ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-002 Test Certificate #: 101316-001
Client Name, Sample Details

Matt Presby
Simi Valley , CA 93063
Sample: Gorilla Glue 4
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Prepsheet ID#: PS171218a
Scale: Veritas-OR1
Temp: 20.1 °C
Baro PE: 998.7 hPa
Analyst: JER
Technician: JER
Sample ID#: 101316

Harvest/Process Date: 12/15/2017
Test Date: 12/20/2017
Sample #101316
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.100 Pass/<LOD Abamectin**** 0.500 0.100 Pass/<LOD
Acephate 0.400 0.100 Pass/<LOD Acequinocyl 2.000 0.200 Pass/<LOD
Acetamiprid 0.200 0.100 Pass/<LOD Azoxystrobin 0.200 0.100 Pass/<LOD
Bifenazate 0.200 0.100 Pass/<LOD Bifenthrin 0.200 0.100 Pass/<LOD
Boscalid 0.400 0.100 Pass/<LOD Carbaryl 0.200 0.100 Pass/<LOD
Carbofuran 0.200 0.100 Pass/<LOD Chlorantraniliprole 0.200 0.100 Pass/<LOD
Chlorfenapyr 1.000 1.000 Pass/<LOD Chlorpyrifos 0.200 0.100 Pass/<LOD
Clofentezine 0.200 0.100 Pass/<LOD Cyfluthrin** 1.000 0.500 Pass/<LOD
Cypermethrin*** 1.000 0.500 Pass/<LOD Daminozide 1.000 0.100 Pass/<LOD
DDVP (Dichlorvos) 0.100 0.100 Pass/<LOD Diazinon 0.200 0.100 Pass/<LOD
Dimethoate 0.200 0.100 Pass/<LOD Ethoprophos 0.200 0.100 Pass/<LOD
Etofenprox 0.400 0.100 Pass/<LOD Etoxazole 0.200 0.100 Pass/<LOD
Fenoxycarb 0.200 0.100 Pass/<LOD Fenpyroximate 0.400 0.100 Pass/<LOD
Fipronil 0.400 0.100 Pass/<LOD Flonicamid 1.000 0.100 Pass/<LOD
Fludioxonil 0.400 0.100 Pass/<LOD Hexythiazox 1.000 0.100 Pass/<LOD
Imazalil 0.200 0.100 Pass/<LOD Imidacloprid 0.400 0.100 Pass/<LOD
Kresoxim Methyl 0.400 0.100 Pass/<LOD Malathion 0.200 0.100 Pass/<LOD
Metalaxyl 0.200 0.100 Pass/<LOD Methiocarb 0.200 0.100 Pass/<LOD
Methomyl 0.400 0.100 Pass/<LOD Methyl Parathion 0.200 0.500 Pass/<LOD
MGK-264‡ 0.200 0.100 Pass/<LOD Myclobutanil 0.200 0.100 Failed/0.911
Naled 0.500 0.100 Pass/<LOD Oxamyl 1.000 0.100 Pass/<LOD
Paclobutrazol 0.400 0.100 Pass/0.333 Permethrins† 0.200 0.100 Pass/<LOD
Phosmet 0.200 0.100 Pass/<LOD Piperonyl Butoxide 2.000 0.100 Pass/<LOD
Prallethrin 0.200 0.100 Pass/<LOD Propiconazole 0.400 0.100 Pass/<LOD
Propoxur 0.200 0.100 Pass/<LOD Pyrethrins* 1.000 0.100 Pass/<LOD
Pyridaben 0.200 0.100 Pass/<LOD Spinosad***** 0.200 0.100 Pass/<LOD
Spiromesifen 0.200 0.100 Pass/<LOD Spirotetramat 0.200 0.100 Pass/<LOD
Spiroxamine‡ 0.400 0.100 Pass/<LOD Tebuconazole 0.400 0.100 Pass/<LOD
Thiacloprid 0.200 0.100 Pass/<LOD Thiamethoxam 0.200 0.100 Pass/<LOD
Trifloxystrobin 0.200 0.100 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 2

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-002
OLCC No. 1002158CD2E

Pesticide QC Report
Testing Accreditation #: 4092-002 Test Certificate #: 101316-001
Client Name, Sample Details

Matt Presby
Simi Valley , CA 93063
Sample: Gorilla Glue 4
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Prepsheet ID#: PS171218a
Scale: Veritas-OR1
Temp: 20.1 °C
Baro PE: 998.7 hPa
Analyst: JER
Technician: JER
Sample ID#: 101316

