ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 111616-001
Client Name, Sample Details

Revel Farms
Eugene, OR 97425
Sample: Headband
License: 10069798E0F
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A401030000F0A1000000348
Metrc Source Pkg#: 1A401030000F0A1000000346
***Water Activity: 0.495
***Moisture: 12.39%
Test Conditions

Prepsheet ID#: ORP180921a
Scale: XS205-OR1
Temp: 21.1 °C
Baro Pressure: 46.8 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 111616

Lot #: Headband 82118
Batch #: 111616
Batch Weight (g): 4063
Harvest/Process Date: 08/21/2018
Package Weight (g):20.4
Date Received: 09/14/2018
Test Date: 09/21/2018
Sample #111616
Sample #111616 Sample #111616
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV Total THC Total CBD
Amount N/D 0.12% N/D 0.09% 0.22% 0.06% 0.88% 18.77% N/D 17.34% 0.11%
LOQ 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05%
Uncertainty 4.02% RPD 3.29% RPD 3.66% RPD 3.33% RPD 3.53% RPD 3.34% RPD ±5% RPD 1.79% RPD 2.63% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 111616-001
Client Name, Sample Details

Revel Farms
Eugene, OR 97425
Sample: Headband
License: 10069798E0F
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A401030000F0A1000000348
Metrc Source Pkg#: 1A401030000F0A1000000346
***Water Activity: 0.495
***Moisture: 12.39%
Test Conditions

Prepsheet ID#: ORP180921a
Scale: XS205-OR1
Temp: 21.1 °C
Baro Pressure: 46.8 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 111616

Lot #: Headband 82118
Batch #: 111616
Batch Weight (g): 4063
Harvest/Process Date: 08/21/2018
Package Weight (g):20.4
Date Received: 09/14/2018
Test Date: 09/21/2018
Sample #111616
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 6.35 6.09 95.91 6.34 99.84 4.02%
Cannabidiolic Acid (CBDA) N.D. 5.61 5.68 101.25 5.87 104.63 3.29%
Cannabigerol (CBG) N.D. 6.1 5.85 95.90 6.06 99.34 3.53%
Cannabidiol (CBD) N.D. 5.87 5.63 95.91 5.84 99.49 3.66%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 6.17 6.01 97.41 6.17 100.00 2.63%
Cannabinol (CBN) N.D. 5.88 5.59 95.07 5.78 98.30 3.34%
Δ9-Tetrahydrocannabinol (THC) N.D. 5.54 5.29 95.49 5.48 98.92 3.53%
Cannabichromene (CBC) N.D. 6.04 5.61 92.88 5.8 96.03 3.33%
Tetrahydrocannabinolic acid (THCA) N.D. 5.61 5.54 98.75 5.64 100.53 1.79%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 111616-001
Client Name, Sample Details

Revel Farms
Eugene, OR 97425
Sample: Headband
License: 10069798E0F
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030000F0A1000000348
Metrc Source Pkg#: 1A401030000F0A1000000346
Test Conditions

Prepsheet ID#: ORPS180919a
Scale: Veritas-OR1
Temp: 1001 °C
Baro PE: 21.6 hPa
Analyst: JER
Technician: HRM
Sample ID#: 111616

