ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 112751-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Trainwreck Animal Cookies Live Resin
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000006963
Metrc Source Pkg#: 1A4010300016E07000006856
Test Conditions

Prepsheet ID#: ORP181101a
Scale: XS205-OR1
Temp: 20.2 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 112751

Lot #: TRAC
Batch #: 112751
Batch Weight (g): 1113.4
Harvest/Process Date: 10/11/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 10/29/2018
Test Date: 11/01/2018
Sample #112751
Sample #112751 Sample #112751
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Avg
Avg. Amount N/D 69.10 mg/g N/D 3.61 mg/g 6.08 mg/g 4.03 mg/g 45.47 mg/g 662.34 mg/g N/D CBD 60.60 mg/g
LOQ 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g 0.05 mg/g THC 626.35 mg/g
Amount per Serving~ N/D 6.91 mg/srv N/D 0.36 mg/srv 0.61 mg/srv 0.40 mg/srv 4.55 mg/srv 66.23 mg/srv N/D Serving Size~ (g): 0.10 g
Uncertainty 3.08% RPD 101.54% RPD 3.32% RPD 79.60% RPD 90.93% RPD 15.38% RPD 74.41% RPD 69.41% RPD 3.55% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 2

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 112751-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Trainwreck Animal Cookies Live Resin
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000006963
Metrc Source Pkg#: 1A4010300016E07000006856
Test Conditions

Prepsheet ID#: ORP181101a
Scale: XS205-OR1
Temp: 20.2 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 112751

Lot #: TRAC
Batch #: 112751
Batch Weight (g): 1113.4
Harvest/Process Date: 10/11/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 10/29/2018
Test Date: 11/01/2018
Sample #112751
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 3.74 3.52 94.12 3.63 97.06 3.08%
Cannabidiolic Acid (CBDA) N.D. 3.67 3.45 94.01 3.59 97.82 3.98%
Cannabigerol (CBG) N.D. 3.81 3.64 95.54 3.73 97.90 2.44%
Cannabidiol (CBD) N.D. 3.49 3.26 93.41 3.37 96.56 3.32%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 3.77 3.6 95.49 3.73 98.94 3.55%
Cannabinol (CBN) N.D. 3.56 3.41 95.79 3.5 98.31 2.60%
Δ9-Tetrahydrocannabinol (THC) N.D. 3.36 3.16 94.05 3.24 96.43 2.50%
Cannabichromene (CBC) N.D. 3.78 3.62 95.77 3.75 99.21 3.53%
Tetrahydrocannabinolic acid (THCA) N.D. 3.45 3.3 95.65 3.43 99.42 3.86%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 2

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 112751-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Trainwreck Animal Cookies Live Resin
Type: AU Tincture
Metrc Test Pkg#: 1A4010300016E07000006963
Metrc Source Pkg#: 1A4010300016E07000006856
Sample ID#: 112751

Lot #: TRAC
Batch #: 112751
Batch Weight (g): 1113.4
Harvest/Process Date: 10/11/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 10/29/2018
Sample #112751
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 436.39 91.37 57.11 432.48 N.D. N.D. 5.04 104.18 N.D. 8.85 3.72
Increment 2 816.29 29.84 33.83 892.20 N.D. N.D. 2.17 34.02 N.D. 3.32 4.34
Average Value 626.34 60.60 45.47 662.34 N.D. N.D. 3.61 69.10 N.D. 6.09 4.03
Max Value 816.29 91.37 57.11 892.20 N.D. N.D. 5.04 104.18 N.D. 8.85 4.34
Min Value 436.39 29.84 33.83 432.48 N.D. N.D. 2.17 34.02 N.D. 3.32 3.72
Relative Percent Difference (RPD) ±60.65 ±101.53 ±51.20 ±69.41 N.D. N.D. ±79.61 ±101.53 N.D. ±90.88 ±15.38
Average Cannabinoids Per Package 626.34 60.60 45.47 662.34 N.D. N.D. 3.61 69.10 N.D. 6.09 4.03
Average Cannabinoids Per Serving 62.63 6.06 4.55 66.23 N.D. N.D. 0.36 6.91 N.D. 0.61 0.40
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Fail
Control Study   Yes, MJ721
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 2