ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 112504-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Chocolope Shatter
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000006350
Metrc Source Pkg#: 1A4010300016E07000006301
Test Conditions

Prepsheet ID#: ORP181024a
Scale: XS205-OR1
Temp: 20.7 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 112504

Lot #: CHOC
Batch #: 112504
Batch Weight (g): 466.2
Harvest/Process Date: 10/05/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 10/18/2018
Test Date: 10/24/2018
Sample #112504
Sample #112504 Sample #112504
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Avg
Avg. Amount N/D 2.31 mg/g N/D 2.20 mg/g 4.75 mg/g 6.47 mg/g 42.47 mg/g 806.95 mg/g N/D CBD 2.03 mg/g
LOQ 0.1 mg/g 0.1 mg/g 0.1 mg/g 0.1 mg/g 0.1 mg/g 0.1 mg/g 0.1 mg/g 0.1 mg/g 0.1 mg/g THC 750.17 mg/g
Amount per Serving~ N/D 0.23 mg/srv N/D 0.22 mg/srv 0.48 mg/srv 0.65 mg/srv 4.25 mg/srv 80.70 mg/srv N/D Serving Size~ (g): 0.10 g
Uncertainty 3.27% RPD 0.74% RPD 3.17% RPD 1.37% RPD 2.48% RPD 1.04% RPD ±5% RPD 1.46% RPD 2.31% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 8

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 112504-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Chocolope Shatter
Type: AU Tincture
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300016E07000006350
Metrc Source Pkg#: 1A4010300016E07000006301
Test Conditions

Prepsheet ID#: ORP181024a
Scale: XS205-OR1
Temp: 20.7 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 112504

Lot #: CHOC
Batch #: 112504
Batch Weight (g): 466.2
Harvest/Process Date: 10/05/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 10/18/2018
Test Date: 10/24/2018
Sample #112504
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 6.5 5.91 90.92 5.72 88.00 3.27%
Cannabidiolic Acid (CBDA) N.D. 5.84 5.4 92.47 5.36 91.78 0.74%
Cannabigerol (CBG) N.D. 6.44 5.97 92.70 6.12 95.03 2.48%
Cannabidiol (CBD) N.D. 6 5.44 90.67 5.27 87.83 3.17%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 6.4 6 93.75 6.14 95.94 2.31%
Cannabinol (CBN) N.D. 6.02 5.75 95.51 5.81 96.51 1.04%
Δ9-Tetrahydrocannabinol (THC) N.D. 5.76 5.65 98.09 5.61 97.40 0.71%
Cannabichromene (CBC) N.D. 6.16 5.82 94.48 5.9 95.78 1.37%
Tetrahydrocannabinolic acid (THCA) N.D. 5.81 5.43 93.46 5.51 94.84 1.46%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 8

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 112504-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Chocolope Shatter
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000006350
Metrc Source Pkg#: 1A4010300016E07000006301
Test Conditions

Prepsheet ID#: ORPST181107b
Scale: Veritas-OR1
Temp: 22.1 °C
Baro PE: 1018 hPa
Analyst: JER
Technician: JDM
Sample ID#: 112504

