ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113357-001
Client Name, Sample Details

Country Grow
Corvallis, OR 97333
Sample: Enigma
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300000FA3000000195
Metrc Source Pkg#: 1A4010300000FA3000000180
***Water Activity: 0.566
***Moisture: 14.056%
Test Conditions

Prepsheet ID#: ORP181129a
Scale: XS205-OR1
Temp: 22.2 °C
Baro Pressure: 987.8 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113357

Lot #: Enig18
Batch #: 113357
Batch Weight (g): 6804
Harvest/Process Date: 10/16/2018
Date Received: 11/27/2018
Test Date: 11/29/2018
Sample #113357
Sample #113357 Sample #113357
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV Total THC Total CBD
Amount N/D 0.13% N/D N/D 0.20% 0.10% 0.93% 23.85% N/D 21.85% 0.11%
LOQ 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05%
Uncertainty 0% RPD 4.04% RPD 4.26% RPD 18.18% RPD 6.90% RPD 16.67% RPD ±5% RPD 1.86% RPD 0% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113357-001
Client Name, Sample Details

Country Grow
Corvallis, OR 97333
Sample: Enigma
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300000FA3000000195
Metrc Source Pkg#: 1A4010300000FA3000000180
***Water Activity: 0.566
***Moisture: 14.056%
Test Conditions

Prepsheet ID#: ORP181129a
Scale: XS205-OR1
Temp: 22.2 °C
Baro Pressure: 987.8 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113357

Lot #: Enig18
Batch #: 113357
Batch Weight (g): 6804
Harvest/Process Date: 10/16/2018
Date Received: 11/27/2018
Test Date: 11/29/2018
Sample #113357
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0%
Cannabidiolic Acid (CBDA) N.D. 1.06 0.97 91.51 1.01 95.28 4.04%
Cannabigerol (CBG) N.D. 0.15 0.14 93.33 0.15 100.00 6.90%
Cannabidiol (CBD) N.D. 0.77 0.69 89.61 0.72 93.51 4.26%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0%
Cannabinol (CBN) N.D. 0.05 0.11 220.00 0.13 260.00 16.67%
Δ9-Tetrahydrocannabinol (THC) N.D. 3.34 2.93 87.72 2.87 85.93 2.07%
Cannabichromene (CBC) N.D. 0.24 0.15 62.50 0.18 75.00 18.18%
Tetrahydrocannabinolic acid (THCA) N.D. 6.45 5.86 90.85 5.97 92.56 1.86%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113357-001
Client Name, Sample Details

Country Grow
Corvallis, OR 97333
Sample: Enigma
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300000FA3000000195
Metrc Source Pkg#: 1A4010300000FA3000000180
Test Conditions

Prepsheet ID#: ORPS181128a
Scale: Veritas-OR1
Temp: 22.3 °C
Baro PE: 990 hPa
Analyst: JER
Technician: JDM
Sample ID#: 113357

