ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 106553-001
Client Name, Sample Details

Self Made Cannabis Company
Portland, OR 97227
Sample: Alien Grenades
License: 060 1002 9559 A03
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300003B63000002614
Metrc Source Pkg#: 1A4010300009FC7000002939
***Water Activity: 0.601
***Moisture: 13.44%
Test Conditions

Prepsheet ID#: P180516a
Scale: XS205-OR1
Temp: 21.3 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 106553

Lot #: 10/4/17
Batch #: 106553
Batch Weight (g): 6804
Harvest/Process Date: 10/04/2017
Date Received: 05/10/2018
Test Date: 05/16/2018
Sample #106553
Sample #106553 Sample #106553
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV Total THC Total CBD
Amount N/D 0.06% N/D 0.15% 0.11% N/D 4.38% 17.76% N/D 19.95% 0.05%
LOQ 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05%
Uncertainty 1.58% RPD 0.74% RPD 0.90% RPD 11.18% RPD 0.00% RPD 1.65% RPD ±5% RPD 1.42% RPD 0.96% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 5

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 106553-001
Client Name, Sample Details

Self Made Cannabis Company
Portland, OR 97227
Sample: Alien Grenades
License: 060 1002 9559 A03
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300003B63000002614
Metrc Source Pkg#: 1A4010300009FC7000002939
***Water Activity: 0.601
***Moisture: 13.44%
Test Conditions

Prepsheet ID#: P180516a
Scale: XS205-OR1
Temp: 21.3 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 106553

Lot #: 10/4/17
Batch #: 106553
Batch Weight (g): 6804
Harvest/Process Date: 10/04/2017
Date Received: 05/10/2018
Test Date: 05/16/2018
Sample #106553
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.87 5.01 102.87 5.09 104.52 1.58%
Cannabidiolic Acid (CBDA) N.D. 5.13 5.46 106.43 5.42 105.65 0.74%
Cannabigerol (CBG) N.D. 5 5.02 100.40 5.02 100.40 0.00%
Cannabidiol (CBD) N.D. 5.53 5.52 99.82 5.57 100.72 0.90%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.22 5.19 99.43 5.24 100.38 0.96%
Cannabinol (CBN) N.D. 5.6 5.4 96.43 5.49 98.04 1.65%
Δ9-Tetrahydrocannabinol (THC) N.D. 5.9 6.67 113.05 6.76 114.58 1.34%
Cannabichromene (CBC) N.D. 6.62 6.08 91.84 6.8 102.72 11.18%
Tetrahydrocannabinolic acid (THCA) N.D. 5.67 5.61 98.94 5.69 100.35 1.42%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 5

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-002 Test Certificate #: 106553-001
Client Name, Sample Details

Self Made Cannabis Company
Portland, OR 97227
Sample: Alien Grenades
License: 060 1002 9559 A03
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300003B63000002614
Metrc Source Pkg#: 1A4010300009FC7000002939
***Water Activity: 0.601
***Moisture: 13.44%
Test Conditions

Prepsheet ID#: P180516a
Scale: XS205-OR1
Temp: 21.3 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 106553

Lot #: 10/4/17
Batch #: 106553
Batch Weight (g): 6804
Harvest/Process Date: 10/04/2017
Date Received: 05/10/2018
Test Date: 05/16/2018
Sample #106553
Sample #106553 Sample #106553
Test
Compounds		 CBDV CBDA CBD CBC CBG CBN THC THCA THCV Total THC Total CBD
Amount N/D 0.06% N/D 0.15% 0.11% N/D 4.38% 17.76% N/D 19.95% 0.05%
LOQ 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05% 0.05%
Uncertainty 1.58% RPD 0.74% RPD 0.90% RPD 11.18% RPD 0.00% RPD 1.65% RPD ±5% RPD 1.42% RPD 0.96% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 5

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 106553-001
Client Name, Sample Details

Self Made Cannabis Company
Portland, OR 97227
Sample: Alien Grenades
License: 060 1002 9559 A03
Type: Adult Use Flower
Method: FE04-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300003B63000002614
Metrc Source Pkg#: 1A4010300009FC7000002939
***Water Activity: 0.601
***Moisture: 13.44%
Test Conditions

