ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 109845-001
Client Name, Sample Details

Robert Drake
Veneta, OR 97487
Sample: Saphire OG
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
***Water Activity: 0.5
***Moisture: 12.33%
Test Conditions

Prepsheet ID#: P180726a
Scale: XS205-OR1
Temp: 21.2 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 109845

Lot #: 7-10-18
Batch #: 109845
Batch Weight (g): 1589
Harvest/Process Date: 07/10/2018
Package Weight (g):9.1
Date Received: 07/23/2018
Test Date: 07/26/2018
Sample #109845
Sample #109845 Sample #109845
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV Total THC Total CBD
Amount N/D N/D N/D N/D 0.09% N/D 0.49% 19.37% N/D 17.47% 0.00%
LOQ 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05%
Uncertainty 3.56% RPD 0.55% RPD 1.14% RPD 3.47% RPD 0.40% RPD 2.09% RPD ±5% RPD 10.37% RPD 1.16% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 3

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 109845-001
Client Name, Sample Details

Robert Drake
Veneta, OR 97487
Sample: Saphire OG
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
***Water Activity: 0.5
***Moisture: 12.33%
Test Conditions

Prepsheet ID#: P180726a
Scale: XS205-OR1
Temp: 21.2 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 109845

Lot #: 7-10-18
Batch #: 109845
Batch Weight (g): 1589
Harvest/Process Date: 07/10/2018
Package Weight (g):9.1
Date Received: 07/23/2018
Test Date: 07/26/2018
Sample #109845
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.9 4.96 101.22 5.14 104.90 3.56%
Cannabidiolic Acid (CBDA) N.D. 5.05 5.46 108.12 5.49 108.71 0.55%
Cannabigerol (CBG) N.D. 4.95 4.94 99.80 4.96 100.20 0.40%
Cannabidiol (CBD) N.D. 5.03 5.23 103.98 5.29 105.17 1.14%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.09 5.14 100.98 5.2 102.16 1.16%
Cannabinol (CBN) N.D. 5.3 5.22 98.49 5.33 100.57 2.09%
Δ9-Tetrahydrocannabinol (THC) N.D. 5.22 5.12 98.08 5.26 100.77 2.70%
Cannabichromene (CBC) N.D. 5.3 5.09 96.04 5.27 99.43 3.47%
Tetrahydrocannabinolic acid (THCA) N.D. 5.23 5.67 108.41 6.29 120.27 10.37%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 3

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 109845-001
Client Name, Sample Details

Robert Drake
Veneta, OR 97487
Sample: Saphire OG
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Prepsheet ID#: PS180724a
Scale: Veritas-OR1
Temp: 21.6 °C
Baro Pressure: 1003 hPa
Analyst: JER
Technician: JER
Sample ID#: 109845