Lot #: CHOC
Batch #: 112504
Batch Weight (g): 466.2
Harvest/Process Date: 10/05/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 10/18/2018
Test Date: 11/10/2018
Sample #112504
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.121 Pass/<LOD Abamectin**** 0.500 0.121 Pass/<LOD
Acephate 0.400 0.121 Pass/<LOD Acequinocyl 2.000 0.242 Pass/<LOD
Acetamiprid 0.200 0.121 Pass/<LOD Azoxystrobin 0.200 0.121 Pass/<LOD
Bifenazate 0.200 0.121 Pass/<LOD Bifenthrin 0.200 0.121 Pass/<LOD
Boscalid 0.400 0.121 Pass/<LOD Carbaryl 0.200 0.121 Pass/<LOD
Carbofuran 0.200 0.121 Pass/<LOD Chlorantraniliprole 0.200 0.121 Pass/<LOD
Chlorfenapyr 1.000 0.485 Pass/<LOD Chlorpyrifos 0.200 0.121 Pass/<LOD
Clofentezine 0.200 0.121 Pass/<LOD Cyfluthrin** 1.000 0.485 Pass/<LOD
Cypermethrin*** 1.000 0.485 Pass/<LOD Daminozide 1.000 0.121 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.242 Pass/<LOD Diazinon 0.200 0.121 Pass/<LOD
Dimethoate 0.200 0.121 Pass/<LOD Ethoprophos 0.200 0.121 Pass/<LOD
Etofenprox 0.400 0.121 Pass/<LOD Etoxazole 0.200 0.121 Pass/<LOD
Fenoxycarb 0.200 0.121 Pass/<LOD Fenpyroximate 0.400 0.121 Pass/<LOD
Fipronil 0.400 0.121 Pass/<LOD Flonicamid 1.000 0.121 Pass/<LOD
Fludioxonil 0.400 0.121 Pass/<LOD Hexythiazox 1.000 0.121 Pass/<LOD
Imazalil 0.200 0.121 Pass/<LOD Imidacloprid 0.400 0.121 Pass/<LOD
Kresoxim Methyl 0.400 0.121 Pass/<LOD Malathion 0.200 0.121 Pass/<LOD
Metalaxyl 0.200 0.121 Pass/<LOD Methiocarb 0.200 0.121 Pass/<LOD
Methomyl 0.400 0.121 Pass/<LOD Methyl Parathion 0.200 0.121 Pass/<LOD
MGK-264‡ 0.200 0.121 Pass/<LOD Myclobutanil 0.000 0.121 Pass/<LOD
Naled 0.500 0.121 Pass/<LOD Oxamyl 1.000 0.121 Pass/<LOD
Paclobutrazol 0.400 0.121 Pass/<LOD Permethrins† 0.200 0.121 Pass/<LOD
Phosmet 0.200 0.121 Pass/<LOD Piperonyl Butoxide 2.000 0.121 Pass/<LOD
Prallethrin 0.200 0.121 Pass/<LOD Propiconazole 0.400 0.121 Pass/<LOD
Propoxur 0.200 0.121 Pass/<LOD Pyrethrins* 1.000 0.121 Pass/<LOD
Pyridaben 0.200 0.121 Pass/<LOD Spinosad***** 0.200 0.121 Pass/<LOD
Spiromesifen 0.200 0.121 Pass/<LOD Spirotetramat 0.200 0.121 Pass/<LOD
Spiroxamine‡ 0.400 0.121 Pass/<LOD Tebuconazole 0.400 0.121 Pass/<LOD
Thiacloprid 0.200 0.121 Pass/<LOD Thiamethoxam 0.200 0.121 Pass/<LOD
Trifloxystrobin 0.200 0.121 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 8

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 112504-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Chocolope Shatter
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300016E07000006350
Metrc Source Pkg#: 1A4010300016E07000006301
Test Conditions

Prepsheet ID#: ORPST181107b
Scale: Veritas-OR1
Temp: 22.1 °C
Baro PE: 1018 hPa
Analyst: JER
Technician: JDM
Sample ID#: 112504