Prepsheet ID#: P180516a
Scale: XS205-OR1
Temp: 21.3 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: EDT
Sample ID#: 106553

Lot #: 10/4/17
Batch #: 106553
Batch Weight (g): 6804
Harvest/Process Date: 10/04/2017
Date Received: 05/10/2018
Test Date: 05/16/2018
Sample #106553
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.87 5.01 102.87 5.09 104.52 1.58%
Cannabidiolic Acid (CBDA) N.D. 5.13 5.46 106.43 5.42 105.65 0.74%
Cannabigerol (CBG) N.D. 5 5.02 100.40 5.02 100.40 0.00%
Cannabidiol (CBD) N.D. 5.53 5.52 99.82 5.57 100.72 0.90%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.22 5.19 99.43 5.24 100.38 0.96%
Cannabinol (CBN) N.D. 5.6 5.4 96.43 5.49 98.04 1.65%
Δ9-Tetrahydrocannabinol (THC) N.D. 5.9 6.67 113.05 6.76 114.58 1.34%
Cannabichromene (CBC) N.D. 6.62 6.08 91.84 6.8 102.72 11.18%
Tetrahydrocannabinolic acid (THCA) N.D. 5.67 5.61 98.94 5.69 100.35 1.42%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 5

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 106553-001
Client Name, Sample Details

Self Made Cannabis Company
Portland, OR 97227
Sample: Alien Grenades
License: 060 1002 9559 A03
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300003B63000002614
Metrc Source Pkg#: 1A4010300009FC7000002939
Test Conditions

Prepsheet ID#: PS180515a
Scale: Veritas-OR1
Temp: 22.3 °C
Baro PE: 999.4 hPa
Analyst: JER
Technician: JER
Sample ID#: 106553

Lot #: 10/4/17
Batch #: 106553
Batch Weight (g): 6804
Harvest/Process Date: 10/04/2017
Date Received: 05/10/2018
Test Date: 05/17/2018
Sample #106553
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.125 Pass/<LOD Abamectin**** 0.500 0.125 Pass/<LOD
Acephate 0.400 0.125 Pass/<LOD Acequinocyl 2.000 0.249 Pass/<LOD
Acetamiprid 0.200 0.125 Pass/<LOD Azoxystrobin 0.200 0.125 Pass/<LOD
Bifenazate 0.200 0.125 Pass/<LOD Bifenthrin 0.200 0.125 Pass/<LOD
Boscalid 0.400 0.125 Pass/<LOD Carbaryl 0.200 0.125 Pass/<LOD
Carbofuran 0.200 0.125 Pass/<LOD Chlorantraniliprole 0.200 0.125 Pass/<LOD
Chlorfenapyr 1.000 0.499 Pass/<LOD Chlorpyrifos 0.200 0.125 Pass/<LOD
Clofentezine 0.200 0.125 Pass/<LOD Cyfluthrin** 1.000 0.499 Pass/<LOD
Cypermethrin*** 1.000 0.499 Pass/<LOD Daminozide 1.000 0.125 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.249 Pass/<LOD Diazinon 0.200 0.125 Pass/<LOD
Dimethoate 0.200 0.125 Pass/<LOD Ethoprophos 0.200 0.125 Pass/<LOD
Etofenprox 0.400 0.125 Pass/<LOD Etoxazole 0.200 0.125 Pass/<LOD
Fenoxycarb 0.200 0.125 Pass/<LOD Fenpyroximate 0.400 0.125 Pass/<LOD
Fipronil 0.400 0.125 Pass/<LOD Flonicamid 1.000 0.125 Pass/<LOD
Fludioxonil 0.400 0.125 Pass/<LOD Hexythiazox 1.000 0.125 Pass/<LOD
Imazalil 0.200 0.125 Pass/<LOD Imidacloprid 0.400 0.125 Pass/<LOD
Kresoxim Methyl 0.400 0.125 Pass/<LOD Malathion 0.200 0.125 Pass/<LOD
Metalaxyl 0.200 0.125 Pass/<LOD Methiocarb 0.200 0.125 Pass/<LOD
Methomyl 0.400 0.125 Pass/<LOD Methyl Parathion 0.200 0.125 Pass/<LOD
MGK-264‡ 0.200 0.125 Pass/<LOD Myclobutanil 0.000 0.125 Pass/<LOD
Naled 0.500 0.125 Pass/<LOD Oxamyl 1.000 0.125 Pass/<LOD
Paclobutrazol 0.400 0.125 Pass/<LOD Permethrins† 0.200 0.125 Pass/<LOD
Phosmet 0.200 0.125 Pass/<LOD Piperonyl Butoxide 2.000 0.125 Pass/<LOD
Prallethrin 0.200 0.125 Pass/<LOD Propiconazole 0.400 0.125 Pass/<LOD
Propoxur 0.200 0.125 Pass/<LOD Pyrethrins* 1.000 0.125 Pass/<LOD
Pyridaben 0.200 0.125 Pass/<LOD Spinosad***** 0.200 0.125 Pass/<LOD
Spiromesifen 0.200 0.125 Pass/<LOD Spirotetramat 0.200 0.125 Pass/<LOD
Spiroxamine‡ 0.400 0.125 Pass/<LOD Tebuconazole 0.400 0.125 Pass/<LOD
Thiacloprid 0.200 0.125 Pass/<LOD Thiamethoxam 0.200 0.125 Pass/<LOD
Trifloxystrobin 0.200 0.125 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 5

