ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113094-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Jack Herrer x GG12 Live Resin
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000007423
Metrc Source Pkg#: 1A4010300016E07000006857
Test Conditions

Prepsheet ID#: ORP181116a
Scale: XS205-OR1
Temp: 21.2 °C
Baro Pressure: 1006 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113094

Lot #: JHGG
Batch #: 113094
Batch Weight (g): 842.48
Harvest/Process Date: 10/15/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 11/13/2018
Test Date: 11/16/2018
Sample #113094
Sample #113094 Sample #113094
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Avg
Avg. Amount N/D 71.21 mg/g N/D 2.23 mg/g 7.72 mg/g 4.19 mg/g 87.82 mg/g 501.34 mg/g N/D CBD 62.45 mg/g
LOQ 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g THC 527.50 mg/g
Amount per Serving~ N/D 7.12 mg/srv N/D 0.22 mg/srv 0.77 mg/srv 0.42 mg/srv 8.78 mg/srv 50.13 mg/srv N/D Serving Size~ (g): 0.10 g
Uncertainty 4.93% RPD 2.71% RPD 4.73% RPD 7.96% RPD 2.41% RPD 2.52% RPD 98.80% RPD 2.28% RPD 3.75% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113094-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Jack Herrer x GG12 Live Resin
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000007423
Metrc Source Pkg#: 1A4010300016E07000006857
Test Conditions

Prepsheet ID#: ORP181116a
Scale: XS205-OR1
Temp: 21.2 °C
Baro Pressure: 1006 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 113094

Lot #: JHGG
Batch #: 113094
Batch Weight (g): 842.48
Harvest/Process Date: 10/15/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 11/13/2018
Test Date: 11/16/2018
Sample #113094
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 3.85 3.56 92.47 3.74 97.14 4.93%
Cannabidiolic Acid (CBDA) N.D. 3.68 3.47 94.29 3.61 98.10 3.95%
Cannabigerol (CBG) N.D. 3.92 3.68 93.88 3.86 98.47 4.77%
Cannabidiol (CBD) N.D. 3.55 3.3 92.96 3.46 97.46 4.73%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 3.86 3.66 94.82 3.8 98.45 3.75%
Cannabinol (CBN) N.D. 3.58 3.44 96.09 3.51 98.04 2.01%
Δ9-Tetrahydrocannabinol (THC) N.D. 3.38 3.22 95.27 3.29 97.34 2.15%
Cannabichromene (CBC) N.D. 3.57 3.38 94.68 3.55 99.44 4.91%
Tetrahydrocannabinolic acid (THCA) N.D. 3.39 3.21 94.69 3.37 99.41 4.86%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113094-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Jack Herrer x GG12 Live Resin
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000007423
Metrc Source Pkg#: 1A4010300016E07000006857
Test Conditions

Prepsheet ID#: ORPS181115a
Scale: Veritas-OR1
Temp: 21.21 °C
Baro PE: 1008 hPa
Analyst: JER
Technician: JDM
Sample ID#: 113094