Lot #: CHOC
Batch #: 112504
Batch Weight (g): 466.2
Harvest/Process Date: 10/05/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 10/18/2018
Test Date: 11/10/2018
Sample #112504
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.16 1.15 116.00 115.00 0.87
Acequinocyl N.D. 1 0.433 0.449 43.30 44.90 3.63 LR
Acetamiprid N.D. 1 1.12 1.14 112.00 114.00 1.77
Aldicarb N.D. 1 1.06 1.04 106.00 104.00 1.90
Avermectin B1a N.D. 0.97 1.55 1.51 159.79 155.67 2.61 HR
Azoxystrobin N.D. 1 1.33 1.28 133.00 128.00 3.83 HR
Bifenazate N.D. 1 2.3 1.77 230.00 177.00 26.04 HRQ
Bifenthrin N.D. 1 1.07 0.981 107.00 98.10 8.68
Boscalid N.D. 1 1.25 1.16 125.00 116.00 7.47
Carbaryl N.D. 1 1.12 1.09 112.00 109.00 2.71
Carbofuran N.D. 1 1.3 1.29 130.00 129.00 0.77
Chlorantraniliprole N.D. 1 1.67 1.48 167.00 148.00 12.06 HRQ
Chlorfenapyr N.D. 1 0.988 1.06 98.80 106.00 7.03
Chlorpyriphos N.D. 1 1.06 1.02 106.00 102.00 3.85
Clofentezine N.D. 1 1.09 1.03 109.00 103.00 5.66
Cyfluthrin N.D. 1 1.34 1.24 134.00 124.00 7.75 HR
Cypermethrin N.D. 1 1.81 1.71 181.00 171.00 5.68 HR
Daminoside N.D. 1 0.771 0.758 77.10 75.80 1.70
Diazanon N.D. 1 4.91 4.98 491.00 498.00 1.42 HR
Dichlorvos N.D. 1 1.22 1.16 122.00 116.00 5.04
Dimethoate N.D. 1 1.24 1.09 124.00 109.00 12.88
Ethoprophos N.D. 1 1.13 1.06 113.00 106.00 6.39
Etofenprox N.D. 1 1.06 1.03 106.00 103.00 2.87
Etoxazole N.D. 1 0.835 0.778 83.50 77.80 7.07
Fenoxycarb N.D. 1 1.5 1.5 150.00 150.00 0.00 HR
Fenpyroximate N.D. 1 1.34 1.24 134.00 124.00 7.75 HR
Fipronil N.D. 1 1.03 1 103.00 100.00 2.96
Flonicamid N.D. 1 1.29 1.29 129.00 129.00 0.00
Fludioxonil N.D. 1 0.962 1.02 96.20 102.00 5.85
Hexythiazox N.D. 1 0.994 0.961 99.40 96.10 3.38
Imazalil N.D. 1 1.49 1.37 149.00 137.00 8.39 HR
Imidacloprid N.D. 1 1.28 1.27 128.00 127.00 0.78
Kresoxim-methyl N.D. 1 1.64 1.58 164.00 158.00 3.73 HR
Malathion N.D. 1 1.53 1.41 153.00 141.00 8.16 HR
Metalaxyl N.D. 1 1.3 1.26 130.00 126.00 3.13
Methiocarb N.D. 1 1.24 1.28 124.00 128.00 3.17
Methomyl N.D. 1 1.31 1.29 131.00 129.00 1.54 HR
MGK-264 N.D. 1 1.08 1.07 108.00 107.00 0.93
Myclobutanil N.D. 1 1.53 1.52 153.00 152.00 0.66 HR
Naled (dibrom) N.D. 1 0.734 0.747 73.40 74.70 1.76
Oxamyl N.D. 1 1.1 1.1 110.00 110.00 0.00
Paclobutrazol N.D. 1 1.64 1.65 164.00 165.00 0.61 HR
Parathion-methyl N.D. 1 0.903 1.07 90.30 107.00 16.93
Permethrins N.D. 1 0.99 0.982 99.00 98.20 0.81
Phosmet N.D. 1 1.43 1.36 143.00 136.00 5.02 HR
Piperonyl butoxide N.D. 1 1.34 1.22 134.00 122.00 9.38 HR
Prallethrin N.D. 1 1.39 1.38 139.00 138.00 0.72 HR
Propiconazole N.D. 1 1.28 1.29 128.00 129.00 0.78
Propoxur N.D. 1 1.19 1.15 119.00 115.00 3.42
Pyrethrin N.D. 0.65 0.83 0.828 127.69 127.38 0.24
Pyridaben N.D. 1 1.07 1.04 107.00 104.00 2.84
SpinosynA N.D. 0.84 1.15 1.08 136.90 128.57 6.28 HR
SpinosynD N.D. 0.16 0.384 0.359 240.00 224.38 6.73 HR
Spiromesifen N.D. 1 0.18 0.187 18.00 18.70 3.81 LR
Spirotetramat N.D. 1 1.1 1 110.00 100.00 9.52
Spiroxamine N.D. 1 1.37 1.4 137.00 140.00 2.17 HR
Tebuconazole N.D. 1 1.52 1.52 152.00 152.00 0.00 HR
Thiacloprid N.D. 1 1.33 1.26 133.00 126.00 5.41 HR
Thiamethoxam N.D. 1 1.48 1.44 148.00 144.00 2.74 HR
Trifloxystrobin N.D. 1 1.19 1.17 119.00 117.00 1.69

