ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 112263-001
Client Name, Sample Details

Firehorse Trading
Springfield , OR 97478
Sample: New Year's Eve Dream
License: 020-10059262 C66
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A401030000DAC2000000060
Metrc Source Pkg#: 1A401030000DAC2000000059
***Water Activity: 0.461
***Moisture: 11.31%
Test Conditions

Prepsheet ID#: ORP181011a
Scale: XS205-OR1
Temp: 21.5 °C
Baro Pressure: 1001 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 112263

Lot #: HRVNDGH1071918
Batch #: 112263
Batch Weight (g): 6803
Harvest/Process Date: 07/19/2018
Package Weight (g):34.2
Date Received: 10/10/2018
Test Date: 10/11/2018
Sample #112263
Sample #112263 Sample #112263
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV Total THC Total CBD
Amount N/D 0.11% N/D 0.07% 0.15% 0.12% 1.76% 22.08% N/D 21.12% 0.10%
LOQ 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05%
Uncertainty 2.89% RPD 3.09% RPD 3.30% RPD 4.64% RPD 2.99% RPD 2.99% RPD ±5% RPD 2.47% RPD 2.83% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 112263-001
Client Name, Sample Details

Firehorse Trading
Springfield , OR 97478
Sample: New Year's Eve Dream
License: 020-10059262 C66
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A401030000DAC2000000060
Metrc Source Pkg#: 1A401030000DAC2000000059
***Water Activity: 0.461
***Moisture: 11.31%
Test Conditions

Prepsheet ID#: ORP181011a
Scale: XS205-OR1
Temp: 21.5 °C
Baro Pressure: 1001 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 112263

Lot #: HRVNDGH1071918
Batch #: 112263
Batch Weight (g): 6803
Harvest/Process Date: 07/19/2018
Package Weight (g):34.2
Date Received: 10/10/2018
Test Date: 10/11/2018
Sample #112263
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 11.07 11.92 107.68 12.27 110.84 2.89%
Cannabidiolic Acid (CBDA) N.D. 5.17 5.74 111.03 5.92 114.51 3.09%
Cannabigerol (CBG) N.D. 5.6 5.94 106.07 6.12 109.29 2.99%
Cannabidiol (CBD) N.D. 5.32 5.67 106.58 5.86 110.15 3.30%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.19 5.57 107.32 5.73 110.40 2.83%
Cannabinol (CBN) N.D. 5.32 5.61 105.45 5.78 108.65 2.99%
Δ9-Tetrahydrocannabinol (THC) N.D. 5.12 5.33 104.10 5.49 107.23 2.96%
Cannabichromene (CBC) N.D. 5.39 5.69 105.57 5.96 110.58 4.64%
Tetrahydrocannabinolic acid (THCA) N.D. 4.97 5.6 112.68 5.74 115.49 2.47%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 112263-001
Client Name, Sample Details

Firehorse Trading
Springfield , OR 97478
Sample: New Year's Eve Dream
License: 020-10059262 C66
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030000DAC2000000060
Metrc Source Pkg#: 1A401030000DAC2000000059
Test Conditions

Prepsheet ID#: ORPS181012a
Scale: Veritas-OR1
Temp: 20.4 °C
Baro PE: 1001 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 112263