Lot #: JHGG
Batch #: 113094
Batch Weight (g): 842.48
Harvest/Process Date: 10/15/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 11/13/2018
Test Date: 07/16/2018
Sample #113094
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.123 Pass/<LOD Abamectin**** 0.500 0.123 Pass/<LOD
Acephate 0.400 0.123 Pass/<LOD Acequinocyl 2.000 0.245 Pass/<LOD
Acetamiprid 0.200 0.123 Pass/<LOD Azoxystrobin 0.200 0.123 Pass/<LOD
Bifenazate 0.200 0.123 Pass/<LOD Bifenthrin 0.200 0.123 Pass/<LOD
Boscalid 0.400 0.123 Pass/<LOD Carbaryl 0.200 0.123 Pass/<LOD
Carbofuran 0.200 0.123 Pass/<LOD Chlorantraniliprole 0.200 0.123 Pass/<LOD
Chlorfenapyr 1.000 0.491 Pass/<LOD Chlorpyrifos 0.200 0.123 Pass/<LOD
Clofentezine 0.200 0.123 Pass/<LOD Cyfluthrin** 1.000 0.491 Pass/<LOD
Cypermethrin*** 1.000 0.491 Pass/<LOD Daminozide 1.000 0.123 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.245 Pass/<LOD Diazinon 0.200 0.123 Pass/<LOD
Dimethoate 0.200 0.123 Pass/<LOD Ethoprophos 0.200 0.123 Pass/<LOD
Etofenprox 0.400 0.123 Pass/<LOD Etoxazole 0.200 0.123 Pass/<LOD
Fenoxycarb 0.200 0.123 Pass/<LOD Fenpyroximate 0.400 0.123 Pass/<LOD
Fipronil 0.400 0.123 Pass/<LOD Flonicamid 1.000 0.123 Pass/<LOD
Fludioxonil 0.400 0.123 Pass/<LOD Hexythiazox 1.000 0.123 Pass/<LOD
Imazalil 0.200 0.123 Pass/<LOD Imidacloprid 0.400 0.123 Pass/<LOD
Kresoxim Methyl 0.400 0.123 Pass/<LOD Malathion 0.200 0.123 Pass/<LOD
Metalaxyl 0.200 0.123 Pass/<LOD Methiocarb 0.200 0.123 Pass/<LOD
Methomyl 0.400 0.123 Pass/<LOD Methyl Parathion 0.200 0.123 Pass/<LOD
MGK-264‡ 0.200 0.123 Pass/<LOD Myclobutanil 0.000 0.123 Pass/<LOD
Naled 0.500 0.123 Pass/<LOD Oxamyl 1.000 0.123 Pass/<LOD
Paclobutrazol 0.400 0.123 Pass/<LOD Permethrins† 0.200 0.123 Pass/<LOD
Phosmet 0.200 0.123 Pass/<LOD Piperonyl Butoxide 2.000 0.123 Pass/<LOD
Prallethrin 0.200 0.123 Pass/<LOD Propiconazole 0.400 0.123 Pass/<LOD
Propoxur 0.200 0.123 Pass/<LOD Pyrethrins* 1.000 0.123 Pass/<LOD
Pyridaben 0.200 0.123 Pass/<LOD Spinosad***** 0.200 0.123 Pass/<LOD
Spiromesifen 0.200 0.123 Pass/<LOD Spirotetramat 0.200 0.123 Pass/<LOD
Spiroxamine‡ 0.400 0.123 Pass/<LOD Tebuconazole 0.400 0.123 Pass/<LOD
Thiacloprid 0.200 0.123 Pass/<LOD Thiamethoxam 0.200 0.123 Pass/<LOD
Trifloxystrobin 0.200 0.123 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113094-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Jack Herrer x GG12 Live Resin
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000007423
Metrc Source Pkg#: 1A4010300016E07000006857
Test Conditions

Prepsheet ID#: ORPS181115a
Scale: Veritas-OR1
Temp: 21.21 °C
Baro PE: 1008 hPa
Analyst: JER
Technician: JDM
Sample ID#: 113094