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 8

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 112504-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Chocolope Shatter
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000006350
Metrc Source Pkg#: 1A4010300016E07000006301
Test Conditions

Prepsheet ID#: ORHS181023a
Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1007 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 112504

Lot #: CHOC
Batch #: 112504
Batch Weight (g): 466.2
Harvest/Process Date: 10/05/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 10/18/2018
Test Date: 10/23/2018
Sample #112504
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/178
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/271 Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 150 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 8

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 112504-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Chocolope Shatter
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000006350
Metrc Source Pkg#: 1A4010300016E07000006301
Test Conditions

Prepsheet ID#: ORHS181023a
Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1007 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 112504

Lot #: CHOC
Batch #: 112504
Batch Weight (g): 466.2
Harvest/Process Date: 10/05/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 10/18/2018
Test Date: 10/23/2018
Sample #112504
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 46 52 18.40 20.80 12.24 LR
Isobutane N.D. 250 90 88 36.00 35.20 2.25 LR
Methanol N.D. 250 240 226 96.00 90.40 6.01
n-Butane N.D. 250 105 106 42.00 42.40 0.95 LR
2,2-Dimethylpropane N.D. 250 115 117 46.00 46.80 1.72 LR
Ethanol N.D. 250 205 221 82.00 88.40 7.51
Isopentane N.D. 250 141 141 56.40 56.40 0.00 LR
Acetonitrile N.D. 250 205 207 82.00 82.80 0.97
Diethyl ether N.D. 250 189 196 75.60 78.40 3.64
2-propanone N.D. 250 219 212 87.60 84.80 3.25
2-propanol N.D. 250 225 248 90.00 99.20 9.73
n-Pentane N.D. 250 124 136 49.60 54.40 9.23 LR
2,2-Dimethylbutane N.D. 250 166 167 66.40 66.80 0.60 LR
2,3-Dimethylbutane N.D. 250 168 174 67.20 69.60 3.51 LR
Methylene chloride N.D. 250 207 211 82.80 84.40 1.91
2-Methylpentane N.D. 250 170 175 68.00 70.00 2.90 LR
3-Methylpentane N.D. 250 180 183 72.00 73.20 1.65
2-Butanol N.D. 250 209 219 83.60 87.60 4.67
n-Hexane N.D. 250 184 195 73.60 78.00 5.80
Ethyl acetate N.D. 250 205 220 82.00 88.00 7.06
Tetrahydrofuran N.D. 250 203 207 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 205 211 0.00 0.00 0.00
Benzene N.D. 250 220 222 88.00 88.80 0.90
Chloroform N.D. 0 0 nan nan
Cyclohexane N.D. 250 197 197 78.80 78.80 0.00
Ethylene glycol N.D. 250 188 206 75.20 82.40 9.14
Heptane N.D. 250 193 198 77.20 79.20 2.56
2-Ethoxyethanol N.D. 250 156 184 62.40 73.60 16.47 LR
1,4-Dioxane N.D. 250 201 211 80.40 84.40 4.85
Pyridine N.D. 250 0 0 0.00 0.00 0.00
Toluene N.D. 250 218 222 87.20 88.80 1.82
Chlorobenzene N.D. 250 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 218 220 87.20 88.00 0.91
m-Xylene/p-Xylene N.D. 500 441 437 88.20 87.40 0.91
o-Xylene N.D. 250 212 211 84.80 84.40 0.47
Cumene N.D. 250 217 197 86.80 78.80 9.66
Ethylene oxide N.D. 250 169 212 67.60 84.80 22.57 Q

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 8

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 112504-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Chocolope Shatter
Type: AU Tincture
Metrc Test Pkg#: 1A4010300016E07000006350
Metrc Source Pkg#: 1A4010300016E07000006301
Sample ID#: 112504