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 106553-001
Client Name, Sample Details

Self Made Cannabis Company
Portland, OR 97227
Sample: Alien Grenades
License: 060 1002 9559 A03
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300003B63000002614
Metrc Source Pkg#: 1A4010300009FC7000002939
Test Conditions

Prepsheet ID#: PS180515a
Scale: Veritas-OR1
Temp: 22.3 °C
Baro PE: 999.4 hPa
Analyst: JER
Technician: JER
Sample ID#: 106553

Lot #: 10/4/17
Batch #: 106553
Batch Weight (g): 6804
Harvest/Process Date: 10/04/2017
Date Received: 05/10/2018
Test Date: 05/17/2018
Sample #106553
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 .688 .699 68.80 69.90 1.59 LR
Acequinocyl N.D. 1 .74 .713 74.00 71.30 3.72
Acetamiprid N.D. 1 1.08 1.06 108.00 106.00 1.87
Aldicarb N.D. 1 .905 .867 90.50 86.70 4.29
Avermectin B1a N.D. .97 1 1.03 103.09 106.19 2.96
Azoxystrobin N.D. 1 1.06 1.05 106.00 105.00 0.95
Bifenazate N.D. 1 .684 .673 68.40 67.30 1.62 LR
Bifenthrin N.D. 1 .76 .833 76.00 83.30 9.17
Boscalid N.D. 1 .749 .753 74.90 75.30 0.53
Carbaryl N.D. 1 1.05 1.04 105.00 104.00 0.96
Carbofuran N.D. 1 1.24 1.22 124.00 122.00 1.63
Chlorantraniliprole N.D. 1 .804 .795 80.40 79.50 1.13
Chlorfenapyr N.D. 1 1.07 1.1 107.00 110.00 2.76
Chlorpyriphos N.D. 1 .818 .837 81.80 83.70 2.30
Clofentezine N.D. 1 .781 .774 78.10 77.40 0.90
Cyfluthrin N.D. 1 .802 .803 80.20 80.30 0.12
Cypermethrin N.D. 1 .779 .874 77.90 87.40 11.49
Daminoside N.D. 1 .455 .470 45.50 47.00 3.24 LR
Diazanon N.D. 1 .742 .756 74.20 75.60 1.87
Dichlorvos N.D. 1 .815 .778 81.50 77.80 4.65
Dimethoate N.D. 1 .918 .895 91.80 89.50 2.54
Ethoprophos N.D. 1 .822 .848 82.20 84.80 3.11
Etofenprox N.D. 1 1.27 1.3 127.00 130.00 2.33
Etoxazole N.D. 1 1.02 1.03 102.00 103.00 0.98
Fenoxycarb N.D. 1 .762 .757 76.20 75.70 0.66
Fenpyroximate N.D. 1 1.12 1.06 112.00 106.00 5.50
Fipronil N.D. 1 1.15 1.14 115.00 114.00 0.87
Flonicamid N.D. 1 .888 .89 88.80 89.00 0.22
Fludioxonil N.D. 1 1.09 1.09 109.00 109.00 0.00
Hexythiazox N.D. 1 .918 .927 91.80 92.70 0.98
Imazalil N.D. 1 .905 .88 90.50 88.00 2.80
Imidacloprid N.D. 1 .751 .726 75.10 72.60 3.39
Kresoxim-methyl N.D. 1 .706 .714 70.60 71.40 1.13
Malathion N.D. 1 .744 .759 74.40 75.90 2.00
Metalaxyl N.D. 1 .731 .724 73.10 72.40 0.96
Methiocarb N.D. 1 .994 .998 99.40 99.80 0.40
Methomyl N.D. 1 .598 .592 59.80 59.20 1.01 LR
MGK-264 N.D. 1 .642 .617 64.20 61.70 3.97 LR
