IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
Gas Chromatography
Testing Accreditation #: 77802 Test Certificate #: 104319-001
Client Name, Sample Details

The Real Biz
, MI
Sample: Gorilla Glue Wax
Type: Medical Compliant Flower
Method: FE03 GC6890-1
Test Conditions

Scale: XS205-MI1
Temp: 21.4 °C
Baro Pressure: 970.8 hPa
Analyst: CTM
Technician: JCM
Sample ID#: 104319

Harvest/Process Date: 03/15/2018
Date Received: 03/15/2018
Test Date: 03/15/2018
Valid Through: 03/15/2019
Report Issued: 03/16/2018
Sample #104319
Sample #104319 Sample #104319
Test
Compounds		 CBDV THCV CBC CBD Δ8 THC Δ9 THC CBG CBN TOTAL
Amount N/D 1.4 1.0 0.2 N/D 59.3 1.1 0.2 63.2%
Min. Value 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% -
Uncertainty† ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD -

†Uncertainty measurement is for the test procedure and the instrument used; and is calculated in accordance with the ISO "Guide of Uncertainty in Measurement" (GUM) Test Results and uncertainty are only representative of the sample submit to our laboratory. Uncertainty does not account for any uncertainty in the sampling. The measurement of uncertainty is the expanded uncertainty and is an estimate of uncertainty calculated with normal distribution and a coverage factor of 2 (K=2) to approximate a 95% confidence level. 

%RSD = Relative Standard Deviation; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units

N/D designates a value that is not detected above the methods Limit of quantitation (min. value)

Values are not adjusted for moisture content.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Jon Markey Iron laboratories Jon Markey

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories

Residual Solvents Analysis by
Mass Spectrometer
Test Certificate #: 104319-001
Client Name, Sample Details

The Real Biz
, MI
Sample: Gorilla Glue Wax
Type: Medical Compliant Flower
Method: SOP FE-44-MI
Test Conditions

Scale: XS205-MI1
Temp: 21.7 °C
Baro Pressure: 979.1 hPa
Analyst: MEH
Technician: JCM
Sample ID#: 104319

Harvest/Process Date: 03/15/2018
Date Received: 03/15/2018
Test Date: 03/15/2018
Valid Through: 03/15/2019
Report Issued: 03/16/2018
Sample #104319
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Not Tested 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 50 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 50 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 150 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 5 Pass/<LOD
Propane 5,000 50 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 200 160 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 5,000 100 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Jon Markey Iron laboratories Jon Markey

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 104319-001
Client Name, Sample Details

The Real Biz
, MI
Sample: Gorilla Glue Wax
Type: Medical Compliant Flower
Method: SOP FE-44-MI
Test Conditions

Scale: XS205-MI1
Temp: 21.7 °C
Baro Pressure: 979.1 hPa
Analyst: MEH
Technician: JCM
Sample ID#: 104319

Harvest/Process Date: 03/15/2018
Date Received: 03/15/2018
Test Date: 03/15/2018
Valid Through: 03/15/2019
Report Issued: 03/16/2018
Sample #104319

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.090 %

β-Ocimene:

 N/D

Camphene:

0.030 %

Eucalyptol (1,8-Cineol):

0.010 %

Sabinene:

 N/D

γ-Terpinene:

0.010 %

Myrcene:

0.090 %

α-Terpinolene:

0.010 %

β-Pinene:

0.120 %

Linalool:

0.180 %

∆3-Carene:

 N/D

Fenchone:

0.010 %

α-Terpinene:

0.010 %

Fenchol:

0.390 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.280 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

1.260 %

α-Humulene:

0.400 %

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 2.890%
(not included in calculated total): a-terpineol = 0.31%

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Jon Markey Iron laboratories Jon Markey

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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