight (g): 205.22
Harvest/Process Date: 10/23/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/03/2018
Test Date: 12/07/2018
Sample #113571
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.16 1.21 116.00 121.00 4.22
Acequinocyl N.D. 1 0.258 0.372 25.80 37.20 36.19 LRQ
Acetamiprid N.D. 1 1.23 1.21 123.00 121.00 1.64
Aldicarb N.D. 1 0.992 1.04 99.20 104.00 4.72
Avermectin B1a N.D. 0.97 2.06 1.74 212.37 179.38 16.84 HR
Azoxystrobin N.D. 1 1.34 1.44 134.00 144.00 7.19 HR
Bifenazate N.D. 1 1.57 1.46 157.00 146.00 7.26 HR
Bifenthrin N.D. 1 1.03 1.19 103.00 119.00 14.41
Boscalid N.D. 1 1.21 1.21 121.00 121.00 0.00
Carbaryl N.D. 1 1.06 1.15 106.00 115.00 8.14
Carbofuran N.D. 1 1.32 1.4 132.00 140.00 5.88 HR
Chlorantraniliprole N.D. 1 1.63 1.83 163.00 183.00 11.56 HR
Chlorfenapyr N.D. 1 0.888 0.952 88.80 95.20 6.96
Chlorpyriphos N.D. 1 0.999 1.13 99.90 113.00 12.31
Clofentezine N.D. 1 1.1 1.31 110.00 131.00 17.43 HR
Cyfluthrin N.D. 1 1.23 1.33 123.00 133.00 7.81 HR
Cypermethrin N.D. 1 1.06 1.26 106.00 126.00 17.24
Daminoside N.D. 1 1.03 1.15 103.00 115.00 11.01
Diazanon N.D. 1 6.93 7.4 693.00 740.00 6.56 HR
Dichlorvos N.D. 1 1.04 1.11 104.00 111.00 6.51
Dimethoate N.D. 1 1.15 1.21 115.00 121.00 5.08
Ethoprophos N.D. 1 1.11 1.18 111.00 118.00 6.11
Etofenprox N.D. 1 0.916 1.01 91.60 101.00 9.76
Etoxazole N.D. 1 1.29 1.36 129.00 136.00 5.28 HR
Fenoxycarb N.D. 1 1.45 1.67 145.00 167.00 14.10 HR
Fenpyroximate N.D. 1 1.25 1.36 125.00 136.00 8.43 HR
Fipronil N.D. 1 1.13 1.06 113.00 106.00 6.39
Flonicamid N.D. 1 1.27 1.3 127.00 130.00 2.33
Fludioxonil N.D. 1 1.05 1.08 105.00 108.00 2.82
Hexythiazox N.D. 1 0.812 1.01 81.20 101.00 21.73 Q
Imazalil N.D. 1 1.56 1.54 156.00 154.00 1.29 HR
Imidacloprid N.D. 1 1.39 1.38 139.00 138.00 0.72 HR
Kresoxim-methyl N.D. 1 1.57 1.67 157.00 167.00 6.17 HR
Malathion N.D. 1 1.38 1.46 138.00 146.00 5.63 HR
Metalaxyl N.D. 1 1.51 1.62 151.00 162.00 7.03 HR
Methiocarb N.D. 1 1.12 1.25 112.00 125.00 10.97
Methomyl N.D. 1 1.44 1.49 144.00 149.00 3.41 HR
MGK-264 N.D. 1 1.02 1.09 102.00 109.00 6.64
Myclobutanil N.D. 1 1.65 1.71 165.00 171.00 3.57 HR
Naled (dibrom) N.D. 1 0.653 0.712 65.30 71.20 8.64 LR
Oxamyl N.D. 1 1.25 1.27 125.00 127.00 1.59
Paclobutrazol N.D. 1 1.79 1.79 179.00 179.00 0.00 HR
Parathion-methyl N.D. 1 1.12 1.18 112.00 118.00 5.22
Permethrins N.D. 1 0.962 1.04 96.20 104.00 7.79
Phosmet N.D. 1 1.41 1.56 141.00 156.00 10.10 HR
Piperonyl butoxide N.D. 1 1.24 1.26 124.00 126.00 1.60
Prallethrin N.D. 1 1.44 1.53 144.00 153.00 6.06 HR
Propiconazole N.D. 1 1.33 1.47 133.00 147.00 10.00 HR
Propoxur N.D. 1 1.08 1.17 108.00 117.00 8.00
Pyrethrin N.D. 0.65 0.777 0.886 119.54 136.31 13.11
Pyridaben N.D. 1 1.05 1.08 105.00 108.00 2.82
SpinosynA N.D. 0.84 1.43 1.38 170.24 164.29 3.56 HR
SpinosynD N.D. 0.16 0.263 0.276 164.38 172.50 4.82 HR
Spiromesifen N.D. 1 0.215 0.249 21.50 24.90 14.66 LR
Spirotetramat N.D. 1 1.12 1.05 112.00 105.00 6.45
Spiroxamine N.D. 1 1.51 1.56 151.00 156.00 3.26 HR
Tebuconazole N.D. 1 1.52 1.71 152.00 171.00 11.76 HR
Thiacloprid N.D. 1 1.36 1.43 136.00 143.00 5.02 HR
Thiamethoxam N.D. 1 1.64 1.72 164.00 172.00 4.76 HR
Trifloxystrobin N.D. 1 1.32 1.37 132.00 137.00 3.72 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113571-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Ray Charles x Grease Monkey sugar wax
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000008337
Metrc Source Pkg#: 1A4010300016E07000007022
Test Conditions