Myclobutanil N.D. 1 .902 .892 90.20 89.20 1.11
Naled (dibrom) N.D. 1 .928 .92 92.80 92.00 0.87
Oxamyl N.D. 1 .825 .81 82.50 81.00 1.83
Paclobutrazol N.D. 1 .817 .789 81.70 78.90 3.49
Parathion-methyl N.D. 1 1.01 1.04 101.00 104.00 2.93
Permethrins N.D. 1 1.06 1.1 106.00 110.00 3.70
Phosmet N.D. 1 .685 .690 68.50 69.00 0.73 LR
Piperonyl butoxide N.D. 1 1.05 1.06 105.00 106.00 0.95
Prallethrin N.D. 1 .701 .67 70.10 67.00 4.52 LR
Propiconazole N.D. 1 .815 .833 81.50 83.30 2.18
Propoxur N.D. 1 1.22 1.18 122.00 118.00 3.33
Pyrethrin N.D. .65 .478 .472 73.54 72.62 1.26
Pyridaben N.D. 1 1.07 .985 107.00 98.50 8.27
SpinosynA N.D. .84 .602 .607 71.67 72.26 0.83
SpinosynD N.D. .16 .102 .0967 63.75 60.44 5.33 LR
Spiromesifen N.D. 1 .76 .736 76.00 73.60 3.21
Spirotetramat N.D. 1 .953 .96 95.30 96.00 0.73
Spiroxamine N.D. 1 .816 .799 81.60 79.90 2.11
Tebuconazole N.D. 1 .773 .76 77.30 76.00 1.70
Thiacloprid N.D. 1 .843 .828 84.30 82.80 1.80
Thiamethoxam N.D. 1 .689 .666 68.90 66.60 3.39 LR
Trifloxystrobin N.D. 1 1.06 1.05 106.00 105.00 0.95

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 5
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 106553-001
Client Name, Sample Details

Self Made Cannabis Company
Portland, OR 97227
Sample: Alien Grenades
License: 060 1002 9559 A03
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003B63000002614
Metrc Source Pkg#: 1A4010300009FC7000002939
Test Conditions

Scale: XS205-OR1
Temp: 21.3 °C
Baro Pressure: 994.8 hPa
Analyst: JER
Technician: EDT
Sample ID#: 106553

Lot #: 10/4/17
Batch #: 106553
Batch Weight (g): 6804
Harvest/Process Date: 10/04/2017
Date Received: 05/10/2018
Test Date: 05/15/2018
Sample #106553

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.190 %

β-Ocimene:

0.120 %

Camphene:

0.010 %

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

0.010 %

Myrcene:

 N/D

α-Terpinolene:

0.010 %

β-Pinene:

0.160 %

Linalool:

0.050 %

∆3-Carene:

 N/D

Fenchone:

0.010 %

α-Terpinene:

0.010 %

Fenchol:

0.060 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.140 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.420 %

α-Humulene:

0.180 %

Nerolidol 1:

0.050 %

Nerolidol 2:

0.010 %

Guaiol:

 N/D

Caryophyllene Oxide:

0.010 %

α-Bisabolol:

0.140 %

Other Terpenes

Total: 1.580%
a-Phellandrene = 0.00 % a-Terpineol = 0.06 % Valencene = 0.00 %

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 5