ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-002 Test Certificate #: 103212-001
Client Name, Sample Details

GreenSea Distribution
Eugene, OR 97401
Sample: OMG- LBSD
License: 060-10041438CDF
Type: Medical Compliant Flower
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300005FB5000005803

Test Conditions

Prepsheet ID#: P180213c
Scale: XS205-OR1
Temp: 20.4 °C
Baro Pressure: 1005 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 103212

Lot #: BHO- Lambs Breath Sour Diesel
Batch #: 103212
Batch Weight (g): 660
Harvest/Process Date: 02/06/2018
Serving Size (g): 0.01
Package Weight (g):1
Date Received: 02/13/2018
Test Date: 02/13/2018

Sample #103212
Sample #103212 Sample #103212
Test
Compounds
CBDV CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Avg
Avg. Amount N/D 1.89 mg/g N/D 5.82 mg/g 3.77 mg/g 20.17 mg/g 66.41 mg/g 786.17 mg/g 3.62 mg/g CBD 1.66 mg/g
LOQ 0.2 mg/g 0.2 mg/g 0.2 mg/g 0.2 mg/g 0.2 mg/g 0.2 mg/g 0.2 mg/g 0.2 mg/g 0.2 mg/g THC 755.88 mg/g
Amount per Serving~ N/D 0.02 mg/srv N/D 0.06 mg/srv 0.04 mg/srv 0.20 mg/srv 0.66 mg/srv 7.86 mg/srv 0.04 mg/srv Serving Size~ (g): 0.01 g
Uncertainty 3.77% RPD 3.49% RPD 3.79% RPD 4.85% RPD 3.40% RPD 6.07% RPD ±5% RPD 2.20% RPD 3.82% RPD

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

*** Designated tests that use the method FE-45.

Total CBD or THC is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

Calc. Avg. is the calculated average of total CBD or total THC for all increments tested.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 6

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

QC Report

Testing Accreditation #: 4092-002 Test Certificate #: 103212-001
Client Name, Sample Details

GreenSea Distribution
Eugene, OR 97401
Sample: OMG- LBSD
License: 060-10041438CDF
Type: Medical Compliant Flower
Method: FE04C-OR4 HPLC1100-OR1
Metrc Test Pkg#: 1A4010300005FB5000005803

Test Conditions

Prepsheet ID#: P180213c
Scale: XS205-OR1
Temp: 20.4 °C
Baro Pressure: 1005 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 103212

Lot #: BHO- Lambs Breath Sour Diesel
Batch #: 103212
Batch Weight (g): 660
Harvest/Process Date: 02/06/2018
Serving Size (g): 0.01
Package Weight (g):1
Date Received: 02/13/2018
Test Date: 02/13/2018

Sample #103212
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.63 4.42 95.46 4.59 99.14 3.77%
Cannabidiolic Acid (CBDA) N.D. 4.73 4.5 95.14 4.66 98.52 3.49%
Cannabigerol (CBG) N.D. 4.54 4.34 95.59 4.49 98.90 3.40%
Cannabidiol (CBD) N.D. 4.9 4.66 95.10 4.84 98.78 3.79%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 4.57 4.37 95.62 4.54 99.34 3.82%
Cannabinol (CBN) N.D. 4.75 4.47 94.11 4.75 100.00 6.07%
Δ9-Tetrahydrocannabinol (THC) N.D. 4.86 4.74 97.53 4.8 98.77 1.26%
Cannabichromene (CBC) N.D. 5.05 4.83 95.64 5.07 100.40 4.85%
Tetrahydrocannabinolic acid (THCA) N.D. 4.66 4.49 96.35 4.59 98.50 2.20%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 6

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-002 Test Certificate #: 103212-001
Client Name, Sample Details

GreenSea Distribution
Eugene, OR 97401
Sample: OMG- LBSD
License: 060-10041438CDF
Type: Medical Compliant Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300005FB5000005803