Prepsheet ID#: ORHS181206c
Scale: XS205-OR1
Temp: 22 °C
Baro PE: 1001 hPa
Analyst: JER
Technician: 34.2
Sample ID#: 113571

Lot #: RCGM7022
Batch #: 113571
Batch Weight (g): 205.22
Harvest/Process Date: 10/23/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/03/2018
Test Date: 12/10/2018
Sample #113571
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/55
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 150 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113571-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Ray Charles x Grease Monkey sugar wax
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000008337
Metrc Source Pkg#: 1A4010300016E07000007022
Test Conditions

Prepsheet ID#: ORHS181206c
Scale: XS205-OR1
Temp: 22 °C
Baro PE: 1001 hPa
Analyst: JER
Technician: 34.2
Sample ID#: 113571

Lot #: RCGM7022
Batch #: 113571
Batch Weight (g): 205.22
Harvest/Process Date: 10/23/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/03/2018
Test Date: 12/10/2018
Sample #113571
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 191 189 76.40 75.60 1.05
Isobutane N.D. 250 223 229 89.20 91.60 2.65
Methanol N.D. 250 530 323 212.00 129.20 48.53 HRQ
n-Butane N.D. 250 222 224 88.80 89.60 0.90
2,2-Dimethylpropane N.D. 250 239 232 95.60 92.80 2.97
Ethanol N.D. 250 241 235 96.40 94.00 2.52
Isopentane N.D. 250 242 246 96.80 98.40 1.64
Acetonitrile N.D. 250 219 211 87.60 84.40 3.72
Diethyl ether N.D. 250 255 249 102.00 99.60 2.38
2-propanone N.D. 250 220 242 88.00 96.80 9.52
2-propanol N.D. 250 185 188 74.00 75.20 1.61
n-Pentane N.D. 250 287 266 114.80 106.40 7.59
2,2-Dimethylbutane N.D. 250 262 253 104.80 101.20 3.50
2,3-Dimethylbutane N.D. 250 265 247 106.00 98.80 7.03
Methylene chloride N.D. 250 245 239 98.00 95.60 2.48
2-Methylpentane N.D. 250 265 268 106.00 107.20 1.13
3-Methylpentane N.D. 250 269 260 107.60 104.00 3.40
2-Butanol N.D. 250 276 285 110.40 114.00 3.21
n-Hexane N.D. 250 254 248 101.60 99.20 2.39
Ethyl acetate N.D. 250 249 247 99.60 98.80 0.81
Tetrahydrofuran N.D. 250 267 263 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 270 272 0.00 0.00 0.00
Benzene N.D. 250 267 267 106.80 106.80 0.00
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 258 257 103.20 102.80 0.39
Ethylene glycol N.D. 250 276 254 110.40 101.60 8.30
Heptane N.D. 250 276 263 110.40 105.20 4.82
2-Ethoxyethanol N.D. 250 357 354 142.80 141.60 0.84 HR
1,4-Dioxane N.D. 250 284 282 113.60 112.80 0.71
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 265 266 106.00 106.40 0.38
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 278 283 111.20 113.20 1.78
m-Xylene/p-Xylene N.D. 500 554 566 110.80 113.20 2.14
o-Xylene N.D. 250 281 291 112.40 116.40 3.50
Cumene N.D. 250 284 301 113.60 120.40 5.81
Ethylene oxide N.D. 250 221 233 88.40 93.20 5.29

