ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 111377-001
Client Name, Sample Details

GroHi Frams
Eugene, OR 97405
Sample: Lemonades
License: 100273799E9
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A401030000CF74000001177
Metrc Source Pkg#: 1A401030000CF74000001180
***Water Activity: 0.467
***Moisture: 11.51%
Test Conditions

Prepsheet ID#: ORP180913a
Scale: XS205-OR1
Temp: 21.6 °C
Baro Pressure: 1001 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 111377

Lot #: Lemonades 7-23-18
Batch #: 111377
Batch Weight (g): 6810
Harvest/Process Date: 09/10/2018
Package Weight (g):34.2
Date Received: 09/10/2018
Test Date: 09/13/2018
Sample #111377
Sample #111377 Sample #111377
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV Total THC Total CBD
Amount N/D 0.08% N/D 0.11% 0.19% 0.19% 0.67% 19.34% N/D 17.64% 0.07%
LOQ 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05%
Uncertainty 1.02% RPD 0.93% RPD 1.29% RPD 1.79% RPD 1.43% RPD 0.74% RPD ±5% RPD 0.75% RPD 1.05% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 111377-001
Client Name, Sample Details

GroHi Frams
Eugene, OR 97405
Sample: Lemonades
License: 100273799E9
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A401030000CF74000001177
Metrc Source Pkg#: 1A401030000CF74000001180
***Water Activity: 0.467
***Moisture: 11.51%
Test Conditions

Prepsheet ID#: ORP180913a
Scale: XS205-OR1
Temp: 21.6 °C
Baro Pressure: 1001 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 111377

Lot #: Lemonades 7-23-18
Batch #: 111377
Batch Weight (g): 6810
Harvest/Process Date: 09/10/2018
Package Weight (g):34.2
Date Received: 09/10/2018
Test Date: 09/13/2018
Sample #111377
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 6.03 5.84 96.85 5.9 97.84 1.02%
Cannabidiolic Acid (CBDA) N.D. 5.29 5.35 101.13 5.4 102.08 0.93%
Cannabigerol (CBG) N.D. 5.8 5.56 95.86 5.64 97.24 1.43%
Cannabidiol (CBD) N.D. 5.61 5.41 96.43 5.48 97.68 1.29%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.88 5.71 97.11 5.77 98.13 1.05%
Cannabinol (CBN) N.D. 5.62 5.37 95.55 5.41 96.26 0.74%
Δ9-Tetrahydrocannabinol (THC) N.D. 5.27 5.26 99.81 5.09 96.58 3.29%
Cannabichromene (CBC) N.D. 5.68 5.64 99.30 5.54 97.54 1.79%
Tetrahydrocannabinolic acid (THCA) N.D. 5.28 5.33 100.95 5.37 101.70 0.75%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 111377-001
Client Name, Sample Details

GroHi Frams
Eugene, OR 97405
Sample: Lemonades
License: 100273799E9
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030000CF74000001177
Metrc Source Pkg#: 1A401030000CF74000001180
Test Conditions

Prepsheet ID#: ORPS180912a
Scale: Veritas-OR1
Temp: 20.6 °C
Baro PE: 998.6 hPa
Analyst: JER
Technician: HRM
Sample ID#: 111377