Lot #: Headband 82118
Batch #: 111616
Batch Weight (g): 4063
Harvest/Process Date: 08/21/2018
Package Weight (g):20.4
Date Received: 09/14/2018
Test Date: 09/21/2018
Sample #111616
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.116 Pass/<LOD Abamectin**** 0.500 0.116 Pass/<LOD
Acephate 0.400 0.116 Pass/<LOD Acequinocyl 2.000 0.231 Pass/<LOD
Acetamiprid 0.200 0.116 Pass/<LOD Azoxystrobin 0.200 0.116 Pass/<LOD
Bifenazate 0.200 0.116 Pass/<LOD Bifenthrin 0.200 0.116 Pass/<LOD
Boscalid 0.400 0.116 Pass/<LOD Carbaryl 0.200 0.116 Pass/<LOD
Carbofuran 0.200 0.116 Pass/<LOD Chlorantraniliprole 0.200 0.116 Pass/<LOD
Chlorfenapyr 1.000 0.463 Pass/<LOD Chlorpyrifos 0.200 0.116 Pass/<LOD
Clofentezine 0.200 0.116 Pass/<LOD Cyfluthrin** 1.000 0.463 Pass/<LOD
Cypermethrin*** 1.000 0.463 Pass/<LOD Daminozide 1.000 0.116 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.231 Pass/<LOD Diazinon 0.200 0.116 Pass/<LOD
Dimethoate 0.200 0.116 Pass/<LOD Ethoprophos 0.200 0.116 Pass/<LOD
Etofenprox 0.400 0.116 Pass/<LOD Etoxazole 0.200 0.116 Pass/<LOD
Fenoxycarb 0.200 0.116 Pass/<LOD Fenpyroximate 0.400 0.116 Pass/<LOD
Fipronil 0.400 0.116 Pass/<LOD Flonicamid 1.000 0.116 Pass/<LOD
Fludioxonil 0.400 0.116 Pass/<LOD Hexythiazox 1.000 0.116 Pass/<LOD
Imazalil 0.200 0.116 Pass/<LOD Imidacloprid 0.400 0.116 Pass/<LOD
Kresoxim Methyl 0.400 0.116 Pass/<LOD Malathion 0.200 0.116 Pass/<LOD
Metalaxyl 0.200 0.116 Pass/<LOD Methiocarb 0.200 0.116 Pass/<LOD
Methomyl 0.400 0.116 Pass/<LOD Methyl Parathion 0.200 0.116 Pass/<LOD
MGK-264‡ 0.200 0.116 Pass/<LOD Myclobutanil 0.000 0.116 Pass/<LOD
Naled 0.500 0.116 Pass/<LOD Oxamyl 1.000 0.116 Pass/<LOD
Paclobutrazol 0.400 0.116 Pass/<LOD Permethrins† 0.200 0.116 Pass/<LOD
Phosmet 0.200 0.116 Pass/<LOD Piperonyl Butoxide 2.000 0.116 Pass/<LOD
Prallethrin 0.200 0.116 Pass/<LOD Propiconazole 0.400 0.116 Pass/<LOD
Propoxur 0.200 0.116 Pass/<LOD Pyrethrins* 1.000 0.116 Pass/<LOD
Pyridaben 0.200 0.116 Pass/<LOD Spinosad***** 0.200 0.116 Pass/<LOD
Spiromesifen 0.200 0.116 Pass/<LOD Spirotetramat 0.200 0.116 Pass/<LOD
Spiroxamine‡ 0.400 0.116 Pass/<LOD Tebuconazole 0.400 0.116 Pass/<LOD
Thiacloprid 0.200 0.116 Pass/<LOD Thiamethoxam 0.200 0.116 Pass/<LOD
Trifloxystrobin 0.200 0.116 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 111616-001
Client Name, Sample Details

Revel Farms
Eugene, OR 97425
Sample: Headband
License: 10069798E0F
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030000F0A1000000348
Metrc Source Pkg#: 1A401030000F0A1000000346
Test Conditions

Prepsheet ID#: ORPS180919a
Scale: Veritas-OR1
Temp: 1001 °C
Baro PE: 21.6 hPa
Analyst: JER
Technician: HRM
Sample ID#: 111616