Test Conditions

Prepsheet ID#: PS180216a
Scale: Veritas-OR1
Temp: 19.4 °C
Baro PE: 1013 hPa
Analyst: JER
Technician: JER

Sample ID#: 103212

Lot #: BHO- Lambs Breath Sour Diesel
Batch #: 103212
Batch Weight (g): 660
Harvest/Process Date: 02/06/2018
Serving Size (g): 0.01
Package Weight (g):1
Date Received: 02/13/2018
Test Date: 02/19/2018

Sample #103212
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.100 Pass/<LOD Abamectin**** 0.500 0.100 Pass/<LOD
Acephate 0.400 0.100 Pass/<LOD Acequinocyl 2.000 0.200 Pass/<LOD
Acetamiprid 0.200 0.100 Pass/<LOD Azoxystrobin 0.200 0.100 Pass/<LOD
Bifenazate 0.200 0.100 Pass/<LOD Bifenthrin 0.200 0.100 Pass/<LOD
Boscalid 0.400 0.100 Pass/<LOD Carbaryl 0.200 0.100 Pass/<LOD
Carbofuran 0.200 0.100 Pass/<LOD Chlorantraniliprole 0.200 0.100 Pass/<LOD
Chlorfenapyr 1.000 1.000 Pass/<LOD Chlorpyrifos 0.200 0.100 Pass/<LOD
Clofentezine 0.200 0.100 Pass/<LOD Cyfluthrin** 1.000 0.500 Pass/<LOD
Cypermethrin*** 1.000 0.500 Pass/<LOD Daminozide 1.000 0.100 Pass/<LOD
DDVP (Dichlorvos) 0.100 0.100 Pass/<LOD Diazinon 0.200 0.100 Pass/<LOD
Dimethoate 0.200 0.100 Pass/<LOD Ethoprophos 0.200 0.100 Pass/<LOD
Etofenprox 0.400 0.100 Pass/<LOD Etoxazole 0.200 0.100 Pass/<LOD
Fenoxycarb 0.200 0.100 Pass/<LOD Fenpyroximate 0.400 0.100 Pass/<LOD
Fipronil 0.400 0.100 Pass/<LOD Flonicamid 1.000 0.100 Pass/<LOD
Fludioxonil 0.400 0.100 Pass/<LOD Hexythiazox 1.000 0.100 Pass/<LOD
Imazalil 0.200 0.100 Pass/<LOD Imidacloprid 0.400 0.100 Pass/<LOD
Kresoxim Methyl 0.400 0.100 Pass/<LOD Malathion 0.200 0.100 Pass/<LOD
Metalaxyl 0.200 0.100 Pass/<LOD Methiocarb 0.200 0.100 Pass/<LOD
Methomyl 0.400 0.100 Pass/<LOD Methyl Parathion 0.200 0.500 Pass/<LOD
MGK-264‡ 0.200 0.100 Pass/<LOD Myclobutanil 0.200 0.100 Pass/<LOD
Naled 0.500 0.100 Pass/<LOD Oxamyl 1.000 0.100 Pass/<LOD
Paclobutrazol 0.400 0.100 Pass/<LOD Permethrins† 0.200 0.100 Pass/<LOD
Phosmet 0.200 0.100 Pass/<LOD Piperonyl Butoxide 2.000 0.100 Pass/<LOD
Prallethrin 0.200 0.100 Pass/<LOD Propiconazole 0.400 0.100 Pass/<LOD
Propoxur 0.200 0.100 Pass/<LOD Pyrethrins* 1.000 0.100 Pass/<LOD
Pyridaben 0.200 0.100 Pass/<LOD Spinosad***** 0.200 0.100 Pass/<LOD
Spiromesifen 0.200 0.100 Pass/<LOD Spirotetramat 0.200 0.100 Pass/<LOD
Spiroxamine‡ 0.400 0.100 Pass/<LOD Tebuconazole 0.400 0.100 Pass/<LOD
Thiacloprid 0.200 0.100 Pass/<LOD Thiamethoxam 0.200 0.100 Pass/<LOD
Trifloxystrobin 0.200 0.100 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 6