Lot #: Lemonades 7-23-18
Batch #: 111377
Batch Weight (g): 6810
Harvest/Process Date: 09/10/2018
Package Weight (g):34.2
Date Received: 09/10/2018
Test Date: 09/14/2018
Sample #111377
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.140 Pass/<LOD Abamectin**** 0.500 0.140 Pass/<LOD
Acephate 0.400 0.140 Pass/<LOD Acequinocyl 2.000 0.279 Pass/<LOD
Acetamiprid 0.200 0.140 Pass/<LOD Azoxystrobin 0.200 0.140 Pass/<LOD
Bifenazate 0.200 0.140 Pass/<LOD Bifenthrin 0.200 0.140 Pass/<LOD
Boscalid 0.400 0.140 Pass/<LOD Carbaryl 0.200 0.140 Pass/<LOD
Carbofuran 0.200 0.140 Pass/<LOD Chlorantraniliprole 0.200 0.140 Pass/<LOD
Chlorfenapyr 1.000 0.558 Pass/<LOD Chlorpyrifos 0.200 0.140 Pass/<LOD
Clofentezine 0.200 0.140 Pass/<LOD Cyfluthrin** 1.000 0.558 Pass/<LOD
Cypermethrin*** 1.000 0.558 Pass/<LOD Daminozide 1.000 0.140 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.279 Pass/<LOD Diazinon 0.200 0.140 Pass/<LOD
Dimethoate 0.200 0.140 Pass/<LOD Ethoprophos 0.200 0.140 Pass/<LOD
Etofenprox 0.400 0.140 Pass/<LOD Etoxazole 0.200 0.140 Pass/<LOD
Fenoxycarb 0.200 0.140 Pass/<LOD Fenpyroximate 0.400 0.140 Pass/<LOD
Fipronil 0.400 0.140 Pass/<LOD Flonicamid 1.000 0.140 Pass/<LOD
Fludioxonil 0.400 0.140 Pass/<LOD Hexythiazox 1.000 0.140 Pass/<LOD
Imazalil 0.200 0.140 Pass/<LOD Imidacloprid 0.400 0.140 Pass/<LOD
Kresoxim Methyl 0.400 0.140 Pass/<LOD Malathion 0.200 0.140 Pass/<LOD
Metalaxyl 0.200 0.140 Pass/<LOD Methiocarb 0.200 0.140 Pass/<LOD
Methomyl 0.400 0.140 Pass/<LOD Methyl Parathion 0.200 0.140 Pass/<LOD
MGK-264‡ 0.200 0.140 Pass/<LOD Myclobutanil 0.000 0.140 Pass/<LOD
Naled 0.500 0.140 Pass/<LOD Oxamyl 1.000 0.140 Pass/<LOD
Paclobutrazol 0.400 0.140 Pass/<LOD Permethrins† 0.200 0.140 Pass/<LOD
Phosmet 0.200 0.140 Pass/<LOD Piperonyl Butoxide 2.000 0.140 Pass/<LOD
Prallethrin 0.200 0.140 Pass/<LOD Propiconazole 0.400 0.140 Pass/<LOD
Propoxur 0.200 0.140 Pass/<LOD Pyrethrins* 1.000 0.140 Pass/<LOD
Pyridaben 0.200 0.140 Pass/<LOD Spinosad***** 0.200 0.140 Pass/<LOD
Spiromesifen 0.200 0.140 Pass/<LOD Spirotetramat 0.200 0.140 Pass/<LOD
Spiroxamine‡ 0.400 0.140 Pass/<LOD Tebuconazole 0.400 0.140 Pass/<LOD
Thiacloprid 0.200 0.140 Pass/<LOD Thiamethoxam 0.200 0.140 Pass/<LOD
Trifloxystrobin 0.200 0.140 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 111377-001
Client Name, Sample Details

GroHi Frams
Eugene, OR 97405
Sample: Lemonades
License: 100273799E9
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030000CF74000001177
Metrc Source Pkg#: 1A401030000CF74000001180
Test Conditions

Prepsheet ID#: ORPS180912a
Scale: Veritas-OR1
Temp: 20.6 °C
Baro PE: 998.6 hPa
Analyst: JER
Technician: HRM
Sample ID#: 111377