Lot #: JHGG
Batch #: 113094
Batch Weight (g): 842.48
Harvest/Process Date: 10/15/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 11/13/2018
Test Date: 07/16/2018
Sample #113094
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.28 1.22 128.00 122.00 4.80
Acequinocyl N.D. 1 0.424 0.372 42.40 37.20 13.07 LR
Acetamiprid N.D. 1 1.37 1.29 137.00 129.00 6.02 HR
Aldicarb N.D. 1 1.06 1.04 106.00 104.00 1.90
Avermectin B1a N.D. 0.97 1.63 1.61 168.04 165.98 1.23 HR
Azoxystrobin N.D. 1 1.46 1.37 146.00 137.00 6.36 HR
Bifenazate N.D. 1 1.29 1.09 129.00 109.00 16.81
Bifenthrin N.D. 1 1.15 1.04 115.00 104.00 10.05
Boscalid N.D. 1 1.18 1.22 118.00 122.00 3.33
Carbaryl N.D. 1 1.19 1.07 119.00 107.00 10.62
Carbofuran N.D. 1 1.43 1.4 143.00 140.00 2.12 HR
Chlorantraniliprole N.D. 1 1.84 1.67 184.00 167.00 9.69 HR
Chlorfenapyr N.D. 1 1.01 0.88 101.00 88.00 13.76
Chlorpyriphos N.D. 1 1.09 1.05 109.00 105.00 3.74
Clofentezine N.D. 1 1.25 1.16 125.00 116.00 7.47
Cyfluthrin N.D. 1 1.37 1.27 137.00 127.00 7.58 HR
Cypermethrin N.D. 1 1.14 1.06 114.00 106.00 7.27
Daminoside N.D. 1 0.925 0.858 92.50 85.80 7.52
Diazanon N.D. 1 5.99 5.48 599.00 548.00 8.89 HR
Dichlorvos N.D. 1 1.12 1.08 112.00 108.00 3.64
Dimethoate N.D. 1 1.26 1.16 126.00 116.00 8.26
Ethoprophos N.D. 1 1.27 1.17 127.00 117.00 8.20
Etofenprox N.D. 1 1.07 0.958 107.00 95.80 11.05
Etoxazole N.D. 1 1.36 1.22 136.00 122.00 10.85 HR
Fenoxycarb N.D. 1 1.68 1.58 168.00 158.00 6.13 HR
Fenpyroximate N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Fipronil N.D. 1 1.04 1.14 104.00 114.00 9.17
Flonicamid N.D. 1 1.35 1.27 135.00 127.00 6.11 HR
Fludioxonil N.D. 1 1.16 1.11 116.00 111.00 4.41
Hexythiazox N.D. 1 1.03 0.966 103.00 96.60 6.41
Imazalil N.D. 1 1.52 1.41 152.00 141.00 7.51 HR
Imidacloprid N.D. 1 1.42 1.36 142.00 136.00 4.32 HR
Kresoxim-methyl N.D. 1 1.74 1.63 174.00 163.00 6.53 HR
Malathion N.D. 1 1.54 1.35 154.00 135.00 13.15 HR
Metalaxyl N.D. 1 1.67 1.5 167.00 150.00 10.73 HR
Methiocarb N.D. 1 1.23 1.18 123.00 118.00 4.15
Methomyl N.D. 1 1.47 1.36 147.00 136.00 7.77 HR
MGK-264 N.D. 1 1.17 0.959 117.00 95.90 19.82
Myclobutanil N.D. 1 1.81 1.7 181.00 170.00 6.27 HR
Naled (dibrom) N.D. 1 0.712 0.733 71.20 73.30 2.91
Oxamyl N.D. 1 1.34 1.24 134.00 124.00 7.75 HR
Paclobutrazol N.D. 1 1.82 1.75 182.00 175.00 3.92 HR
Parathion-methyl N.D. 1 1.19 1.19 119.00 119.00 0.00
Permethrins N.D. 1 1.08 1.04 108.00 104.00 3.77
Phosmet N.D. 1 1.62 1.43 162.00 143.00 12.46 HR
Piperonyl butoxide N.D. 1 1.34 1.27 134.00 127.00 5.36 HR
Prallethrin N.D. 1 1.61 1.42 161.00 142.00 12.54 HR
Propiconazole N.D. 1 1.41 1.28 141.00 128.00 9.67 HR
Propoxur N.D. 1 1.23 1.25 123.00 125.00 1.61
Pyrethrin N.D. 0.65 0.929 0.852 142.92 131.08 8.65 HR
Pyridaben N.D. 1 1.13 0.991 113.00 99.10 13.11
SpinosynA N.D. 0.84 1.28 1.14 152.38 135.71 11.57 HR
SpinosynD N.D. 0.16 0.262 0.241 163.75 150.63 8.35 HR
Spiromesifen N.D. 1 0.181 0.177 18.10 17.70 2.23 LR
Spirotetramat N.D. 1 1.12 1.04 112.00 104.00 7.41
Spiroxamine N.D. 1 1.58 1.42 158.00 142.00 10.67 HR
Tebuconazole N.D. 1 1.77 1.7 177.00 170.00 4.03 HR
Thiacloprid N.D. 1 1.57 1.44 157.00 144.00 8.64 HR
Thiamethoxam N.D. 1 1.75 1.65 175.00 165.00 5.88 HR
Trifloxystrobin N.D. 1 1.36 1.17 136.00 117.00 15.02 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 113094-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Jack Herrer x GG12 Live Resin
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000007423
Metrc Source Pkg#: 1A4010300016E07000006857
Test Conditions