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide QC Report

Testing Accreditation #: 4092-002 Test Certificate #: 103212-001
Client Name, Sample Details

GreenSea Distribution
Eugene, OR 97401
Sample: OMG- LBSD
License: 060-10041438CDF
Type: Medical Compliant Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300005FB5000005803

Test Conditions

Prepsheet ID#: PS180216a
Scale: Veritas-OR1
Temp: 19.4 °C
Baro PE: 1013 hPa
Analyst: JER
Technician: JER

Sample ID#: 103212

Lot #: BHO- Lambs Breath Sour Diesel
Batch #: 103212
Batch Weight (g): 660
Harvest/Process Date: 02/06/2018
Serving Size (g): 0.01
Package Weight (g):1
Date Received: 02/13/2018
Test Date: 02/19/2018

Sample #103212
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 .908 .979 90.80 97.90 7.53
Acequinocyl N.D. 1 .317 .495 31.70 49.50 43.84 LRQ
Acetamiprid N.D. 1 .941 1.02 94.10 102.00 8.06
Aldicarb N.D. 1 .941 .951 94.10 95.10 1.06
Avermectin B1a N.D. 0.97 1.17 .965 120.62 99.48 19.20
Azoxystrobin N.D. 1 1.03 .983 103.00 98.30 4.67
Bifenazate N.D. 1 .723 .767 72.30 76.70 5.91
Bifenthrin N.D. 1 .673 .748 67.30 74.80 10.56 LR
Boscalid N.D. 1 .788 .866 78.80 86.60 9.43
Carbaryl N.D. 1 1.08 1.07 108.00 107.00 0.93
Carbofuran N.D. 1 1.22 1.09 122.00 109.00 11.26
Chlorantraniliprole N.D. 1 .905 .968 90.50 96.80 6.73
Chlorfenapyr N.D. 1 .991 1.01 99.10 101.00 1.90
Chlorpyriphos N.D. 1 .820 .881 82.00 88.10 7.17
Clofentezine N.D. 1 .725 .847 72.50 84.70 15.52
Cyfluthrin N.D. 1 .833 .748 83.30 74.80 10.75
Cypermethrin N.D. 1 .924 .753 92.40 75.30 20.39
Daminoside N.D. 1 .679 .837 67.90 83.70 20.84 LR
Diazanon N.D. 1 .80 .860 80.00 86.00 7.23
Dichlorvos N.D. 1 .894 .972 89.40 97.20 8.36
Dimethoate N.D. 1 .980 .966 98.00 96.60 1.44
Ethoprophos N.D. 1 .811 .930 81.10 93.00 13.67
Etofenprox N.D. 1 .639 .735 63.90 73.50 13.97 LR
Etoxazole N.D. 1 .985 .830 98.50 83.00 17.08
Fenoxycarb N.D. 1 .975 1.02 97.50 102.00 4.51
Fenpyroximate N.D. 1 .679 .734 67.90 73.40 7.78 LR
Fipronil N.D. 1 1.02 1.02 102.00 102.00 0.00
Flonicamid N.D. 1 .914 1.01 91.40 101.00 9.98
Fludioxonil N.D. 1 .946 .946 94.60 94.60 0.00
Hexythiazox N.D. 1 .680 .604 68.00 60.40 11.84 LR
Imazalil N.D. 1 1.11 1.04 111.00 104.00 6.51
Imidacloprid N.D. 1 .767 .97 76.70 97.00 23.37 Q
Kresoxim-methyl N.D. 1 .831 .88 83.10 88.00 5.73
Malathion N.D. 1 .985 .978 98.50 97.80 0.71
Metalaxyl N.D. 1 .976 .979 97.60 97.90 0.31
Methiocarb N.D. 1 .936 .998 93.60 99.80 6.41
Methomyl N.D. 1 .853 .920 85.30 92.00 7.56
MGK-264 N.D. 1 .857 .905 85.70 90.50 5.45
Myclobutanil N.D. 1 .910 .968 91.00 96.80 6.18
Naled (dibrom) N.D. 1 .909 .948 90.90 94.80 4.20
Oxamyl N.D. 1 .967 .974 96.70 97.40 0.72
Paclobutrazol N.D. 1 .918 1.01 91.80 101.00 9.54
Parathion-methyl N.D. 1 .772 .824 77.20 82.40 6.52
Permethrins N.D. 1 .875 .728 87.50 72.80 18.34
Phosmet N.D. 1 .975 1.01 97.50 101.00 3.53
Piperonyl butoxide N.D. 1 .944 .924 94.40 92.40 2.14
Prallethrin N.D. 1 1.1 1.03 110.00 103.00 6.57
Propiconazole N.D. 1 .818 .946 81.80 94.60 14.51
Propoxur N.D. 1 1.09 1.10 109.00 110.00 0.91
Pyrethrin N.D. .65 .674 .605 103.69 93.08 10.79
Pyridaben N.D. 1 .750 .716 75.00 71.60 4.64
SpinosynA N.D. .84 .894 .960 106.43 114.29 7.12
SpinosynD N.D. .16 .164 .166 102.50 103.75 1.21
Spiromesifen N.D. 1 .780 .706 78.00 70.60 9.96
Spirotetramat N.D. 1 1.12 1.01 112.00 101.00 10.33
Spiroxamine N.D. 1 1.04 .942 104.00 94.20 9.89
Tebuconazole N.D. 1 .824 .945 82.40 94.50 13.68
Thiacloprid N.D. 1 .840 .996 84.00 99.60 16.99
Thiamethoxam N.D. 1 .828 .902 82.80 90.20 8.55
Trifloxystrobin N.D. 1 1 1.02 100.00 102.00 1.98