Lot #: 7-10-18
Batch #: 109845
Batch Weight (g): 1589
Harvest/Process Date: 07/10/2018
Package Weight (g):9.1
Date Received: 07/23/2018
Test Date: 07/25/2018
Sample #109845
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.120 Pass/<LOD Abamectin**** 0.500 0.120 Pass/<LOD
Acephate 0.400 0.120 Pass/<LOD Acequinocyl 2.000 0.240 Pass/<LOD
Acetamiprid 0.200 0.120 Pass/<LOD Azoxystrobin 0.200 0.120 Pass/<LOD
Bifenazate 0.200 0.120 Pass/<LOD Bifenthrin 0.200 0.120 Pass/<LOD
Boscalid 0.400 0.120 Pass/<LOD Carbaryl 0.200 0.120 Pass/<LOD
Carbofuran 0.200 0.120 Pass/<LOD Chlorantraniliprole 0.200 0.120 Pass/<LOD
Chlorfenapyr 1.000 0.481 Pass/<LOD Chlorpyrifos 0.200 0.120 Pass/<LOD
Clofentezine 0.200 0.120 Pass/<LOD Cyfluthrin** 1.000 0.481 Pass/<LOD
Cypermethrin*** 1.000 0.481 Pass/<LOD Daminozide 1.000 0.120 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.240 Pass/<LOD Diazinon 0.200 0.120 Pass/<LOD
Dimethoate 0.200 0.120 Pass/<LOD Ethoprophos 0.200 0.120 Pass/<LOD
Etofenprox 0.400 0.120 Pass/<LOD Etoxazole 0.200 0.120 Pass/<LOD
Fenoxycarb 0.200 0.120 Pass/<LOD Fenpyroximate 0.400 0.120 Pass/<LOD
Fipronil 0.400 0.120 Pass/<LOD Flonicamid 1.000 0.120 Pass/<LOD
Fludioxonil 0.400 0.120 Pass/<LOD Hexythiazox 1.000 0.120 Pass/<LOD
Imazalil 0.200 0.120 Pass/<LOD Imidacloprid 0.400 0.120 Pass/<LOD
Kresoxim Methyl 0.400 0.120 Pass/<LOD Malathion 0.200 0.120 Pass/<LOD
Metalaxyl 0.200 0.120 Pass/<LOD Methiocarb 0.200 0.120 Pass/<LOD
Methomyl 0.400 0.120 Pass/<LOD Methyl Parathion 0.200 0.120 Pass/<LOD
MGK-264‡ 0.200 0.120 Pass/<LOD Myclobutanil 0.000 0.120 Pass/<LOD
Naled 0.500 0.120 Pass/<LOD Oxamyl 1.000 0.120 Pass/<LOD
Paclobutrazol 0.400 0.120 Pass/<LOD Permethrins† 0.200 0.120 Pass/<LOD
Phosmet 0.200 0.120 Pass/<LOD Piperonyl Butoxide 2.000 0.120 Pass/<LOD
Prallethrin 0.200 0.120 Pass/<LOD Propiconazole 0.400 0.120 Pass/<LOD
Propoxur 0.200 0.120 Pass/<LOD Pyrethrins* 1.000 0.120 Pass/<LOD
Pyridaben 0.200 0.120 Pass/<LOD Spinosad***** 0.200 0.120 Pass/<LOD
Spiromesifen 0.200 0.120 Pass/<LOD Spirotetramat 0.200 0.120 Pass/<LOD
Spiroxamine‡ 0.400 0.120 Pass/<LOD Tebuconazole 0.400 0.120 Pass/<LOD
Thiacloprid 0.200 0.120 Pass/<LOD Thiamethoxam 0.200 0.120 Pass/<LOD
Trifloxystrobin 0.200 0.120 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 3

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 109845-001
Client Name, Sample Details

Robert Drake
Veneta, OR 97487
Sample: Saphire OG
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Prepsheet ID#: PS180724a
Scale: Veritas-OR1
Temp: 21.6 °C
Baro Pressure: 1003 hPa
Analyst: JER
Technician: JER
Sample ID#: 109845