Harvest/Process Date: 12/15/2017
Test Date: 12/20/2017
Sample #101316
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N/D 1 .862 .862 86.20 86.20 0.00
Acequinocyl N/D 1 1.37 1.07 137.00 107.00 24.59 HRQ
Acetamiprid N/D 1 1.02 1.03 102.00 103.00 0.98
Aldicarb N/D 1 .852 .821 85.20 82.10 3.71
Avermectin B1a N/D .97 .936 .889 96.49 91.65 5.15
Azoxystrobin N/D 1 .797 .707 79.70 70.70 11.97
Bifenazate N/D 1 .927 .912 92.70 91.20 1.63
Bifenthrin N/D 1 .807 .693 80.70 69.30 15.20 LR
Boscalid N/D 1 1.06 1.03 106.00 103.00 2.87
Carbaryl N/D 1 .874 .843 87.40 84.30 3.61
Carbofuran N/D 1 .974 .968 97.40 96.80 0.62
Chlorantraniliprole N/D 1 .556 .536 55.60 53.60 3.66 LR
Chlorfenapyr N/D 1 1.1 1.15 110.00 115.00 4.44
Chlorpyriphos N/D 1 .972 .989 97.20 98.90 1.73
Clofentezine N/D 1 .826 .836 82.60 83.60 1.20
Cyfluthrin N/D 1 .826 .876 82.60 87.60 5.88
Cypermethrin N/D 1 .838 .891 83.80 89.10 6.13
Daminoside N/D 1 0.012 .06 1.20 6.00 133.33 LRQ
Diazanon N/D 1 .755 .734 75.50 73.40 2.82
Dichlorvos N/D 1 1.07 1.04 107.00 104.00 2.84
Dimethoate N/D 1 .915 1.05 91.50 105.00 13.74
Ethoprophos N/D 1 1.03 .995 103.00 99.50 3.46
Etofenprox N/D 1 .823 .749 82.30 74.90 9.41
Etoxazole N/D 1 .936 .928 93.60 92.80 0.86
Fenoxycarb N/D 1 .893 .865 89.30 86.50 3.19
Fenpyroximate N/D 1 .998 1.01 99.80 101.00 1.20
Fipronil N/D 1 .867 1.03 86.70 103.00 17.19
Flonicamid N/D 1 1.27 1.12 127.00 112.00 12.55
Fludioxonil N/D 1 .751 .937 75.10 93.70 22.04 Q
Hexythiazox N/D 1 .658 .637 65.80 63.70 3.24 LR
Imazalil N/D 1 .568 .475 56.80 47.50 17.83 LR
Imidacloprid N/D 1 1.02 1.09 102.00 109.00 6.64
Kresoxim-methyl N/D 1 1.09 1.04 109.00 104.00 4.69
Malathion N/D 1 1.14 1.17 114.00 117.00 2.60
Metalaxyl N/D 1 .964 .922 96.40 92.20 4.45
Methiocarb N/D 1 .971 .965 97.10 96.50 0.62
Methomyl N/D 1 1.01 1.05 101.00 105.00 3.88
MGK-264 N/D 1 .848 .807 84.80 80.70 4.95
Myclobutanil N/D 1 1.03 1.063 103.00 106.30 3.15
Naled (dibrom) N/D 1 .664 .646 66.40 64.60 2.75 LR
Oxamyl N/D 1 1.12 1.17 112.00 117.00 4.37
Paclobutrazol N/D 1 1.07 1.03 107.00 103.00 3.81
Parathion-methyl N/D 1 1.01 .940 101.00 94.00 7.18
Permethrins N/D 1 .994 .524 99.40 52.40 61.92 LRQ
Phosmet N/D 1 1.02 .957 102.00 95.70 6.37
Piperonyl butoxide N/D 1 1.16 1.21 116.00 121.00 4.22
Prallethrin N/D 1 .904 .818 90.40 81.80 9.99
Propiconazole N/D 1 1.21 1.17 121.00 117.00 3.36
Propoxur N/D 1 .959 .956 95.90 95.60 0.31
Pyrethrin N/D .65 .673 .632 103.54 97.23 6.28
Pyridaben N/D 1 .956 .925 95.60 92.50 3.30
SpinosynA N/D .84 .796 .778 94.76 92.62 2.29
SpinosynD N/D .16 .145 .139 90.63 86.88 4.23
Spiromesifen N/D 1 .267 .274 26.70 27.40 2.59 LR
Spirotetramat N/D 1 1.18 1.15 118.00 115.00 2.58
Spiroxamine N/D 1 .847 .714 84.70 71.40 17.04
Tebuconazole N/D 1 1.03 .969 103.00 96.90 6.10
Thiacloprid N/D 1 .839 .846 83.90 84.60 0.83
Thiamethoxam N/D 1 1.03 1.1 103.00 110.00 6.57
Trifloxystrobin N/D 1 1.02 1.01 102.00 101.00 0.99

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 2