Lot #: Headband 82118
Batch #: 111616
Batch Weight (g): 4063
Harvest/Process Date: 08/21/2018
Package Weight (g):20.4
Date Received: 09/14/2018
Test Date: 09/21/2018
Sample #111616
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. .5 0.303 0.276 60.60 55.20 9.33 LR
Acequinocyl N.D. .5 0.279 0.263 55.80 52.60 5.90 LR
Acetamiprid N.D. .5 0.354 0.339 70.80 67.80 4.33 LR
Aldicarb N.D. .5 0.319 0.305 63.80 61.00 4.49 LR
Avermectin B1a N.D. .48 0.403 0.432 83.96 90.00 6.95
Azoxystrobin N.D. .5 0.384 0.366 76.80 73.20 4.80
Bifenazate N.D. .5 0.303 0.292 60.60 58.40 3.70 LR
Bifenthrin N.D. .5 0.37 0.37 74.00 74.00 0.00
Boscalid N.D. .5 0.391 0.367 78.20 73.40 6.33
Carbaryl N.D. .5 0.381 0.329 76.20 65.80 14.65
Carbofuran N.D. .5 0.392 0.371 78.40 74.20 5.50
Chlorantraniliprole N.D. .5 0.302 0.293 60.40 58.60 3.03 LR
Chlorfenapyr N.D. .5 0.322 0.295 64.40 59.00 8.75 LR
Chlorpyriphos N.D. .5 0.378 0.366 75.60 73.20 3.23
Clofentezine N.D. .5 0.27 0.227 54.00 45.40 17.30 LR
Cyfluthrin N.D. .5 0.388 0.415 77.60 83.00 6.72
Cypermethrin N.D. .5 0.384 0.38 76.80 76.00 1.05
Daminoside N.D. .5 0.18 0.195 36.00 39.00 8.00 LR
Diazanon N.D. .5 0.76 0.749 152.00 149.80 1.46 HR
Dichlorvos N.D. .5 0.289 0.26 57.80 52.00 10.56 LR
Dimethoate N.D. .5 0.329 0.312 65.80 62.40 5.30 LR
Ethoprophos N.D. .5 0.302 0.277 60.40 55.40 8.64 LR
Etofenprox N.D. .5 0.424 0.423 84.80 84.60 0.24
Etoxazole N.D. .5 0.394 0.43 78.80 86.00 8.74
Fenoxycarb N.D. .5 0.297 0.291 59.40 58.20 2.04 LR
Fenpyroximate N.D. .5 0.45 0.437 90.00 87.40 2.93
Fipronil N.D. .5 0.403 0.413 80.60 82.60 2.45
Flonicamid N.D. .5 0.317 0.301 63.40 60.20 5.18 LR
Fludioxonil N.D. .5 0.402 0.38 80.40 76.00 5.63
Hexythiazox N.D. .5 0.375 0.355 75.00 71.00 5.48
Imazalil N.D. .5 0.284 0.284 56.80 56.80 0.00 LR
Imidacloprid N.D. .5 0.296 0.322 59.20 64.40 8.41 LR
Kresoxim-methyl N.D. .5 0.289 0.26 57.80 52.00 10.56 LR
Malathion N.D. .5 0.347 0.348 69.40 69.60 0.29 LR
Metalaxyl N.D. .5 0.285 0.318 57.00 63.60 10.95 LR
Methiocarb N.D. .5 0.363 0.343 72.60 68.60 5.67 LR
Methomyl N.D. .5 0.199 0.214 39.80 42.80 7.26 LR
MGK-264 N.D. .5 0.312 0.29 62.40 58.00 7.31 LR
Myclobutanil N.D. .5 0.225 0.232 45.00 46.40 3.06 LR
Naled (dibrom) N.D. .5 0.267 0.24 53.40 48.00 10.65 LR
Oxamyl N.D. .5 0.29 0.288 58.00 57.60 0.69 LR
Paclobutrazol N.D. .5 0.294 0.279 58.80 55.80 5.24 LR
Parathion-methyl N.D. .5 0.371 0.38 74.20 76.00 2.40
Permethrins N.D. .5 0.394 0.366 78.80 73.20 7.37
Phosmet N.D. .5 0.319 0.304 63.80 60.80 4.82 LR
Piperonyl butoxide N.D. .5 0.497 0.448 99.40 89.60 10.37
Prallethrin N.D. .5 0.313 0.314 62.60 62.80 0.32 LR
Propiconazole N.D. .5 0.352 0.358 70.40 71.60 1.69
Propoxur N.D. .5 0.368 0.355 73.60 71.00 3.60
Pyrethrin N.D. .325 0.195 0.192 60.00 59.08 1.55 LR
Pyridaben N.D. .5 0.423 0.418 84.60 83.60 1.19
SpinosynA N.D. .42 0 0 0.00 0.00 LR
SpinosynD N.D. .08 0 0 0.00 0.00 LR
Spiromesifen N.D. .5 0.155 0.168 31.00 33.60 8.05 LR
Spirotetramat N.D. .5 0.359 0.339 71.80 67.80 5.73 LR
Spiroxamine N.D. .5 0.318 0.322 63.60 64.40 1.25 LR
Tebuconazole N.D. .5 0.33 0.303 66.00 60.60 8.53 LR
Thiacloprid N.D. .5 0.233 0.222 46.60 44.40 4.84 LR
Thiamethoxam N.D. .5 0.267 0.255 53.40 51.00 4.60 LR
Trifloxystrobin N.D. .5 0.429 0.413 85.80 82.60 3.80

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 111616-001
Client Name, Sample Details

Revel Farms
Eugene, OR 97425
Sample: Headband
License: 10069798E0F
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030000F0A1000000348
Metrc Source Pkg#: 1A401030000F0A1000000346
Test Conditions

Scale: XS205-OR1
Temp: 20.2 °C
Baro Pressure: 1009 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 111616

Lot #: Headband 82118
Batch #: 111616
Batch Weight (g): 4063
Harvest/Process Date: 08/21/2018
Package Weight (g):20.4
Date Received: 09/14/2018
Test Date: 09/19/2018
Sample #111616

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.060 %

β-Ocimene:

0.020 %

Camphene:

0.020 %

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

0.250 %

α-Terpinolene:

0.060 %

β-Pinene:

0.100 %

Linalool:

0.120 %

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

0.080 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.190 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.460 %

α-Humulene:

0.280 %

Nerolidol 1:

0.030 %

Nerolidol 2:

0.030 %

Guaiol:

 N/D

Caryophyllene Oxide:

0.040 %

α-Bisabolol:

0.020 %

Other Terpenes

Total: 1.760%
a-Phellandrene = 0 % a-Terpineol = 0.07 % Valencene = 0.31 %

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4