Prepsheet ID#: ORHS181115a
Scale: XS205-OR1
Temp: 20.9 °C
Baro Pressure: 1013 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 113094

Lot #: JHGG
Batch #: 113094
Batch Weight (g): 842.48
Harvest/Process Date: 10/15/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 11/13/2018
Test Date: 11/17/2018
Sample #113094
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 50 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 50 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 50 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 5,000 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/117
2-Propanone (Acetone) 50 50 Pass/81 3-Methylpentane (Hexanes) 50 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 1 100 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 6 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 113094-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Jack Herrer x GG12 Live Resin
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000007423
Metrc Source Pkg#: 1A4010300016E07000006857
Test Conditions

Prepsheet ID#: ORHS181115a
Scale: XS205-OR1
Temp: 20.9 °C
Baro Pressure: 1013 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 113094

Lot #: JHGG
Batch #: 113094
Batch Weight (g): 842.48
Harvest/Process Date: 10/15/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 11/13/2018
Test Date: 11/17/2018
Sample #113094
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 0 0 0.00 0.00 LR
Isobutane N.D. 250 39 38 15.60 15.20 2.60 LR
Methanol N.D. 250 163 195 65.20 78.00 17.88 LR
n-Butane N.D. 250 47 52 18.80 20.80 10.10 LR
2,2-Dimethylpropane N.D. 250 57 60 22.80 24.00 5.13
Ethanol N.D. 250 165 193 66.00 77.20 15.64 LR
Isopentane N.D. 250 85 89 34.00 35.60 4.60 LR
Acetonitrile N.D. 250 182 192 72.80 76.80 5.35
Diethyl ether N.D. 250 148 152 59.20 60.80 2.67 LR
2-propanone N.D. 250 139 144 55.60 57.60 3.53 LR
2-propanol N.D. 250 342 450 136.80 180.00 27.27 Q
n-Pentane N.D. 250 88 66 35.20 26.40 28.57 Q
2,2-Dimethylbutane N.D. 250 114 119 45.60 47.60 4.29 LR
2,3-Dimethylbutane N.D. 250 124 129 49.60 51.60 3.95 LR
Methylene chloride N.D. 250 170 183 68.00 73.20 7.37
2-Methylpentane N.D. 250 123 131 49.20 52.40 6.30 LR
3-Methylpentane N.D. 250 131 134 52.40 53.60 2.26 LR
2-Butanol N.D. 250 188 209 75.20 83.60 10.58
n-Hexane N.D. 250 140 142 56.00 56.80 1.42 LR
Ethyl acetate N.D. 250 174 193 69.60 77.20 10.35
Tetrahydrofuran N.D. 250 179 189 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 184 198 0.00 0.00 0.00
Benzene N.D. 250 197 194 78.80 77.60 1.53
Chloroform N.D. 250 0 0 0.00 0.00
Cyclohexane N.D. 250 166 169 66.40 67.60 1.79 LR
Ethylene glycol N.D. 250 165 204 66.00 81.60 21.14 Q
Heptane N.D. 250 171 162 68.40 64.80 5.41 LR
2-Ethoxyethanol N.D. 250 184 208 73.60 83.20 12.24
1,4-Dioxane N.D. 250 193 200 77.20 80.00 3.56
Pyridine N.D. 250 0 0 0.00 0.00 0.00
Toluene N.D. 250 228 214 91.20 85.60 6.33
Chlorobenzene N.D. 250 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 308 272 123.20 108.80 12.41
m-Xylene/p-Xylene N.D. 500 660 582 132.00 116.40 12.56 HR
o-Xylene N.D. 250 350 307 140.00 122.80 13.09
Cumene N.D. 250 409 349 163.60 139.60 15.83 HR
Ethylene oxide N.D. 250 125 142 50.00 56.80 12.73 LR