Lot #: Lemonades 7-23-18
Batch #: 111377
Batch Weight (g): 6810
Harvest/Process Date: 09/10/2018
Package Weight (g):34.2
Date Received: 09/10/2018
Test Date: 09/14/2018
Sample #111377
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.907 0.813 90.70 81.30 10.93
Acequinocyl N.D. 1 0.682 0.692 68.20 69.20 1.46
Acetamiprid N.D. 1 0.986 0.958 98.60 95.80 2.88
Aldicarb N.D. 1 0.921 0.9 92.10 90.00 2.31
Avermectin B1a N.D. 0.97 1.11 1.19 114.43 122.68 6.96
Azoxystrobin N.D. 1 1.1 1.03 110.00 103.00 6.57
Bifenazate N.D. 1 0.927 0.901 92.70 90.10 2.84
Bifenthrin N.D. 1 0.97 0.948 97.00 94.80 2.29
Boscalid N.D. 1 1.05 1.07 105.00 107.00 1.89
Carbaryl N.D. 1 0.963 0.898 96.30 89.80 6.99
Carbofuran N.D. 1 1.02 0.974 102.00 97.40 4.61
Chlorantraniliprole N.D. 1 0.897 0.91 89.70 91.00 1.44
Chlorfenapyr N.D. 1 0.98 1.06 98.00 106.00 7.84
Chlorpyriphos N.D. 1 1.01 1.06 101.00 106.00 4.83
Clofentezine N.D. 1 0.797 0.768 79.70 76.80 3.71
Cyfluthrin N.D. 1 1.1 1.03 110.00 103.00 6.57
Cypermethrin N.D. 1 1.04 0.975 104.00 97.50 6.45
Daminoside N.D. 1 0.664 0.592 66.40 59.20 11.46 LR
Diazanon N.D. 1 2.46 1.92 246.00 192.00 24.66 HRQ
Dichlorvos N.D. 1 0.81 0.74 81.00 74.00 9.03
Dimethoate N.D. 1 0.919 0.903 91.90 90.30 1.76
Ethoprophos N.D. 1 0.934 0.874 93.40 87.40 6.64
Etofenprox N.D. 1 1.13 1.13 113.00 113.00 0.00
Etoxazole N.D. 1 1.28 1.3 128.00 130.00 1.55
Fenoxycarb N.D. 1 0.912 0.91 91.20 91.00 0.22
Fenpyroximate N.D. 1 1.14 1.12 114.00 112.00 1.77
Fipronil N.D. 1 1.11 1.07 111.00 107.00 3.67
Flonicamid N.D. 1 0.927 0.885 92.70 88.50 4.64
Fludioxonil N.D. 1 1.07 1.02 107.00 102.00 4.78
Hexythiazox N.D. 1 1.08 1.04 108.00 104.00 3.77
Imazalil N.D. 1 0.897 0.909 89.70 90.90 1.33
Imidacloprid N.D. 1 0.874 0.852 87.40 85.20 2.55
Kresoxim-methyl N.D. 1 0.983 0.83 98.30 83.00 16.88
Malathion N.D. 1 0.897 1 89.70 100.00 10.86
Metalaxyl N.D. 1 0.869 0.924 86.90 92.40 6.13
Methiocarb N.D. 1 0.942 0.914 94.20 91.40 3.02
Methomyl N.D. 1 0.839 0.86 83.90 86.00 2.47
MGK-264 N.D. 1 0.871 0.855 87.10 85.50 1.85
Myclobutanil N.D. 1 0.951 0.875 95.10 87.50 8.32
Naled (dibrom) N.D. 1 0.723 0.669 72.30 66.90 7.76 LR
Oxamyl N.D. 1 0.938 0.873 93.80 87.30 7.18
Paclobutrazol N.D. 1 0.915 0.862 91.50 86.20 5.97
Parathion-methyl N.D. 1 0.992 0.967 99.20 96.70 2.55
Permethrins N.D. 1 1.04 1.01 104.00 101.00 2.93
Phosmet N.D. 1 0.931 0.914 93.10 91.40 1.84
Piperonyl butoxide N.D. 1 1.24 1.14 124.00 114.00 8.40
Prallethrin N.D. 1 0.999 0.976 99.90 97.60 2.33
Propiconazole N.D. 1 0.987 1.01 98.70 101.00 2.30
Propoxur N.D. 1 1.04 0.954 104.00 95.40 8.63
Pyrethrin N.D. 0.65 0.609 0.603 93.69 92.77 0.99
Pyridaben N.D. 1 1.09 1.13 109.00 113.00 3.60
SpinosynA N.D. 0.84 0.227 0.196 27.02 23.33 14.66 LR
SpinosynD N.D. 0.16 0.145 0.18 90.63 112.50 21.54 Q
Spiromesifen N.D. 1 0.378 0.38 37.80 38.00 0.53 LR
Spirotetramat N.D. 1 0.916 0.894 91.60 89.40 2.43
Spiroxamine N.D. 1 0.955 0.919 95.50 91.90 3.84
Tebuconazole N.D. 1 0.959 0.936 95.90 93.60 2.43
Thiacloprid N.D. 1 0.939 0.879 93.90 87.90 6.60
Thiamethoxam N.D. 1 0.9 0.87 90.00 87.00 3.39
Trifloxystrobin N.D. 1 1.09 1.08 109.00 108.00 0.92

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 111377-001
Client Name, Sample Details

GroHi Frams
Eugene, OR 97405
Sample: Lemonades
License: 100273799E9
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030000CF74000001177
Metrc Source Pkg#: 1A401030000CF74000001180
Test Conditions

Scale: XS205-OR1
Temp: 20.8 °C
Baro Pressure: 999.6 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 111377

Lot #: Lemonades 7-23-18
Batch #: 111377
Batch Weight (g): 6810
Harvest/Process Date: 09/10/2018
Package Weight (g):34.2
Date Received: 09/10/2018
Test Date: 09/12/2018
Sample #111377

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.080 %

β-Ocimene:

0.180 %

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

0.020 %

Sabinene:

0.030 %

γ-Terpinene:

0.080 %

Myrcene:

0.110 %

α-Terpinolene:

0.490 %

β-Pinene:

0.120 %

Linalool:

 N/D

∆3-Carene:

0.050 %

Fenchone:

 N/D

α-Terpinene:

0.180 %

Fenchol:

0.050 %

Ocimene:

0.050 %

Isopulegol:

 N/D

Limonene:

0.100 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.480 %

α-Humulene:

0.220 %

Nerolidol 1:

0.020 %

Nerolidol 2:

0.020 %

Guaiol:

 N/D

Caryophyllene Oxide:

0.040 %

α-Bisabolol:

0.030 %

Other Terpenes

Total: 2.350%
a-Phellandrene = 0.41 % a-Terpineol = 0.07 % Valencene = 0.19 %

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4