IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 103579-001
Client Name, Sample Details

Tri-Comb
Inkster, MI 48141
Sample: Straw Nana Sauce/THCa
Type: Infused Product
Method: FE04 HPLC1100-1
Test Conditions

Scale: XS205-MI2
Temp: 21.5 °C
Baro Pressure: 959.4 hPa
Analyst: MEH
Technician: MEH
Sample ID#: 103579

Harvest/Process Date: 02/26/2018
Serving Size (g): 1
Date Received: 02/26/2018
Test Date: 02/27/2018
Valid Through: 02/27/2019
Report Issued: 02/27/2018
Sample #103579
Sample #103579 Sample #103579
Test
Compounds		 CBDA CBD CBN THC THCA TOTAL CBD Act. THC Act.
Amount 22.9 N/D 1.5 126.5 682.9 833.8 0% 16%
Min. Value 0.1 mg/g 0.1 mg/g 0.1 mg/g 0.1 mg/g 0.1 mg/g - - -
Amount per Serving~ 22.9 mg/srv N/D 1.5 mg/srv 126.5 mg/srv 682.9 mg/srv 833.8 mg/srv Serving Size~ (g): 1.00 g
Uncertainty† ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD - - -

†Uncertainty measurement is for the test procedure and the instrument used; and is calculated in accordance with the ISO "Guide of Uncertainty in Measurement" (GUM) Test Results and uncertainty are only representative of the sample submit to our laboratory. Uncertainty does not account for any uncertainty in the sampling. The measurement of uncertainty is the expanded uncertainty and is an estimate of uncertainty calculated with normal distribution and a coverage factor of 2 (K=2) to approximate a 95% confidence level. 

%RSD = Relative Standard Deviation; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units

N/D designates a value that is not detected above the methods Limit of quantitation (min. value)

Values are not adjusted for moisture content.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Jon Markey Iron laboratories Jon Markey

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 2
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 103579-001
Client Name, Sample Details

Tri-Comb
Inkster, MI 48141
Sample: Straw Nana Sauce/THCa
Type: Infused Product
Method: SOP FE-44-MI
Test Conditions

Scale: XS205-MI2
Temp: 21.5 °C
Baro Pressure: 989.4 hPa
Analyst: MEH
Technician: CTM
Sample ID#: 103579

Harvest/Process Date: 02/26/2018
Serving Size (g): 1
Date Received: 02/26/2018
Test Date: 02/28/2018
Valid Through: 02/28/2019
Report Issued: 03/01/2018
Sample #103579

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.110 %

β-Ocimene:

 N/D

Camphene:

0.040 %

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

0.010 %

Myrcene:

0.380 %

α-Terpinolene:

0.020 %

β-Pinene:

0.140 %

Linalool:

0.460 %

∆3-Carene:

 N/D

Fenchone:

0.010 %

α-Terpinene:

0.010 %

Fenchol:

0.300 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.490 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

2.200 %

α-Humulene:

1.160 %

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 5.330%
(not included in calculated total): a-terpineol = 0.24%

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Jon Markey Iron laboratories Jon Markey

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 2