Lot #: Enig18
Batch #: 113357
Batch Weight (g): 6804
Harvest/Process Date: 10/16/2018
Date Received: 11/27/2018
Test Date: 12/04/2018
Sample #113357
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.142 Pass/<LOD Abamectin**** 0.500 0.142 Pass/<LOD
Acephate 0.400 0.142 Pass/<LOD Acequinocyl 2.000 0.285 Pass/<LOD
Acetamiprid 0.200 0.142 Pass/<LOD Azoxystrobin 0.200 0.142 Pass/<LOD
Bifenazate 0.200 0.142 Pass/<LOD Bifenthrin 0.200 0.142 Pass/<LOD
Boscalid 0.400 0.142 Pass/<LOD Carbaryl 0.200 0.142 Pass/<LOD
Carbofuran 0.200 0.142 Pass/<LOD Chlorantraniliprole 0.200 0.142 Pass/<LOD
Chlorfenapyr 1.000 0.569 Pass/<LOD Chlorpyrifos 0.200 0.142 Failed/0.810
Clofentezine 0.200 0.142 Pass/<LOD Cyfluthrin** 1.000 0.569 Pass/<LOD
Cypermethrin*** 1.000 0.569 Pass/<LOD Daminozide 1.000 0.142 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.285 Pass/<LOD Diazinon 0.200 0.142 Pass/<LOD
Dimethoate 0.200 0.142 Pass/<LOD Ethoprophos 0.200 0.142 Pass/<LOD
Etofenprox 0.400 0.142 Pass/<LOD Etoxazole 0.200 0.142 Pass/<LOD
Fenoxycarb 0.200 0.142 Pass/<LOD Fenpyroximate 0.400 0.142 Pass/<LOD
Fipronil 0.400 0.142 Pass/<LOD Flonicamid 1.000 0.142 Pass/<LOD
Fludioxonil 0.400 0.142 Pass/<LOD Hexythiazox 1.000 0.142 Pass/<LOD
Imazalil 0.200 0.142 Pass/<LOD Imidacloprid 0.400 0.142 Pass/<LOD
Kresoxim Methyl 0.400 0.142 Pass/<LOD Malathion 0.200 0.142 Pass/<LOD
Metalaxyl 0.200 0.142 Pass/<LOD Methiocarb 0.200 0.142 Pass/<LOD
Methomyl 0.400 0.142 Pass/<LOD Methyl Parathion 0.200 0.142 Pass/<LOD
MGK-264‡ 0.200 0.142 Pass/<LOD Myclobutanil 0.000 0.142 Pass/<LOD
Naled 0.500 0.142 Pass/<LOD Oxamyl 1.000 0.142 Pass/<LOD
Paclobutrazol 0.400 0.142 Pass/<LOD Permethrins† 0.200 0.142 Pass/<LOD
Phosmet 0.200 0.142 Pass/<LOD Piperonyl Butoxide 2.000 0.142 Pass/<LOD
Prallethrin 0.200 0.142 Pass/<LOD Propiconazole 0.400 0.142 Pass/<LOD
Propoxur 0.200 0.142 Pass/<LOD Pyrethrins* 1.000 0.142 Pass/<LOD
Pyridaben 0.200 0.142 Pass/<LOD Spinosad***** 0.200 0.142 Pass/<LOD
Spiromesifen 0.200 0.142 Pass/<LOD Spirotetramat 0.200 0.142 Pass/<LOD
Spiroxamine‡ 0.400 0.142 Pass/<LOD Tebuconazole 0.400 0.142 Pass/<LOD
Thiacloprid 0.200 0.142 Pass/<LOD Thiamethoxam 0.200 0.142 Pass/<LOD
Trifloxystrobin 0.200 0.142 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113357-001
Client Name, Sample Details

Country Grow
Corvallis, OR 97333
Sample: Enigma
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300000FA3000000195
Metrc Source Pkg#: 1A4010300000FA3000000180
Test Conditions

Prepsheet ID#: ORPS181128a
Scale: Veritas-OR1
Temp: 22.3 °C
Baro PE: 990 hPa
Analyst: JER
Technician: JDM
Sample ID#: 113357