Lot #: 7-10-18
Batch #: 109845
Batch Weight (g): 1589
Harvest/Process Date: 07/10/2018
Package Weight (g):9.1
Date Received: 07/23/2018
Test Date: 07/25/2018
Sample #109845
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.919 0.993 91.90 99.30 7.74
Acequinocyl N.D. 1 0.858 0.865 85.80 86.50 0.81
Acetamiprid N.D. 1 1 1.08 100.00 108.00 7.69
Aldicarb N.D. 1 1.01 1.07 101.00 107.00 5.77
Avermectin B1a N.D. 1 0.901 0.984 90.10 98.40 8.81
Azoxystrobin N.D. 1 0.907 0.992 90.70 99.20 8.95
Bifenazate N.D. 1 0.92 0.925 92.00 92.50 0.54
Bifenthrin N.D. 1 0.917 0.969 91.70 96.90 5.51
Boscalid N.D. 1 0.874 0.944 87.40 94.40 7.70
Carbaryl N.D. 1 1.06 1.13 106.00 113.00 6.39
Carbofuran N.D. 1 1.02 1.08 102.00 108.00 5.71
Chlorantraniliprole N.D. 1 0.761 0.856 76.10 85.60 11.75
Chlorfenapyr N.D. 1 1.06 1.02 106.00 102.00 3.85
Chlorpyriphos N.D. 1 0.911 0.951 91.10 95.10 4.30
Clofentezine N.D. 1 0.859 0.846 85.90 84.60 1.52
Cyfluthrin N.D. 1 0.951 0.915 95.10 91.50 3.86
Cypermethrin N.D. 1 1.07 1.09 107.00 109.00 1.85
Daminoside N.D. 1 0.683 0.713 68.30 71.30 4.30 LR
Diazanon N.D. 1 1.1 1.14 110.00 114.00 3.57
Dichlorvos N.D. 1 0.926 0.93 92.60 93.00 0.43
Dimethoate N.D. 1 0.961 1.04 96.10 104.00 7.90
Ethoprophos N.D. 1 0.823 0.888 82.30 88.80 7.60
Etofenprox N.D. 1 1.11 1.17 111.00 117.00 5.26
Etoxazole N.D. 1 1.01 1.04 101.00 104.00 2.93
Fenoxycarb N.D. 1 0.827 0.847 82.70 84.70 2.39
Fenpyroximate N.D. 1 1.07 1.11 107.00 111.00 3.67
Fipronil N.D. 1 1.09 1.03 109.00 103.00 5.66
Flonicamid N.D. 1 0.916 1.03 91.60 103.00 11.72
Fludioxonil N.D. 1 1.11 1.05 111.00 105.00 5.56
Hexythiazox N.D. 1 0.883 0.944 88.30 94.40 6.68
Imazalil N.D. 1 0.817 0.86 81.70 86.00 5.13
Imidacloprid N.D. 1 0.919 0.921 91.90 92.10 0.22
Kresoxim-methyl N.D. 1 0.819 0.895 81.90 89.50 8.87
Malathion N.D. 1 0.82 0.884 82.00 88.40 7.51
Metalaxyl N.D. 1 0.842 0.88 84.20 88.00 4.41
Methiocarb N.D. 1 0.962 1.04 96.20 104.00 7.79
Methomyl N.D. 1 0.822 0.882 82.20 88.20 7.04
MGK-264 N.D. 1 0.8 0.808 80.00 80.80 1.00
Myclobutanil N.D. 1 0.776 0.848 77.60 84.80 8.87
Naled (dibrom) N.D. 1 0.947 1.06 94.70 106.00 11.26
Oxamyl N.D. 1 0.912 0.984 91.20 98.40 7.59
Paclobutrazol N.D. 1 0.858 0.903 85.80 90.30 5.11
Parathion-methyl N.D. 1 1.07 1.14 107.00 114.00 6.33
Permethrins N.D. 1 1.03 1.06 103.00 106.00 2.87
Phosmet N.D. 1 0.864 0.889 86.40 88.90 2.85
Piperonyl butoxide N.D. 1 1.08 1.14 108.00 114.00 5.41
Prallethrin N.D. 1 0.803 0.823 80.30 82.30 2.46
Propiconazole N.D. 1 0.834 0.867 83.40 86.70 3.88
Propoxur N.D. 1 1.08 1.14 108.00 114.00 5.41
Pyrethrin N.D. 1 0.506 0.561 50.60 56.10 10.31
Pyridaben N.D. 1 0.956 1.02 95.60 102.00 6.48
SpinosynA N.D. 1 0.502 0.681 50.20 68.10 30.26 LRQ
SpinosynD N.D. 1 0.0771 0.125 7.71 12.50 47.40 LRQ
Spiromesifen N.D. 1 0.633 0.645 63.30 64.50 1.88
Spirotetramat N.D. 1 0.934 1.01 93.40 101.00 7.82
Spiroxamine N.D. 1 0.87 0.901 87.00 90.10 3.50
Tebuconazole N.D. 1 0.83 0.905 83.00 90.50 8.65
Thiacloprid N.D. 1 0.904 0.965 90.40 96.50 6.53
Thiamethoxam N.D. 1 0.807 0.895 80.70 89.50 10.34
Trifloxystrobin N.D. 1 1.05 1.14 105.00 114.00 8.22

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 3