Lot #: CHOC
Batch #: 112504
Batch Weight (g): 466.2
Harvest/Process Date: 10/05/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 10/18/2018
Sample #112504
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 751.57 1.95 42.69 808.30 N.D. N.D. 2.16 2.22 N.D. 4.76 6.45
Increment 2 748.75 2.10 42.25 805.59 N.D. N.D. 2.24 2.40 N.D. 4.73 6.49
Average Value 750.16 2.03 42.47 806.95 N.D. N.D. 2.20 2.31 N.D. 4.75 6.47
Max Value 751.57 2.10 42.69 808.30 N.D. N.D. 2.24 2.40 N.D. 4.76 6.49
Min Value 748.75 1.95 42.25 805.59 N.D. N.D. 2.16 2.22 N.D. 4.73 6.45
Relative Percent Difference (RPD) ±0.38 ±7.79 ±1.04 ±0.34 N.D. N.D. ±3.64 ±7.79 N.D. ±0.63 ±0.62
Average Cannabinoids Per Package 750.16 2.03 42.47 806.95 N.D. N.D. 2.20 2.31 N.D. 4.75 6.47
Average Cannabinoids Per Serving 75.02 0.20 4.25 80.69 N.D. N.D. 0.22 0.23 N.D. 0.47 0.65
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ721
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 8
IRON Laboratories

Oregon Compliant Terpene Report by
Mass Spectrometer
Test Certificate #: 112504-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Chocolope Shatter
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000006350
Metrc Source Pkg#: 1A4010300016E07000006301
Test Conditions

Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1007 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 112504

Lot #: CHOC
Batch #: 112504
Batch Weight (g): 466.2
Harvest/Process Date: 10/05/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 10/18/2018
Test Date: 10/25/2018
Sample #112504

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.150 %

β-Ocimene:

0.100 %

Camphene:

0.020 %

Eucalyptol (1,8-Cineol):

0.030 %

Sabinene:

 N/D

γ-Terpinene:

0.020 %

Myrcene:

0.260 %

α-Terpinolene:

0.070 %

β-Pinene:

0.130 %

Linalool:

0.090 %

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

0.030 %

Fenchol:

0.080 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.130 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.720 %

α-Humulene:

0.450 %

Nerolidol 1:

0.040 %

Nerolidol 2:

0.050 %

Guaiol:

0.460 %

Caryophyllene Oxide:

0.090 %

α-Bisabolol:

0.040 %

Other Terpenes

Total: 2.960%
a-Phellandrene = 0.03 % a-Terpineol = 0.07 % Valencene = 0.09 %

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 8
IRON Laboratories

Oregon Compliant Terpene Report by
Mass Spectrometer
Test Certificate #: 112504-001
Client Name, Sample Details

Mana Extracts
Portland, OR 97217
Sample: Chocolope Shatter
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300016E07000006350
Metrc Source Pkg#: 1A4010300016E07000006301
Test Conditions

Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1007 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 112504

Lot #: CHOC
Batch #: 112504
Batch Weight (g): 466.2
Harvest/Process Date: 10/05/2018
Serving Size (g): 0.1
Package Weight (g):1
Date Received: 10/18/2018
Test Date: 10/25/2018
Sample #112504

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.160 %

β-Ocimene:

0.090 %

Camphene:

0.020 %

Eucalyptol (1,8-Cineol):

0.030 %

Sabinene:

 N/D

γ-Terpinene:

0.020 %

Myrcene:

0.270 %

α-Terpinolene:

0.080 %

β-Pinene:

0.130 %

Linalool:

0.090 %

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

0.030 %

Fenchol:

0.080 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.130 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.720 %

α-Humulene:

0.470 %

Nerolidol 1:

0.040 %

Nerolidol 2:

0.050 %

Guaiol:

0.510 %

Caryophyllene Oxide:

0.070 %

α-Bisabolol:

0.050 %

Other Terpenes

Total: 3.040%
a-Phellandrene = 0.04 % a-Terpineol = 0.07 % Valencene = 0.13 %

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 8