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 6

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-002 Test Certificate #: 103212-001
Client Name, Sample Details

GreenSea Distribution
Eugene, OR 97401
Sample: OMG- LBSD
License: 060-10041438CDF
Type: Medical Compliant Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300005FB5000005803

Test Conditions

Prepsheet ID#: HS180215a
Scale: XS205-OR1
Temp: 20.4 °C
Baro PE: 1016 hPa
Analyst: JER
Technician: JER

Sample ID#: 103212

Lot #: BHO- Lambs Breath Sour Diesel
Batch #: 103212
Batch Weight (g): 660
Harvest/Process Date: 02/06/2018
Serving Size (g): 0.01
Package Weight (g):1
Date Received: 02/13/2018
Test Date: 02/16/2018

Sample #103212
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/54 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 150 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 5 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 5,000 100 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 6

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Residual Solvents QC Report

Testing Accreditation #: 4092-002 Test Certificate #: 103212-001
Client Name, Sample Details

GreenSea Distribution
Eugene, OR 97401
Sample: OMG- LBSD
License: 060-10041438CDF
Type: Medical Compliant Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300005FB5000005803

Test Conditions

Prepsheet ID#: HS180215a
Scale: XS205-OR1
Temp: 20.4 °C
Baro PE: 1016 hPa
Analyst: JER
Technician: JER

Sample ID#: 103212

Lot #: BHO- Lambs Breath Sour Diesel
Batch #: 103212
Batch Weight (g): 660
Harvest/Process Date: 02/06/2018
Serving Size (g): 0.01
Package Weight (g):1
Date Received: 02/13/2018
Test Date: 02/16/2018

