IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 111541-001
Client Name, Sample Details

Grene MI LLC
Ypsilanti, MI 48197
Sample: Afghani Mango
License: P376728-200801
Type: Flower
Method: FE04P HPLC1100-1

Test Conditions

Scale: XS205-MI2
Temp: 22.7 °C
Baro Pressure: 988.2 hPa
Analyst: MEH
Technician: JRT

Sample ID#: 111541

Harvest/Process Date: 09/13/2018
Date Received: 09/13/2018
Test Date: 09/13/2018
Valid Through: 09/13/2019
Report Issued: 09/14/2018

Sample #111541
Sample #111541 Sample #111541
Test
Compounds
CBDV* CBDA CBD CBC* CBG* CBN THC THCA THCV* Calc. Max THC Calc. Max CBD
Amount N/D 1.3% N/D N/D N/D N/D 0.9% 18.9% N/D 17.5% 1.1%
LOQ 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1%
Uncertainty ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD

LOQ = Limit of Quantitation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates compounds that are not currently included in Iron Laboratories' accredited scope.

*** Designates tests that use the method FE-45.

Calc. Max is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the CBDA or THCA value.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories

Terpene Report by
Mass Spectrometer

Test Certificate #: 111541-001
Client Name, Sample Details

Grene MI LLC
Ypsilanti, MI 48197
Sample: Afghani Mango
License: P376728-200801
Type: Flower
Method: SOP FE-44-MI

Test Conditions

Scale: XS205-MI2
Temp: 22.3 °C
Baro Pressure: 981.8 hPa
Analyst: MEH
Technician: JRT

Sample ID#: 111541

Harvest/Process Date: 09/13/2018
Date Received: 09/13/2018
Test Date: 09/19/2018
Valid Through: 09/19/2019
Report Issued: 09/21/2018

Sample #111541

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.034 %

β-Ocimene:

0.096 %

Camphene:

N/D

Eucalyptol (1,8-Cineol):

N/D

Sabinene:

N/D

γ-Terpinene:

N/D

Myrcene:

0.257 %

α-Terpinolene:

N/D

β-Pinene:

0.029 %

Linalool:

0.036 %

∆3-Carene:

N/D

Fenchone:

N/D

α-Terpinene:

N/D

Fenchol:

0.045 %

Ocimene:

N/D

Isopulegol:

N/D

Limonene:

0.188 %

Geraniol:

N/D

4-Cymene:

N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.042 %

α-Humulene:

0.013 %

Nerolidol 1:

N/D

Nerolidol 2:

N/D

Guaiol:

N/D

Caryophyllene Oxide:

N/D

α-Bisabolol:

N/D

Other Terpenes

Total: 0.740%
(not included in calculated total): a-Terpineol = 0.026%

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 3

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Bio Analysis by
Microscopic Visual Inspection

Testing Accreditation #: 77802 Test Certificate #: 111541-001
Client Name, Sample Details

Grene MI LLC
Ypsilanti, MI 48197
Sample: Afghani Mango
License: P376728-200801
Type: Flower
Method: FE02 Microscope Dissection

Test Conditions

Analyst: ACR
Technician: ACR

Sample ID#: 111541

Harvest/Process Date: 09/13/2018
Date Received: 09/13/2018
Test Date: 09/13/2018
Valid Through: 09/13/2019
Report Issued: 09/13/2018

Sample #111541
Sample #111541 Sample #111541
Impurities: Not Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture 7

The gland heads range from small to large in size and are moderately abundant. Slightly more of them are clear than milky with a moderate amount turning amber in color. Some of the trichomes are damaged and degrading. A few of the trichomes are reduced due to stress.

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ACR - LM Iron laboratories ACR - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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