Lot #: HRVNDGH1071918
Batch #: 112263
Batch Weight (g): 6803
Harvest/Process Date: 07/19/2018
Package Weight (g):34.2
Date Received: 10/10/2018
Test Date: 10/13/2018
Sample #112263
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.121 Pass/<LOD Abamectin**** 0.500 0.121 Pass/<LOD
Acephate 0.400 0.121 Pass/<LOD Acequinocyl 2.000 0.242 Pass/<LOD
Acetamiprid 0.200 0.121 Pass/<LOD Azoxystrobin 0.200 0.121 Pass/<LOD
Bifenazate 0.200 0.121 Pass/<LOD Bifenthrin 0.200 0.121 Pass/<LOD
Boscalid 0.400 0.121 Pass/<LOD Carbaryl 0.200 0.121 Pass/<LOD
Carbofuran 0.200 0.121 Pass/<LOD Chlorantraniliprole 0.200 0.121 Pass/<LOD
Chlorfenapyr 1.000 0.484 Pass/<LOD Chlorpyrifos 0.200 0.121 Pass/<LOD
Clofentezine 0.200 0.121 Pass/<LOD Cyfluthrin** 1.000 0.484 Pass/<LOD
Cypermethrin*** 1.000 0.484 Pass/<LOD Daminozide 1.000 0.121 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.242 Pass/<LOD Diazinon 0.200 0.121 Pass/<LOD
Dimethoate 0.200 0.121 Pass/<LOD Ethoprophos 0.200 0.121 Pass/<LOD
Etofenprox 0.400 0.121 Pass/<LOD Etoxazole 0.200 0.121 Pass/<LOD
Fenoxycarb 0.200 0.121 Pass/<LOD Fenpyroximate 0.400 0.121 Pass/<LOD
Fipronil 0.400 0.121 Pass/<LOD Flonicamid 1.000 0.121 Pass/<LOD
Fludioxonil 0.400 0.121 Pass/<LOD Hexythiazox 1.000 0.121 Pass/<LOD
Imazalil 0.200 0.121 Pass/<LOD Imidacloprid 0.400 0.121 Pass/<LOD
Kresoxim Methyl 0.400 0.121 Pass/<LOD Malathion 0.200 0.121 Pass/<LOD
Metalaxyl 0.200 0.121 Pass/<LOD Methiocarb 0.200 0.121 Pass/<LOD
Methomyl 0.400 0.121 Pass/<LOD Methyl Parathion 0.200 0.121 Pass/<LOD
MGK-264‡ 0.200 0.121 Pass/<LOD Myclobutanil 0.000 0.121 Pass/<LOD
Naled 0.500 0.121 Pass/<LOD Oxamyl 1.000 0.121 Pass/<LOD
Paclobutrazol 0.400 0.121 Pass/<LOD Permethrins† 0.200 0.121 Pass/<LOD
Phosmet 0.200 0.121 Pass/<LOD Piperonyl Butoxide 2.000 0.121 Pass/<LOD
Prallethrin 0.200 0.121 Pass/<LOD Propiconazole 0.400 0.121 Pass/<LOD
Propoxur 0.200 0.121 Pass/<LOD Pyrethrins* 1.000 0.121 Pass/<LOD
Pyridaben 0.200 0.121 Pass/<LOD Spinosad***** 0.200 0.121 Pass/<LOD
Spiromesifen 0.200 0.121 Pass/<LOD Spirotetramat 0.200 0.121 Pass/<LOD
Spiroxamine‡ 0.400 0.121 Pass/<LOD Tebuconazole 0.400 0.121 Pass/<LOD
Thiacloprid 0.200 0.121 Pass/<LOD Thiamethoxam 0.200 0.121 Pass/<LOD
Trifloxystrobin 0.200 0.121 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 112263-001
Client Name, Sample Details

Firehorse Trading
Springfield , OR 97478
Sample: New Year's Eve Dream
License: 020-10059262 C66
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030000DAC2000000060
Metrc Source Pkg#: 1A401030000DAC2000000059
Test Conditions

Prepsheet ID#: ORPS181012a
Scale: Veritas-OR1
Temp: 20.4 °C
Baro PE: 1001 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 112263