Sample #103212
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane N.D. 250 174 163 69.60 65.20 6.53 LR
Isobutane N.D. 250 197 182 78.80 72.80 7.92
Methanol N.D. 250 272 236 108.80 94.40 14.17
n-Butane N.D. 250 206 199 82.40 79.60 3.46
2,2-Dimethylpropane N.D. 250 210 198 84.00 79.20 5.88
Ethanol N.D. 250 247 243 98.80 97.20 1.63
Isopentane N.D. 250 225 218 90.00 87.20 3.16
Acetonitrile N.D. 250 261 254 104.40 101.60 2.72
Diethyl ether N.D. 250 237 236 94.80 94.40 0.42
2-propanone N.D. 250 281 267 112.40 106.80 5.11
2-propanol N.D. 250 468 717 187.20 286.80 42.03 HRQ
n-Pentane N.D. 250 202 190 80.80 76.00 6.12
2,2-Dimethylbutane N.D. 250 225 225 90.00 90.00 0.00
2,3-Dimethylbutane N.D. 250 237 227 94.80 90.80 4.31
Methylene chloride N.D. 250 270 269 108.00 107.60 0.37
2-Methylpentane N.D. 250 236 235 94.40 94.00 0.42
3-Methylpentane N.D. 250 230 231 92.00 92.40 0.43
2-Butanol N.D. 250 246 242 98.40 96.80 1.64
n-Hexane N.D. 250 232 227 92.80 90.80 2.18
Ethyl acetate N.D. 250 251 257 100.40 102.80 2.36
Tetrahydrofuran N.D. 250 241 237 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate N.D. 250 263 255 0.00 0.00 0.00
Benzene N.D. 250 254 248 101.60 99.20 2.39
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 238 237 95.20 94.80 0.42
Ethylene glycol N.D. 250 198 230 79.20 92.00 14.95
Heptane N.D. 250 239 242 95.60 96.80 1.25
2-Ethoxyethanol N.D. 250 254 254 101.60 101.60 0.00
1,4-Dioxane N.D. 250 245 244 98.00 97.60 0.41
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 255 253 102.00 101.20 0.79
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 249 241 99.60 96.40 3.27
m-Xylene/p-Xylene N.D. 500 504 492 100.80 98.40 2.41
o-Xylene N.D. 250 250 240 100.00 96.00 4.08
Cumene N.D. 250 247 241 98.80 96.40 2.46
Ethylene oxide N.D. 250 343 337 137.20 134.80 1.76 HR

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Homogeneity Report by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-002 Test Certificate #: 103212-001
Client Name, Sample Details

GreenSea Distribution
Eugene, OR 97401
Sample: OMG- LBSD
License: 060-10041438CDF
Type: Medical Compliant Flower
Metrc Test Pkg#: 1A4010300005FB5000005803

Sample ID#: 103212

Lot #: BHO- Lambs Breath Sour Diesel
Batch #: 103212
Batch Weight (g): 660
Harvest/Process Date: 02/06/2018
Serving Size (g): 0.01
Package Weight (g):1
Date Received: 02/13/2018

Sample #103212
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 757.00 1.66 65.21 788.81 3.48 N.D. 6.07 1.89 N.D. 3.75 20.35
Increment 2 754.76 1.66 67.61 783.52 3.76 N.D. 5.57 1.89 N.D. 3.78 19.99
Average Value 755.88 1.66 66.41 786.17 3.62 N.D. 5.82 1.89 N.D. 3.77 20.17
Max Value 757.00 1.66 67.61 788.81 3.76 N.D. 6.07 1.89 N.D. 3.78 20.35
Min Value 754.76 1.66 65.21 783.52 3.48 N.D. 5.57 1.89 N.D. 3.75 19.99
Relative Percent Difference (RPD) ±0.30 N.D. ±3.61 ±0.67 ±7.73 N.D. ±8.59 N.D. N.D. ±0.80 ±1.78
Average Cannabinoids Per Package 755.88 1.66 66.41 786.17 3.62 N.D. 5.82 1.89 N.D. 3.77 20.17
Average Cannabinoids Per Serving 7.56 0.02 0.66 7.86 0.04 N.D. 0.06 0.02 N.D. 0.04 0.20
Max Concentration Per Serving (THC)   Pass
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ380
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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