Lot #: Enig18
Batch #: 113357
Batch Weight (g): 6804
Harvest/Process Date: 10/16/2018
Date Received: 11/27/2018
Test Date: 12/04/2018
Sample #113357
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.06 1.07 106.00 107.00 0.94
Acequinocyl N.D. 1 0.518 0.581 51.80 58.10 11.46 LR
Acetamiprid N.D. 1 1.2 1.16 120.00 116.00 3.39
Aldicarb N.D. 1 1.04 1.04 104.00 104.00 0.00
Avermectin B1a N.D. 0.97 1.14 1.23 117.53 126.80 7.59
Azoxystrobin N.D. 1 1.19 1.09 119.00 109.00 8.77
Bifenazate N.D. 1 0.931 0.922 93.10 92.20 0.97
Bifenthrin N.D. 1 1.25 1.22 125.00 122.00 2.43
Boscalid N.D. 1 1.1 1.12 110.00 112.00 1.80
Carbaryl N.D. 1 1.09 1.23 109.00 123.00 12.07
Carbofuran N.D. 1 1.2 1.2 120.00 120.00 0.00
Chlorantraniliprole N.D. 1 1.1 1.05 110.00 105.00 4.65
Chlorfenapyr N.D. 1 0.87 0.829 87.00 82.90 4.83
Chlorpyriphos N.D. 1 1.06 1.11 106.00 111.00 4.61
Clofentezine N.D. 1 1.03 1.01 103.00 101.00 1.96
Cyfluthrin N.D. 1 1.16 1.25 116.00 125.00 7.47
Cypermethrin N.D. 1 1.32 1.12 132.00 112.00 16.39
Daminoside N.D. 1 0.532 0.612 53.20 61.20 13.99 LR
Diazanon N.D. 1 4.89 4.78 489.00 478.00 2.28 HR
Dichlorvos N.D. 1 1.14 1.06 114.00 106.00 7.27
Dimethoate N.D. 1 1.18 1.23 118.00 123.00 4.15
Ethoprophos N.D. 1 1.08 1.03 108.00 103.00 4.74
Etofenprox N.D. 1 1.21 1.24 121.00 124.00 2.45
Etoxazole N.D. 1 1.19 1.3 119.00 130.00 8.84
Fenoxycarb N.D. 1 1.14 1.1 114.00 110.00 3.57
Fenpyroximate N.D. 1 1.29 1.38 129.00 138.00 6.74
Fipronil N.D. 1 0.961 1.03 96.10 103.00 6.93
Flonicamid N.D. 1 1.23 1.22 123.00 122.00 0.82
Fludioxonil N.D. 1 1.02 1.04 102.00 104.00 1.94
Hexythiazox N.D. 1 0.915 0.862 91.50 86.20 5.97
Imazalil N.D. 1 1.09 1.17 109.00 117.00 7.08
Imidacloprid N.D. 1 1.22 1.23 122.00 123.00 0.82
Kresoxim-methyl N.D. 1 1.09 1.03 109.00 103.00 5.66
Malathion N.D. 1 1.08 1.08 108.00 108.00 0.00
Metalaxyl N.D. 1 1.17 1.18 117.00 118.00 0.85
Methiocarb N.D. 1 1.17 1.16 117.00 116.00 0.86
Methomyl N.D. 1 1.13 1.14 113.00 114.00 0.88
MGK-264 N.D. 1 1.23 1.18 123.00 118.00 4.15
Myclobutanil N.D. 1 1.15 1.21 115.00 121.00 5.08
Naled (dibrom) N.D. 1 0.643 0.605 64.30 60.50 6.09 LR
Oxamyl N.D. 1 1.24 1.28 124.00 128.00 3.17
Paclobutrazol N.D. 1 1.12 1.09 112.00 109.00 2.71
Parathion-methyl N.D. 1 0.869 0.993 86.90 99.30 13.32
Permethrins N.D. 1 1.28 1.25 128.00 125.00 2.37
Phosmet N.D. 1 1.09 1.08 109.00 108.00 0.92
Piperonyl butoxide N.D. 1 1.13 1.16 113.00 116.00 2.62
Prallethrin N.D. 1 1.07 1.05 107.00 105.00 1.89
Propiconazole N.D. 1 0.95 0.943 95.00 94.30 0.74
Propoxur N.D. 1 1.04 0.976 104.00 97.60 6.35
Pyrethrin N.D. 0.65 0.637 0.618 98.00 95.08 3.03
Pyridaben N.D. 1 1.09 1.16 109.00 116.00 6.22
SpinosynA N.D. 0.84 0.696 0.647 82.86 77.02 7.30
SpinosynD N.D. 0.16 0.169 0.15 105.63 93.75 11.91
Spiromesifen N.D. 1 0.217 0.242 21.70 24.20 10.89 LR
Spirotetramat N.D. 1 0.804 0.795 80.40 79.50 1.13
Spiroxamine N.D. 1 1.09 1.12 109.00 112.00 2.71
Tebuconazole N.D. 1 1.07 1.03 107.00 103.00 3.81
Thiacloprid N.D. 1 1.16 1.16 116.00 116.00 0.00
Thiamethoxam N.D. 1 1.2 1.21 120.00 121.00 0.83
Trifloxystrobin N.D. 1 1.27 1.32 127.00 132.00 3.86 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4
IRON Laboratories

Oregon Compliant Terpene Report by
Mass Spectrometer
Test Certificate #: 113357-001
Client Name, Sample Details

Country Grow
Corvallis, OR 97333
Sample: Enigma
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300000FA3000000195
Metrc Source Pkg#: 1A4010300000FA3000000180
Test Conditions

Scale: XS205-OR1
Temp: 22 °C
Baro Pressure: 1001 hPa
Analyst: JER
Technician: JDM
Sample ID#: 113357

Lot #: Enig18
Batch #: 113357
Batch Weight (g): 6804
Harvest/Process Date: 10/16/2018
Date Received: 11/27/2018
Test Date: 12/07/2018
Sample #113357

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.320 %

β-Ocimene:

0.080 %

Camphene:

0.020 %

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

0.010 %

Myrcene:

0.540 %

α-Terpinolene:

0.060 %

β-Pinene:

0.270 %

Linalool:

0.080 %

∆3-Carene:

 N/D

Fenchone:

0.010 %

α-Terpinene:

0.020 %

Fenchol:

0.040 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.190 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.440 %

α-Humulene:

0.230 %

Nerolidol 1:

 N/D

Nerolidol 2:

0.030 %

Guaiol:

0.050 %

Caryophyllene Oxide:

0.020 %

α-Bisabolol:

0.140 %

Other Terpenes

Total: 2.550%
a-Phellandrene = 0.03 % a-Terpineol = 0.05 % Valencene = 0.08 %

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4