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113571-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Ray Charles x Grease Monkey sugar wax
Type: AU Tincture
Metrc Test Pkg#: 1A4010300016E07000008337
Metrc Source Pkg#: 1A4010300016E07000007022
Sample ID#: 113571

Lot #: RCGM7022
Batch #: 113571
Batch Weight (g): 205.22
Harvest/Process Date: 10/23/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/03/2018
Sample #113571
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 799.91 27.28 63.45 839.75 N.D. N.D. 2.13 31.11 N.D. 6.68 6.91
Increment 2 802.58 26.43 55.48 851.88 N.D. N.D. 2.12 30.14 N.D. 6.11 7.07
Average Value 801.24 26.86 59.47 845.82 N.D. N.D. 2.13 30.63 N.D. 6.40 6.99
Max Value 802.58 27.28 63.45 851.88 N.D. N.D. 2.13 31.11 N.D. 6.68 7.07
Min Value 799.91 26.43 55.48 839.75 N.D. N.D. 2.12 30.14 N.D. 6.11 6.91
Relative Percent Difference (RPD) ±0.33 ±3.17 ±13.40 ±1.43 N.D. N.D. ±0.47 ±3.17 N.D. ±8.91 ±2.29
Average Cannabinoids Per Package 801.24 26.86 59.47 845.82 N.D. N.D. 2.13 30.63 N.D. 6.40 6.99
Average Cannabinoids Per Serving 80.12 2.69 5.95 84.58 N.D. N.D. 0.21 3.06 N.D. 0.64 0.70
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ721
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 7
IRON Laboratories

Oregon Compliant Terpene Report by
Mass Spectrometer
Test Certificate #: 113571-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Ray Charles x Grease Monkey sugar wax
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000008337
Metrc Source Pkg#: 1A4010300016E07000007022
Test Conditions

Scale: XS205-OR1
Temp: 22 °C
Baro Pressure: 1001 hPa
Analyst: JER
Technician: JDM
Sample ID#: 113571

Lot #: RCGM7022
Batch #: 113571
Batch Weight (g): 205.22
Harvest/Process Date: 10/23/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 12/03/2018
Test Date: 12/09/2018
Sample #113571

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.080 %

β-Ocimene:

0.090 %

Camphene:

0.010 %

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

0.040 %

Myrcene:

0.250 %

α-Terpinolene:

0.220 %

β-Pinene:

0.080 %

Linalool:

0.160 %

∆3-Carene:

0.010 %

Fenchone:

0.010 %

α-Terpinene:

0.050 %

Fenchol:

0.090 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.170 %

Geraniol:

0.010 %

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.840 %

α-Humulene:

0.380 %

Nerolidol 1:

 N/D

Nerolidol 2:

0.030 %

Guaiol:

0.040 %

Caryophyllene Oxide:

0.050 %

α-Bisabolol:

0.130 %

Other Terpenes

Total: 2.740%
a-Phellandrene = 0.11 % a-Terpineol = 0.09 % Valencene = 0.09 %

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 7