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 7

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 113094-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Jack Herrer x GG12 Live Resin
Type: AU Tincture
Metrc Test Pkg#: 1A4010300016E07000007423
Metrc Source Pkg#: 1A4010300016E07000006857
Sample ID#: 113094

Lot #: JHGG
Batch #: 113094
Batch Weight (g): 842.48
Harvest/Process Date: 10/15/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 11/13/2018
Sample #113094
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 523.55 63.29 88.87 495.64 N.D. N.D. 2.32 72.17 N.D. 7.81 4.24
Increment 2 531.45 61.60 86.77 507.05 N.D. N.D. 2.14 70.24 N.D. 7.62 4.13
Average Value 527.50 62.45 87.82 501.34 N.D. N.D. 2.23 71.21 N.D. 7.72 4.19
Max Value 531.45 63.29 88.87 507.05 N.D. N.D. 2.32 72.17 N.D. 7.81 4.24
Min Value 523.55 61.60 86.77 495.64 N.D. N.D. 2.14 70.24 N.D. 7.62 4.13
Relative Percent Difference (RPD) ±1.50 ±2.71 ±2.39 ±2.28 N.D. N.D. ±7.96 ±2.71 N.D. ±2.41 ±2.52
Average Cannabinoids Per Package 527.50 62.45 87.82 501.34 N.D. N.D. 2.23 71.21 N.D. 7.72 4.19
Average Cannabinoids Per Serving 52.75 6.24 8.78 50.13 N.D. N.D. 0.22 7.12 N.D. 0.77 0.42
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ721
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 7
IRON Laboratories

Oregon Compliant Terpene Report by
Mass Spectrometer
Test Certificate #: 113094-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Jack Herrer x GG12 Live Resin
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000007423
Metrc Source Pkg#: 1A4010300016E07000006857
Test Conditions

Scale: XS205-OR1
Temp: 20.9 °C
Baro Pressure: 1013 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 113094

Lot #: JHGG
Batch #: 113094
Batch Weight (g): 842.48
Harvest/Process Date: 10/15/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 11/13/2018
Test Date: 11/17/2018
Sample #113094

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.440 %

β-Ocimene:

0.800 %

Camphene:

0.060 %

Eucalyptol (1,8-Cineol):

0.030 %

Sabinene:

0.020 %

γ-Terpinene:

0.100 %

Myrcene:

0.720 %

α-Terpinolene:

1.070 %

β-Pinene:

0.420 %

Linalool:

0.020 %

∆3-Carene:

0.060 %

Fenchone:

 N/D

α-Terpinene:

0.210 %

Fenchol:

0.040 %

Ocimene:

0.050 %

Isopulegol:

 N/D

Limonene:

0.310 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.780 %

α-Humulene:

0.400 %

Nerolidol 1:

0.020 %

Nerolidol 2:

0.020 %

Guaiol:

 N/D

Caryophyllene Oxide:

0.020 %

α-Bisabolol:

 N/D

Other Terpenes

Total: 5.590%
a-Phellandrene = 0.61 % a-Terpineol = 0.04 % Valencene = 0.14 %

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 7