Lot #: HRVNDGH1071918
Batch #: 112263
Batch Weight (g): 6803
Harvest/Process Date: 07/19/2018
Package Weight (g):34.2
Date Received: 10/10/2018
Test Date: 10/13/2018
Sample #112263
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.867 0.844 86.70 84.40 2.69
Acequinocyl N.D. 1 0.592 0.63 59.20 63.00 6.22 LR
Acetamiprid N.D. 1 0.998 0.968 99.80 96.80 3.05
Aldicarb N.D. 1 0.835 0.845 83.50 84.50 1.19
Avermectin B1a N.D. 0.97 1.08 1.17 111.34 120.62 8.00
Azoxystrobin N.D. 1 0.981 1.01 98.10 101.00 2.91
Bifenazate N.D. 1 0.828 0.826 82.80 82.60 0.24
Bifenthrin N.D. 1 0.92 0.981 92.00 98.10 6.42
Boscalid N.D. 1 0.968 0.988 96.80 98.80 2.04
Carbaryl N.D. 1 1.01 0.982 101.00 98.20 2.81
Carbofuran N.D. 1 0.995 0.984 99.50 98.40 1.11
Chlorantraniliprole N.D. 1 0.892 0.902 89.20 90.20 1.11
Chlorfenapyr N.D. 1 1.11 0.989 111.00 98.90 11.53
Chlorpyriphos N.D. 1 1.03 1.02 103.00 102.00 0.98
Clofentezine N.D. 1 0.88 0.907 88.00 90.70 3.02
Cyfluthrin N.D. 1 0.593 0.619 59.30 61.90 4.29 LR
Cypermethrin N.D. 1 0.885 0.887 88.50 88.70 0.23
Daminoside N.D. 1 0.444 0.42 44.40 42.00 5.56 LR
Diazanon N.D. 1 2.24 2.28 224.00 228.00 1.77 HR
Dichlorvos N.D. 1 0.835 0.883 83.50 88.30 5.59
Dimethoate N.D. 1 0.89 0.917 89.00 91.70 2.99
Ethoprophos N.D. 1 0.821 0.837 82.10 83.70 1.93
Etofenprox N.D. 1 1.09 1.13 109.00 113.00 3.60
Etoxazole N.D. 1 1.17 1.17 117.00 117.00 0.00
Fenoxycarb N.D. 1 0.876 0.912 87.60 91.20 4.03
Fenpyroximate N.D. 1 1.13 1.19 113.00 119.00 5.17
Fipronil N.D. 1 1.08 1.06 108.00 106.00 1.87
Flonicamid N.D. 1 0.85 0.898 85.00 89.80 5.49
Fludioxonil N.D. 1 0.95 0.952 95.00 95.20 0.21
Hexythiazox N.D. 1 0.949 0.98 94.90 98.00 3.21
Imazalil N.D. 1 0.817 0.839 81.70 83.90 2.66
Imidacloprid N.D. 1 0.83 0.853 83.00 85.30 2.73
Kresoxim-methyl N.D. 1 0.971 1.02 97.10 102.00 4.92
Malathion N.D. 1 0.831 0.824 83.10 82.40 0.85
Metalaxyl N.D. 1 0.849 0.846 84.90 84.60 0.35
Methiocarb N.D. 1 0.948 0.983 94.80 98.30 3.63
Methomyl N.D. 1 0.787 0.797 78.70 79.70 1.26
MGK-264 N.D. 1 0.815 0.871 81.50 87.10 6.64
Myclobutanil N.D. 1 0.831 0.863 83.10 86.30 3.78
Naled (dibrom) N.D. 1 0.612 0.62 61.20 62.00 1.30 LR
Oxamyl N.D. 1 0.902 0.909 90.20 90.90 0.77
Paclobutrazol N.D. 1 0.845 0.873 84.50 87.30 3.26
Parathion-methyl N.D. 1 0.988 1.02 98.80 102.00 3.19
Permethrins N.D. 1 0.693 0.769 69.30 76.90 10.40 LR
Phosmet N.D. 1 0.902 0.897 90.20 89.70 0.56
Piperonyl butoxide N.D. 1 1.19 1.18 119.00 118.00 0.84
Prallethrin N.D. 1 0.916 0.895 91.60 89.50 2.32
Propiconazole N.D. 1 0.984 1.01 98.40 101.00 2.61
Propoxur N.D. 1 0.979 0.984 97.90 98.40 0.51
Pyrethrin N.D. 0.65 0.604 0.613 92.92 94.31 1.48
Pyridaben N.D. 1 1.08 1.13 108.00 113.00 4.52
SpinosynA N.D. 0.84 0.381 0.471 45.36 56.07 21.13 LRQ
SpinosynD N.D. 0.16 0.0737 0.113 46.06 70.63 42.10 LRQ
Spiromesifen N.D. 1 0.29 0.288 29.00 28.80 0.69 LR
Spirotetramat N.D. 1 0.83 0.833 83.00 83.30 0.36
Spiroxamine N.D. 1 0.898 0.905 89.80 90.50 0.78
Tebuconazole N.D. 1 0.888 0.905 88.80 90.50 1.90
Thiacloprid N.D. 1 0.866 0.882 86.60 88.20 1.83
Thiamethoxam N.D. 1 0.856 0.842 85.60 84.20 1.65
Trifloxystrobin N.D. 1 1.07 1.07 107.00 107.00 0.00

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 112263-001
Client Name, Sample Details

Firehorse Trading
Springfield , OR 97478
Sample: New Year's Eve Dream
License: 020-10059262 C66
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030000DAC2000000060
Metrc Source Pkg#: 1A401030000DAC2000000059
Test Conditions

Scale: XS205-OR1
Temp: 19.4 °C
Baro Pressure: 1008 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 112263

Lot #: HRVNDGH1071918
Batch #: 112263
Batch Weight (g): 6803
Harvest/Process Date: 07/19/2018
Package Weight (g):34.2
Date Received: 10/10/2018
Test Date: 10/13/2018
Sample #112263

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.130 %

β-Ocimene:

0.030 %

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

0.320 %

α-Terpinolene:

 N/D

β-Pinene:

0.110 %

Linalool:

0.020 %

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

0.020 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.080 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.310 %

α-Humulene:

0.160 %

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

0.030 %

Other Terpenes

Total: 1.210%
a-Phellandrene = 0.02 % a-Terpineol = 0.02 % Valencene = 0.07 %

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4